16-oxoandrostenediol, MO TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-12851.Hähnel, Wilkinson, et al., 1985He; Column length: 25. m; Column diameter: 0.3 mm; Program: 40C (1min) => 20C/min => 200C => 2C/min => 300C (11min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-12902.Yong, Pitt, et al., 1988Helium, 3. K/min; Column length: 25. m; Column diameter: 0.22 mm; Tstart: 180. C; Tend: 300. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Hähnel, Wilkinson, et al., 1985
Hähnel, E.; Wilkinson, S.P.; Hähnel, R., Urinary steroid profiles in pregnancy by capillary column gas chromatography, Clin. Chim. Acta, 1985, 151, 3, 259-271, https://doi.org/10.1016/0009-8981(85)90089-0 . [all data]

Yong, Pitt, et al., 1988
Yong, A.B.W.; Pitt, J.J.; Montalto, J.; Davies, H.E.; Warne, G.L.; Connelly, J.F., Diagnosis of 21-hydroxylase deficiency in newborn infants by GC-MS of urinary steroids, Aust. Paediatr., 1988, 24, 280-285. [all data]


Notes

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