β-Lactose, TMS


Gas Chromatography

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

View large format table.

Column type Active phase Temperature (C) I Reference Comment
CapillarySE-54280.2833.García-Raso, Páez, et al., 1992N2; Column length: 40. m; Column diameter: 0.18 mm
CapillaryOV-101272.2790.Adam and Jennings, 1975Column length: 45. m; Column diameter: 0.25 mm

Kovats' RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-5MS2838.Medeiros and Simoneit, 200730. m/0.25 mm/0.25 μm, He, 65. C @ 2. min, 6. K/min, 300. C @ 15. min

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

García-Raso, Páez, et al., 1992
García-Raso, A.; Páez, M.I.; Martínez-Castro, I.; Sanz, J.; Calvo, M.M., Gas chromatographic retention of carbohydrate trimethylsilyl ethers. IV. Disaccharides, J. Chromatogr., 1992, 607, 2, 221-225, https://doi.org/10.1016/0021-9673(92)87079-N . [all data]

Adam and Jennings, 1975
Adam, S.; Jennings, W.G., Gas chromatographic separation of silylated derivatives of disaccharide mixtures on open tubular glass capillary columns, J. Chromatogr., 1975, 115, 1, 218-221, https://doi.org/10.1016/S0021-9673(00)89035-4 . [all data]

Medeiros and Simoneit, 2007
Medeiros, P.M.; Simoneit, B.R.T., Analysis of sugars in environmental samples by gas chromatography-mass spectrometry, J. Chromatogr. A, 2007, 1141, 2, 271-278, https://doi.org/10.1016/j.chroma.2006.12.017 . [all data]


Notes

Go To: Top, Gas Chromatography, References