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4a«alpha»,7«alpha»,7a«alpha»-Nepetalactone


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1344.Gkinis, Tzakou, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51371.Tzakou, Harvala, et al., 200050. C @ 5. min, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tend: 250. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51365.Bertoli, Menichini, et al., 200430. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-51365.Ertugrul, Dural, et al., 200330. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-51375.Skaltsa, Lazari, et al., 200030. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 4. K/min; Tend: 280. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-5MS1370.Eom S.H., Yang H.S., et al., 200630. m/0.25 mm/0.25 «mu»m, He; Program: 50C(3min) => 200C(2min) => 15C/min => 300C(5min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-11322.Sefidkon, Jamzad, et al., 2006He, 4. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 40. C; Tend: 250. C
CapillaryDB-11322.Sefidkon and Shaabani, 200460. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-11317.Dabiri and Sefidkon, 2003He, 4. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 250. C
CapillaryDB-11323.Dabiri and Sefidkon, 2003, 2He, 4. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 250. C
CapillaryCP Sil 5 CB1337.Rustaiyan and Nadji, 199925. m/0.25 mm/0.39 «mu»m, N2, 5. K/min; Tstart: 60. C; Tend: 220. C
CapillaryOV-11344.Kökdil, Kurucu, et al., 199730. m/0.32 mm/0.25 «mu»m, He, 40. C @ 4. min, 2. K/min; Tend: 270. C
CapillaryOV-11322.de Pooter, Nicolai, et al., 198850. m/0.20 mm/0.20 «mu»m, He, 2. K/min; Tstart: 30. C; Tend: 220. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOptima-5MS1353.HEuskin, Godin, et al., 200930. m/0.32 mm/0.25 «mu»m, Helium; Program: 40 0C (5 min) 5 0C/min -> 230 0C 30 0C/min -> 280 0C (5 min)
CapillaryOV-11331.Suschke, Sporer, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium; Program: 40 0C (2 min) 6 0C/min -> 130 0C 10 0C/min -> 300 0C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Gkinis, Tzakou, et al., 2003
Gkinis, G.; Tzakou, O.; Iliopoulou, D.; Roussis, V., Chemical Composition and Biological Activity of Nepeta parnassica Oils and Isolated Nepetalactones, Z. Naturforsch. C:, 2003, 58, 681-686. [all data]

Tzakou, Harvala, et al., 2000
Tzakou, O.; Harvala, C.; Galati, E.M.; Sanogo, R., Essential oil composition of Nepeta argolica Borey et Chaub. subsp. argolica, Flavour Fragr. J., 2000, 15, 2, 115-118, https://doi.org/10.1002/(SICI)1099-1026(200003/04)15:2<115::AID-FFJ877>3.0.CO;2-9 . [all data]

Bertoli, Menichini, et al., 2004
Bertoli, A.; Menichini, F.; Noccioli, C.; Morelli, I.; Pistelli, L., Volatile constituents of different organs of Psoralea bituminosa L., Flavour Fragr. J., 2004, 19, 2, 166-171, https://doi.org/10.1002/ffj.1315 . [all data]

Ertugrul, Dural, et al., 2003
Ertugrul, K.; Dural, H.; Tugay, O.; Flamini, G.; Cioni, P.L.; Morelli, I., Essential oils from flowers of Centaurea kotschyi var. kotschyi and C. kotschyi var. decumbens from Turkey, Flavour Fragr. J., 2003, 18, 2, 95-97, https://doi.org/10.1002/ffj.1168 . [all data]

Skaltsa, Lazari, et al., 2000
Skaltsa, H.D.; Lazari, D.M.; Loukis, A.E.; Constantinidis, T., Essential oil analysis of Nepeta argolica Bory Chaub. subsp. argolica (Lamiaceae) growing wild in Greece, Flavour Fragr. J., 2000, 15, 2, 96-99, https://doi.org/10.1002/(SICI)1099-1026(200003/04)15:2<96::AID-FFJ873>3.0.CO;2-F . [all data]

Eom S.H., Yang H.S., et al., 2006
Eom S.H.; Yang H.S.; Weston L.A., An evaluation of the allelopathic potential of selected perennial groundcovers: Foliar volatiles of catmint (Nepeta x faassenii) inhibit seedling growth, J. Chem. Ecol., 2006, 32, 8, 1835-1848, https://doi.org/10.1007/s10886-006-9112-1 . [all data]

Sefidkon, Jamzad, et al., 2006
Sefidkon, F.; Jamzad, Z.; Mirza, M., Chemical composition of the essential oil of five Iranian Nepeta species (N. crispa, N. mahanensis, N. ispahanica, N. eremophila and N. rivularis), Flavour Fragr. J., 2006, 21, 5, 764-767, https://doi.org/10.1002/ffj.1668 . [all data]

Sefidkon and Shaabani, 2004
Sefidkon, F.; Shaabani, A., Essential oil composition of Nepeta meyeri Benth. from Iran, Flavour Fragr. J., 2004, 19, 3, 236-238, https://doi.org/10.1002/ffj.1294 . [all data]

Dabiri and Sefidkon, 2003
Dabiri, M.; Sefidkon, F., Chemical composition of the essential oil of Nepeta racemosa Lam. from Iran, Flavour Fragr. J., 2003, 18, 2, 157-158, https://doi.org/10.1002/ffj.1151 . [all data]

Dabiri and Sefidkon, 2003, 2
Dabiri, M.; Sefidkon, F., Chemical compositional of Nepeta crassifolia Boiss. Buhse oil from Iran, Flavour Fragr. J., 2003, 18, 3, 225-227, https://doi.org/10.1002/ffj.1199 . [all data]

Rustaiyan and Nadji, 1999
Rustaiyan, A.; Nadji, K., Composition of the essential oils of Nepeta ispahanica Boiss. and Nepeta binaludensis Jamzad from Iran, Flavour Fragr. J., 1999, 14, 1, 35-37, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<35::AID-FFJ776>3.0.CO;2-N . [all data]

Kökdil, Kurucu, et al., 1997
Kökdil, G.; Kurucu, S.; Topcu, G., Chemical constituents of the essential oils of Nepeta italica L. and Nepeta sulfuriflora P. H. Davis, Flavour Fragr. J., 1997, 12, 1, 33-35, https://doi.org/10.1002/(SICI)1099-1026(199701)12:1<33::AID-FFJ609>3.0.CO;2-V . [all data]

de Pooter, Nicolai, et al., 1988
de Pooter, H.L.; Nicolai, B.; De Laet, J.; De Buyck, L.F.; Schamp, N.M.; Goetghebeur, P., The Essential Oils of Five Nepeta Species. A Preliminary Evaluation of their Use in Chemotaxonomy by Cluster Analysis, Flavour Fragr. J., 1988, 3, 4, 155-159, https://doi.org/10.1002/ffj.2730030404 . [all data]

HEuskin, Godin, et al., 2009
HEuskin, S.; Godin, B.; Leroy, P.; Quentin C.; Wathelet, J.-P.; Verheggen, F.; Haubruge, E.; Lognay, G., Fast gas chromatography characterization of purified semiochemicals from essential oils of Matricaria chamomilla L. (Asteraceae) and Nepeta cataria L. (Lamiaceae), J. Chromatorg. A., 2009, 1216, 14, 2768-2775, https://doi.org/10.1016/j.chroma.2008.09.109 . [all data]

Suschke, Sporer, et al., 2007
Suschke, U.; Sporer, F.; Schneele, J.; Geiss, H.K.; Reichling, J., Antibacterial and Cytotoxic activity of Nepeta cataria L., Nepeta cataria var. citriodora (Beck.) Balb. and Melissa officinalis L. essential oils, Natural Product Communications, 2007, 2, 12, 1277-1286. [all data]


Notes

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