5-β-Cholestan-3-one, oxime, TMS # 2
- Formula: C30H55NOSi
- Molecular weight: 473.8493
- IUPAC Standard InChI: InChI=1S/C30H55NOSi/c1-21(2)10-9-11-22(3)26-14-15-27-25-13-12-23-20-24(31-32-33(6,7)8)16-18-29(23,4)28(25)17-19-30(26,27)5/h21-23,25-28H,9-20H2,1-8H3/t22?,23-,25?,26?,27?,28?,29?,30?/m0/s1
- IUPAC Standard InChIKey: VSEPXMZPXCXVEF-OQJUFFJBSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Species with the same structure:
- Information on this page:
- Other data available:
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Normal alkane RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary |
|---|---|
| Active phase | SE-30 |
| Column length (m) | 25. |
| Carrier gas | He |
| Substrate | |
| Column diameter (mm) | 0.32 |
| Phase thickness (μm) | 0.25 |
| Tstart (C) | 200. |
| Tend (C) | 270. |
| Heat rate (K/min) | 10. |
| Initial hold (min) | |
| Final hold (min) | |
| I | 3198. |
| Reference | Tandon, Axelson, et al., 1984 |
| Comment | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Tandon, Axelson, et al., 1984
Tandon, R.; Axelson, M.; Sjövall, J.,
Selective liquid chromatographic isolation and gas chromatographic-mass spectrometric analysis of ketonic bile acids in faeces,
J. Chromatogr., 1984, 302, 1-14, https://doi.org/10.1016/S0021-9673(01)88993-7
. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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