Aphyllidine
- Formula: C15H22N2O
- Molecular weight: 246.3480
- IUPAC Standard InChI: InChI=1S/C15H22N2O/c18-15-12-9-11(13-5-2-4-8-17(13)15)10-16-7-3-1-6-14(12)16/h5,11-12,14H,1-4,6-10H2/t11?,12?,14-/m1/s1
- IUPAC Standard InChIKey: UAAWNTMXVSONPU-ORHYLEIMSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-1 | DB-5 | DB-1 | DB-1 | DB-1 |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | |||
| Tstart (C) | 150. | 180. | 120. | 150. | 150. |
| Tend (C) | 300. | 300. | 260. | 280. | 300. |
| Heat rate (K/min) | 6. | 5. | 10. | 2. | 6. |
| Initial hold (min) | 2. | 3. | |||
| Final hold (min) | 10. | 10. | 15. | ||
| I | 2120. | 2127. | 2145. | 2125. | 2127. |
| Reference | Beuerle, 2010 | Przybylak, Ciesiolka, et al., 2005 | Torres, Quintos, et al., 2002 | Martínez-Herrera, Robledo-Quintos, et al., 2001 | Greinwald, Bachmann, et al., 1995 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Beuerle, 2010
Beuerle, T.,
MS and RI data. Personal communication., 2010. [all data]
Przybylak, Ciesiolka, et al., 2005
Przybylak, J.K.; Ciesiolka, D.; Wysocka, W.; García-López, P.M.; Ruiz-López, M.A.; Wysocki, W.; Gulewicz, K.,
Alkaloid profiles of Mexican wild lupin and an effect of alkaloid preparation from Lupinus exaltatus seeds on growth and yield of paprika (Capsicum annuum L.),
Ind. Crops Prod., 2005, 21, 1, 1-7, https://doi.org/10.1016/j.indcrop.2003.12.001
. [all data]
Torres, Quintos, et al., 2002
Torres, K.B.; Quintos, N.R.; Necha, L.L.B.; Wink, M.,
Alkaloid profile of leaves and seeds of Lupinus hintonii C.P. Smith,
Z. Naturforsch., 2002, 57c, 243-247. [all data]
Martínez-Herrera, Robledo-Quintos, et al., 2001
Martínez-Herrera, J.; Robledo-Quintos, N.; Mora-Escobedo, R.; Dávila-Ortiz, G.,
Alkaloid composition of Lupinus campestris from Mexico,
J. Food Biochem., 2001, 25, 2, 117-125, https://doi.org/10.1111/j.1745-4514.2001.tb00728.x
. [all data]
Greinwald, Bachmann, et al., 1995
Greinwald, R.; Bachmann, P.; Lewis, G.; Witte, L.; Czygan, F.-C.,
Alkaloids of the genus Poecilanthe (Leguminosae: Papilionoideae),
Biochem. Syst. Ecol., 1995, 23, 5, 547-553, https://doi.org/10.1016/0305-1978(95)00050-5
. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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