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5-Methylhentriacontane


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHT-53145.Goh S.H., Ooi K.E., et al., 199325. m/0.53 mm/0.22 «mu»m, N2, 15. K/min, 320. C @ 20. min; Tstart: 150. C
CapillaryHT-53144.Goh S.H., Ooi K.E., et al., 199325. m/0.53 mm/0.22 «mu»m, N2, 15. K/min, 320. C @ 20. min; Tstart: 150. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-13150.Bernier, Carlson, et al., 199830. m/0.32 mm/0.25 «mu»m; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-53152.Juárez, Blomquist, et al., 2001He, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 200. C; Tend: 280. C
CapillaryDB-13150.Katritzky, Chen, et al., 200030. m/0.32 mm/0.25 «mu»m; Tstart: 60. C; Tend: 320. C
PackedOV-1013145.Nelson, de Renobales, et al., 1989Helium, Gas-Chrom Q (100-120 mesh), 3. K/min, 320. C @ 25. min; Column length: 3. m; Tstart: 150. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryPolydimethyl siloxane3150.Junkes, Castanho, et al., 2003Program: not specified
CapillaryHP-53149.Juárez, Carlson, et al., 2002H2; Column length: 30. m; Column diameter: 0.32 mm; Program: 60C (2min) => 20C/min => 180C => 3C/min => 310 C (10min)
CapillaryHP-53150.Juárez, Carlson, et al., 2002H2; Column length: 30. m; Column diameter: 0.32 mm; Program: 60C (2min) => 20C/min => 180C => 3C/min => 310 C (10min)
CapillaryDB-13150.Carlson, Geden, et al., 199930. m/0.32 mm/0.25 «mu»m, He; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C (12 - 42 min)

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Goh S.H., Ooi K.E., et al., 1993
Goh S.H.; Ooi K.E.; Chuah C.H.; Yong H.S.; Khoo S.G.; Ong S.H., Cuticular hydrocarbons from two species of Malaysian Bactrocera fruit flies, Biochem. Syst. Ecol., 1993, 21, 2, 215-226, https://doi.org/10.1016/0305-1978(93)90039-T . [all data]

Bernier, Carlson, et al., 1998
Bernier, U.R.; Carlson, D.A.; Geden, C.J., Gas chromatography/mass spectrometry analysis of the cuticular hydrocarbons from parasitic wasps of the genus Muscidifurax, J. Am. Soc. Mass Spectrom., 1998, 9, 4, 320-332, https://doi.org/10.1016/S1044-0305(97)00288-2 . [all data]

Juárez, Blomquist, et al., 2001
Juárez, P.; Blomquist, G.J.; Schofield, C.J., Hydrocarbons of Rhodnius prolixus, a Chagas disease vector, Comp. Biochem. Physiol. B: Comp. Biochem., 2001, 129, 4, 733-746, https://doi.org/10.1016/S1096-4959(01)00380-3 . [all data]

Katritzky, Chen, et al., 2000
Katritzky, A.R.; Chen, K.; Maran, U.; Carlson, D.A., QSPR Correlation and predictions of GC retention indexes for methyl-branched hydrocarbons produced by insects, Anal. Chem., 2000, 72, 1, 101-109, https://doi.org/10.1021/ac990800w . [all data]

Nelson, de Renobales, et al., 1989
Nelson, D.R.; de Renobales, M.; Dwyer, L.A.; Zamboni, A.C.; Fatland, C.L.; Blomquist, G.J., Novel very long-chain methyl branched alcohols and their esters, and methyl branched alkanes in pupae of the gabbage looper, Trichoplusa ni (Hubner), Insect Biochem., 1989, 19, 2, 197-208, https://doi.org/10.1016/0020-1790(89)90092-9 . [all data]

Junkes, Castanho, et al., 2003
Junkes, B.S.; Castanho, R.D.M.; Amboni, C.; Yunes, R.A.; Heinzen, V.E.F., Semiempirical Topological Index: A Novel Molecular Descriptor for Quantitative Structure-Retention Relationship Studies, Internet Electronic Journal of Molecular Design, 2003, 2, 1, 33-49. [all data]

Juárez, Carlson, et al., 2002
Juárez, M.P.; Carlson, D.A.; Schettino, P.M.S.; Mijailovsky, S.; Rojas, G., Cuticular hydrocarbons of Chagas disease vectors in Mexico, Mem. Inst. Oswaldo Cruz., 2002, 97, 6, 819-827, https://doi.org/10.1590/S0074-02762002000600012 . [all data]

Carlson, Geden, et al., 1999
Carlson, D.A.; Geden, C.J.; Bernier, U.R., Identification of pupal exiviae of Nasania vitripennis and Muscidifurax raptorellus parasitoids using cuticular hydrocarbons, Biol. Control, 1999, 15, 2, 97-106, https://doi.org/10.1006/bcon.1999.0708 . [all data]


Notes

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