Home Symbol which looks like a small house Up Solid circle with an upward pointer in it

epi-Bicyclosesquiphellandrene


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5SE-30HP-5SPB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.260.250.250.25
Tstart (C) 50.60.40.40.50.
Tend (C) 280.240.250.250.250.
Heat rate (K/min) 4.4.5.5.2.
Initial hold (min)  2.5.5. 
Final hold (min)  20.10.10. 
I 1452.1430.1495.1491.1434.
ReferenceZhao, Zeng, et al., 2009Farsam, Amanlou, et al., 2007Loizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Raal, Orav, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 8 CBDB-1Methyl SiliconeDB-1
Column length (m) 30.30.50.12.530.
Carrier gas HeliumHeHeHeN2
Substrate      
Column diameter (mm) 0.320.250.220.250.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 60.80.70.50.50.
Tend (C) 260.200.220.270.200.
Heat rate (K/min) 5.3.4.4.5.
Initial hold (min) 2.5.   
Final hold (min) 13.5.   
I 1430.1494.1452.1431.1458.
ReferenceKucuk, Gulec, et al., 2006Facey, Porter, et al., 2005Palá-Paúl, García-Jiménez, et al., 2004Curini, Bianchi, et al., 2003Fekam Boyom, Ngouana, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5SE-30HP-1
Column length (m) 30.30.30.50.60.
Carrier gas HeH2H2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.70.60.
Tend (C) 250.280.280.240.200.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min)  10.10. 5.
Final hold (min)  40.40. 25.
I 1492.1490.1490.1430.1493.
ReferenceLimberger, Simões-Pires, et al., 2003Pino, Marbot, et al., 2003Pino, Marbot, et al., 2003Iñigo, Palá-Paúl, et al., 2002Meccia, Rojas, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-30
Column length (m) 30.
Carrier gas Helium
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum) 0.20
Tstart (C) 60.
Tend (C) 200.
Heat rate (K/min) 3.
Initial hold (min) 4.
Final hold (min)  
I 1478.
ReferencePrikhod'ko, Klyuev, et al., 1999
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Farsam, Amanlou, et al., 2007
Farsam, H.; Amanlou, M.; Taghi-Cheetsaz, N.; Amin, G.R.; Saledi-Sormaghi, M.H., Essential Oil of Chimonanthus fragrans flowers Population of Tehran, DARU, 2007, 15, 3, 129-131. [all data]

Loizzo, Tundis, et al., 2007
Loizzo, M.R.; Tundis, R.; Conforti, F.; Saab, A.M.; Statti, G.A.; Menichini, F., Comparative chemical composition, antioxidant and hypoglycaemic activities of Juniperus oxycedrus ssp. oxycedrus L. berry and wood oils from Lebanon, Food Chem., 2007, 105, 2, 572-578, https://doi.org/10.1016/j.foodchem.2007.04.015 . [all data]

Raal, Orav, et al., 2007
Raal, A.; Orav, A.; Arak, E.; Kailas, T.; Müürisepp, M., Variation in the composition of the essential oil of Valeriana officinalis L. roots from Estonia, Proc. Est. Acad. Sci. Chem., 2007, 56, 2, 67-74. [all data]

Kucuk, Gulec, et al., 2006
Kucuk, M.; Gulec, C.; Yasar, A.; Ucuncu, O.; Yayh, N.; Coskuncelebi, K.; Terzioglu, S.; Yayh, N., Chemical composition and antimicrobial activities of the essential oils of Teucrium chamaedrys subsp. chamaedrys, T. orientale var. puberulens, and T. chamaedrys subsp. lydium, Pharm. Biol., 2006, 44, 8, 592-599, https://doi.org/10.1080/13880200600896868 . [all data]

Facey, Porter, et al., 2005
Facey, P.C.; Porter, R.B.R.; Reese, P.B.; Williams, L.A.D., Biological activity and chemical composition of the essential oil from Jamaican Hyptis verticillata Jacq., J. Agric. Food Chem., 2005, 53, 12, 4774-4777, https://doi.org/10.1021/jf050008y . [all data]

Palá-Paúl, García-Jiménez, et al., 2004
Palá-Paúl, J.; García-Jiménez, R.; Pérez-Alonso, M.J.; Velasco-Negueruela, A.; Sanz, J., Essential oil composition of the leaves and stems of Meum athamanticum Jacq., from Spain, J. Chromatogr. A, 2004, 1036, 2, 245-247, https://doi.org/10.1016/j.chroma.2004.02.064 . [all data]

Curini, Bianchi, et al., 2003
Curini, M.; Bianchi, A.; Epifano, F.; Bruni, R.; Torta, L.; Zambonelli, A., Composition and in vitro antifungal activity of essential oils of Erigeron canadensis and Myrtus communis from France, Chem. Nat. Compd. (Engl. Transl.), 2003, 39, 2, 191-194, https://doi.org/10.1023/A:1024818015122 . [all data]

Fekam Boyom, Ngouana, et al., 2003
Fekam Boyom, F.; Ngouana, V.; Amvam Zollo, P.H.; Menut, C.; Bessiere, J.M.; Gut, J.; Rosenthal, P.J., Composition and anti-plasmodial activities of essential oils from some Cameroonian medicinal plants, Phytochemistry, 2003, 64, 7, 1269-1275, https://doi.org/10.1016/j.phytochem.2003.08.004 . [all data]

Limberger, Simões-Pires, et al., 2003
Limberger, R.P.; Simões-Pires, C.A.; Sobral, M.; Menut, C.; Bessiere, J.-M.; Henriques, A.T., Essential oils of six Gomidesia spp. from southern Brazil, Flavour Fragr. J., 2003, 18, 2, 144-147, https://doi.org/10.1002/ffj.1122 . [all data]

Pino, Marbot, et al., 2003
Pino, J.A.; Marbot, R.; Fuentes, V., Characterization of volatiles in Bullock's heart (Annona reticulata L.) fruit cultivars from Cuba, J. Agric. Food Chem., 2003, 51, 13, 3836-3839, https://doi.org/10.1021/jf020733y . [all data]

Iñigo, Palá-Paúl, et al., 2002
Iñigo, A.; Palá-Paúl, J.; Pérez-Alonso, M.J.; Velasco-Negueruela, A., Essential oil composition from the aerial parts of Haplophyllum linifolium (L.) G. Don fil., Botanica Complutensis, 2002, 26, 79-83. [all data]

Meccia, Rojas, et al., 2000
Meccia, G.; Rojas, L.B.; Rosquete, C.; Feliciano, A.S., Essential oil of Croton ovalifolius Vahl from Venezuela, Flavour Fragr. J., 2000, 15, 3, 144-146, https://doi.org/10.1002/1099-1026(200005/06)15:3<144::AID-FFJ882>3.0.CO;2-C . [all data]

Prikhod'ko, Klyuev, et al., 1999
Prikhod'ko, A.B.; Klyuev, N.A.; Volkovich, S.V.; Emets, T.I.; Petrenko, V.V.; Dolya, E.V., Component composition od the essential oil of Thymus dimorphus, Chem. Nat. Comp., 1999, 35, 1, 46-51, https://doi.org/10.1007/BF02238208 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References