epi-Bicyclosesquiphellandrene
- Formula: C15H24
- Molecular weight: 204.3511
- IUPAC Standard InChI: InChI=1S/C15H24/c1-10(2)13-8-6-12(4)14-7-5-11(3)9-15(13)14/h9-10,12-14H,3,5-8H2,1-2,4H3/t12-,13+,14?/m1/s1
- IUPAC Standard InChIKey: RNDFUOKDULDZPR-AMIUJLCOSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Species with the same structure:
- Stereoisomers:
- Information on this page:
- Other data available:
- Options:
Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-5 MS | HP-5 | SE-30 | HP-5 | SPB-5 |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | Helium | Helium | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.26 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 50. | 60. | 40. | 40. | 50. |
| Tend (C) | 280. | 240. | 250. | 250. | 250. |
| Heat rate (K/min) | 4. | 4. | 5. | 5. | 2. |
| Initial hold (min) | 2. | 5. | 5. | ||
| Final hold (min) | 20. | 10. | 10. | ||
| I | 1452. | 1430. | 1495. | 1491. | 1434. |
| Reference | Zhao, Zeng, et al., 2009 | Farsam, Amanlou, et al., 2007 | Loizzo, Tundis, et al., 2007 | Loizzo, Tundis, et al., 2007 | Raal, Orav, et al., 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-5 | CP Sil 8 CB | DB-1 | Methyl Silicone | DB-1 |
| Column length (m) | 30. | 30. | 50. | 12.5 | 30. |
| Carrier gas | Helium | He | He | He | N2 |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.25 | 0.22 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 60. | 80. | 70. | 50. | 50. |
| Tend (C) | 260. | 200. | 220. | 270. | 200. |
| Heat rate (K/min) | 5. | 3. | 4. | 4. | 5. |
| Initial hold (min) | 2. | 5. | |||
| Final hold (min) | 13. | 5. | |||
| I | 1430. | 1494. | 1452. | 1431. | 1458. |
| Reference | Kucuk, Gulec, et al., 2006 | Facey, Porter, et al., 2005 | Palá-Paúl, García-Jiménez, et al., 2004 | Curini, Bianchi, et al., 2003 | Fekam Boyom, Ngouana, et al., 2003 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-5 | DB-5 | DB-5 | SE-30 | HP-1 |
| Column length (m) | 30. | 30. | 30. | 50. | 60. |
| Carrier gas | He | H2 | H2 | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 60. | 60. | 60. | 70. | 60. |
| Tend (C) | 250. | 280. | 280. | 240. | 200. |
| Heat rate (K/min) | 3. | 4. | 4. | 4. | 4. |
| Initial hold (min) | 10. | 10. | 5. | ||
| Final hold (min) | 40. | 40. | 25. | ||
| I | 1492. | 1490. | 1490. | 1430. | 1493. |
| Reference | Limberger, Simões-Pires, et al., 2003 | Pino, Marbot, et al., 2003 | Pino, Marbot, et al., 2003 | Iñigo, Palá-Paúl, et al., 2002 | Meccia, Rojas, et al., 2000 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary |
|---|---|
| Active phase | SE-30 |
| Column length (m) | 30. |
| Carrier gas | Helium |
| Substrate | |
| Column diameter (mm) | 0.25 |
| Phase thickness (μm) | 0.20 |
| Tstart (C) | 60. |
| Tend (C) | 200. |
| Heat rate (K/min) | 3. |
| Initial hold (min) | 4. |
| Final hold (min) | |
| I | 1478. |
| Reference | Prikhod'ko, Klyuev, et al., 1999 |
| Comment | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T.,
Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods,
J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484
. [all data]
Farsam, Amanlou, et al., 2007
Farsam, H.; Amanlou, M.; Taghi-Cheetsaz, N.; Amin, G.R.; Saledi-Sormaghi, M.H.,
Essential Oil of Chimonanthus fragrans flowers Population of Tehran,
DARU, 2007, 15, 3, 129-131. [all data]
Loizzo, Tundis, et al., 2007
Loizzo, M.R.; Tundis, R.; Conforti, F.; Saab, A.M.; Statti, G.A.; Menichini, F.,
Comparative chemical composition, antioxidant and hypoglycaemic activities of Juniperus oxycedrus ssp. oxycedrus L. berry and wood oils from Lebanon,
Food Chem., 2007, 105, 2, 572-578, https://doi.org/10.1016/j.foodchem.2007.04.015
. [all data]
Raal, Orav, et al., 2007
Raal, A.; Orav, A.; Arak, E.; Kailas, T.; Müürisepp, M.,
Variation in the composition of the essential oil of Valeriana officinalis L. roots from Estonia,
Proc. Est. Acad. Sci. Chem., 2007, 56, 2, 67-74. [all data]
Kucuk, Gulec, et al., 2006
Kucuk, M.; Gulec, C.; Yasar, A.; Ucuncu, O.; Yayh, N.; Coskuncelebi, K.; Terzioglu, S.; Yayh, N.,
Chemical composition and antimicrobial activities of the essential oils of Teucrium chamaedrys subsp. chamaedrys, T. orientale var. puberulens, and T. chamaedrys subsp. lydium,
Pharm. Biol., 2006, 44, 8, 592-599, https://doi.org/10.1080/13880200600896868
. [all data]
Facey, Porter, et al., 2005
Facey, P.C.; Porter, R.B.R.; Reese, P.B.; Williams, L.A.D.,
Biological activity and chemical composition of the essential oil from Jamaican Hyptis verticillata Jacq.,
J. Agric. Food Chem., 2005, 53, 12, 4774-4777, https://doi.org/10.1021/jf050008y
. [all data]
Palá-Paúl, García-Jiménez, et al., 2004
Palá-Paúl, J.; García-Jiménez, R.; Pérez-Alonso, M.J.; Velasco-Negueruela, A.; Sanz, J.,
Essential oil composition of the leaves and stems of Meum athamanticum Jacq., from Spain,
J. Chromatogr. A, 2004, 1036, 2, 245-247, https://doi.org/10.1016/j.chroma.2004.02.064
. [all data]
Curini, Bianchi, et al., 2003
Curini, M.; Bianchi, A.; Epifano, F.; Bruni, R.; Torta, L.; Zambonelli, A.,
Composition and in vitro antifungal activity of essential oils of Erigeron canadensis and Myrtus communis from France,
Chem. Nat. Compd. (Engl. Transl.), 2003, 39, 2, 191-194, https://doi.org/10.1023/A:1024818015122
. [all data]
Fekam Boyom, Ngouana, et al., 2003
Fekam Boyom, F.; Ngouana, V.; Amvam Zollo, P.H.; Menut, C.; Bessiere, J.M.; Gut, J.; Rosenthal, P.J.,
Composition and anti-plasmodial activities of essential oils from some Cameroonian medicinal plants,
Phytochemistry, 2003, 64, 7, 1269-1275, https://doi.org/10.1016/j.phytochem.2003.08.004
. [all data]
Limberger, Simões-Pires, et al., 2003
Limberger, R.P.; Simões-Pires, C.A.; Sobral, M.; Menut, C.; Bessiere, J.-M.; Henriques, A.T.,
Essential oils of six Gomidesia spp. from southern Brazil,
Flavour Fragr. J., 2003, 18, 2, 144-147, https://doi.org/10.1002/ffj.1122
. [all data]
Pino, Marbot, et al., 2003
Pino, J.A.; Marbot, R.; Fuentes, V.,
Characterization of volatiles in Bullock's heart (Annona reticulata L.) fruit cultivars from Cuba,
J. Agric. Food Chem., 2003, 51, 13, 3836-3839, https://doi.org/10.1021/jf020733y
. [all data]
Iñigo, Palá-Paúl, et al., 2002
Iñigo, A.; Palá-Paúl, J.; Pérez-Alonso, M.J.; Velasco-Negueruela, A.,
Essential oil composition from the aerial parts of Haplophyllum linifolium (L.) G. Don fil.,
Botanica Complutensis, 2002, 26, 79-83. [all data]
Meccia, Rojas, et al., 2000
Meccia, G.; Rojas, L.B.; Rosquete, C.; Feliciano, A.S.,
Essential oil of Croton ovalifolius Vahl from Venezuela,
Flavour Fragr. J., 2000, 15, 3, 144-146, https://doi.org/10.1002/1099-1026(200005/06)15:3<144::AID-FFJ882>3.0.CO;2-C
. [all data]
Prikhod'ko, Klyuev, et al., 1999
Prikhod'ko, A.B.; Klyuev, N.A.; Volkovich, S.V.; Emets, T.I.; Petrenko, V.V.; Dolya, E.V.,
Component composition od the essential oil of Thymus dimorphus,
Chem. Nat. Comp., 1999, 35, 1, 46-51, https://doi.org/10.1007/BF02238208
. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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