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9-Angeloylretronecine


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-11797.El-Shazly, El-Domiaty, et al., 1998He, 6. K/min; Column length: 30. m; Tstart: 150. C; Tend: 300. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-11797.Weber, Eisenreich, et al., 1999He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 150. C; Tend: 300. C
CapillaryDB-11797.Witte, Rubiolo, et al., 1992He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 150. C; Tend: 300. C
CapillaryDB-51840.Witte, Rubiolo, et al., 1992He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 150. C; Tend: 300. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11795.Asres, Sporer, et al., 2004He; Column length: 30. m; Column diameter: 0.3 mm; Program: 120C => (6C/min or 1.5C/min) => 300C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

El-Shazly, El-Domiaty, et al., 1998
El-Shazly, A.; El-Domiaty, M.; Witte, L.; Wink, M., Pyrrolizidine alkaloids in members of the boraginaceae from Sinai (Egypt), Biochem. Syst. Ecol., 1998, 26, 6, 619-636, https://doi.org/10.1016/S0305-1978(98)00028-3 . [all data]

Weber, Eisenreich, et al., 1999
Weber, S.; Eisenreich, W.; Bacher, A.; Hartmann, T., Pyrrolizidine alkaloids of the lycopsamine type: biosynthesis of thracelanthic acid, Phytochemistry, 1999, 50, 6, 1005-1014, https://doi.org/10.1016/S0031-9422(98)00203-9 . [all data]

Witte, Rubiolo, et al., 1992
Witte, L.; Rubiolo, P.; Bicchi, C.; Hartmann, T., Comparative analysis of pyrrolizidine alkaloids from natural sources by gas chromatography-mass spectrometry, Phytochemistry, 1992, 32, 1, 187-196, https://doi.org/10.1016/0031-9422(92)80130-7 . [all data]

Asres, Sporer, et al., 2004
Asres, K.; Sporer, F.; Wink, M., Patterns of pyrrolizidine alkaloids in 12 Ethiopian Crotalaria species, Biochem. Syst. Ecol., 2004, 32, 10, 915-930, https://doi.org/10.1016/j.bse.2004.03.004 . [all data]


Notes

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