4-Pentenoic acid, 2-(1-oxopropyl), enol-bis-TMS, # 2


Van Den Dool and Kratz RI, non-polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase DB-1
Column length (m) 60.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum) 0.25
Program 40 0C "rapidly" -> 80 0C 2 0C/min -> 120 0C 4 0C/min -> 180 0C "rapidly" -> 250 0C
I 1435.
ReferenceRettenmeier, Howald, et al., 1989
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Rettenmeier, Howald, et al., 1989
Rettenmeier, A.W.; Howald, W.N.; Levy, R.H.; Witek, D.J.; Gordon, W.P.; Porubek, D.J.; Baillie, T.A., Quantitative metabolic profiling of valproic acid in humans using automated gas chromatographic/mass spectrometric techniques, Biomed. Environ. Mass Spectrom., 1989, 18, 3, 192-199, https://doi.org/10.1002/bms.1200180308 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, References