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13,17-Dimethylheptatriacontane


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryMethyl Silicone225.3752.Pomonis, Hakk, et al., 1989He; Column length: 12.5 m

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryUltra-13758.Nelson, Adams, et al., 2003150. C @ 4. min, 4. K/min, 320. C @ 30. min; Column length: 12. m; Column diameter: 0.2 mm

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-13755.Bernier, Carlson, et al., 199830. m/0.32 mm/0.25 «mu»m; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryUltra-13758.Nelson and Charlet, 2003He, 4. K/min; Column length: 12.5 m; Column diameter: 0.2 mm; Tstart: 150. C; Tend: 320. C
PackedOV-1013758.Nelson, de Renobales, et al., 1989Helium, Gas-Chrom Q (100-120 mesh), 3. K/min, 320. C @ 25. min; Column length: 3. m; Tstart: 150. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-13755.Carlson, Geden, et al., 199930. m/0.32 mm/0.25 «mu»m, He; Program: 60C (2min) => 10C/min => 220C => 3C/min => 310C (12 - 42 min)
CapillaryCP Sil 5 CB3758.Kenig, Sinninghe Damsté, et al., 199525. m/0.32 mm/0.2 «mu»m, He; Program: 50C => 20C/min => 130C => 4C/min => 300C (20min)

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pomonis, Hakk, et al., 1989
Pomonis, J.G.; Hakk, H.; Fatland, C.L., Synthetic methyl- and dimethylalkanes. Kovats indices [13C]NMR and mass spectra of some methylpentacosanes and 2,X-dimethylheptacosanes, J. Chem. Ecol., 1989, 15, 9, 2319-2333. [all data]

Nelson, Adams, et al., 2003
Nelson, D.R.; Adams, T.S.; Fatland, C.L., Hydrocarbons in the surface wax of eggs and adults of the Colorado potato beetle, Leptinotarsa decemlineata, Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 134, 3, 447-466, https://doi.org/10.1016/S1096-4959(02)00262-2 . [all data]

Bernier, Carlson, et al., 1998
Bernier, U.R.; Carlson, D.A.; Geden, C.J., Gas chromatography/mass spectrometry analysis of the cuticular hydrocarbons from parasitic wasps of the genus Muscidifurax, J. Am. Soc. Mass Spectrom., 1998, 9, 4, 320-332, https://doi.org/10.1016/S1044-0305(97)00288-2 . [all data]

Nelson and Charlet, 2003
Nelson, D.R.; Charlet, L.D., Cuticular hydrocarbons of the sunflower beetle,Zygogramma exclamationis, Comp. Biochem. Physiol. B: Comp. Biochem., 2003, 135, 2, 273-284, https://doi.org/10.1016/S1096-4959(03)00080-0 . [all data]

Nelson, de Renobales, et al., 1989
Nelson, D.R.; de Renobales, M.; Dwyer, L.A.; Zamboni, A.C.; Fatland, C.L.; Blomquist, G.J., Novel very long-chain methyl branched alcohols and their esters, and methyl branched alkanes in pupae of the gabbage looper, Trichoplusa ni (Hubner), Insect Biochem., 1989, 19, 2, 197-208, https://doi.org/10.1016/0020-1790(89)90092-9 . [all data]

Carlson, Geden, et al., 1999
Carlson, D.A.; Geden, C.J.; Bernier, U.R., Identification of pupal exiviae of Nasania vitripennis and Muscidifurax raptorellus parasitoids using cuticular hydrocarbons, Biol. Control, 1999, 15, 2, 97-106, https://doi.org/10.1006/bcon.1999.0708 . [all data]

Kenig, Sinninghe Damsté, et al., 1995
Kenig, F.; Sinninghe Damsté, J.S.; Kock-van Dalen, A.C.; Rijpstra, W.I.C.; Huc, A.Y.; de Leeuw, J.W., Occurrence and origin of mono-, di-, and trimethylalkanes in modern and holocene cyanobacterial mats from Abu Dhabi, United Arab Emirates, Geochim. Cosmochim. Acta, 1995, 59, 14, 2999-3015, https://doi.org/10.1016/0016-7037(95)00190-5 . [all data]


Notes

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