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Allo-pregnanediol, MO TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30221.2762.Mitra, 1982N2; Column length: 30. m; Column diameter: 0.25 mm
CapillarySE-30231.2776.Mitra, 1982N2; Column length: 30. m; Column diameter: 0.25 mm
CapillarySE-30241.2791.Mitra, 1982N2; Column length: 30. m; Column diameter: 0.25 mm

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryZB-12803.Ebner, Corol, et al., 200630. m/0.25 mm/0.25 «mu»m, He; Program: 70C(5min) => 20C/min => 220C(0.33min) => 5C/min => 315C (4min)

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-12785.Hähnel, Wilkinson, et al., 1985He; Column length: 25. m; Column diameter: 0.3 mm; Program: 40C (1min) => 20C/min => 200C => 2C/min => 300C (11min)

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Mitra, 1982
Mitra, G.D., Determination of precise retention indices of steroids using an all-glass solid injection system, J. Chromatogr., 1982, 234, 1, 214-217, https://doi.org/10.1016/S0021-9673(00)81795-1 . [all data]

Ebner, Corol, et al., 2006
Ebner, M.J.; Corol, D.I.; Havlíková, H.; Honour, J.W.; Fry, J.P., Identification of neuroactive steroids and their precursors and metabolites in adult male rat brain, Endocrinology, 2006, 147, 1, 179-190, https://doi.org/10.1210/en.2005-1065 . [all data]

Hähnel, Wilkinson, et al., 1985
Hähnel, E.; Wilkinson, S.P.; Hähnel, R., Urinary steroid profiles in pregnancy by capillary column gas chromatography, Clin. Chim. Acta, 1985, 151, 3, 259-271, https://doi.org/10.1016/0009-8981(85)90089-0 . [all data]


Notes

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