3-Ketovaleric acid, oxime, TMS


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type PackedPacked
Active phase OV-1OV-1
Column length (m) 1.81.8
Carrier gas N2N2
Substrate 100-120 mesh100-120 mesh
Column diameter (mm)   
Phase thickness (μm)   
Tstart (C) 70.70.
Tend (C) 290.290.
Heat rate (K/min) 28.28.
Initial hold (min) 0.50.5
Final hold (min)   
I 1272.1286.
ReferenceTanaka, Hine, et al., 1980Tanaka, Hine, et al., 1980
Comment MSDC-RI MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Tanaka, Hine, et al., 1980
Tanaka, K.; Hine, D.G.; West-Dull, A.; Lynn, T.B., Gas-chromatographic method of analysis for urinary organic acids. I. Retention indices of 155 metabolically important compounds, Clin. Chem., 1980, 26, 13, 1839-1846. [all data]


Notes

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