Thymidine, 3',5'-bis(O-TMTBSi)
- Formula: C26H46N2O5Si2
- Molecular weight: 522.8248
- IUPAC Standard InChI: InChI=1S/C26H46N2O5Si2/c1-19-17-28(24(30)27-23(19)29)22-16-20(33-35(26(5,6)7)14-10-11-15-35)21(32-22)18-31-34(25(2,3)4)12-8-9-13-34/h17,20-22H,8-16,18H2,1-7H3,(H,27,29,30)/t20-,21+,22?/m0/s1
- IUPAC Standard InChIKey: GNVQMTMGCIFNFP-UGGDCYSXSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Thymidine, 3',5'-bis-O-cyclotetramethylene-tertbutylsilyl
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-1 | 260. | 3416. | Quilliam, Ogilvie, et al., 1980 | N2, Gas-Chrom Q |
| Packed | OV-1 | 260. | 3416. | Quilliam and Westmore, 1978 | Gas Chrom Q; Column length: 1. m |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Quilliam, Ogilvie, et al., 1980
Quilliam, M.A.; Ogilvie, K.K.; Sadana, K.L.; Westmore, J.B.,
Gas chromatographic retention data for silyl and acyl derivatives of nucleosides,
J. Chromatogr., 1980, 196, 3, 367-378, https://doi.org/10.1016/S0021-9673(00)84739-1
. [all data]
Quilliam and Westmore, 1978
Quilliam, M.A.; Westmore, J.B.,
Sterically crowded trialkylsilyl derivatives for chromatography and mass spectrometry of biologically-important compounds,
Anal. Chem., 1978, 50, 1, 59-68, https://doi.org/10.1021/ac50023a020
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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