γ-Terpinene

Formula: C₁₀H₁₆
Molecular weight: 136.2340
IUPAC Standard InChI: InChI=1S/C10H16/c1-8(2)10-6-4-9(3)5-7-10/h4,7-8H,5-6H2,1-3H3
IUPAC Standard InChIKey: YKFLAYDHMOASIY-UHFFFAOYSA-N
CAS Registry Number: 99-85-4
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Other names: 1,4-Cyclohexadiene, 1-methyl-4-(1-methylethyl)-; γ-Terpinen; p-Mentha-1,4-diene; Crithmene; Moslene; 1-methyl-4-(1-methylethyl)-1,4-cyclohexadiene; 1-Methyl-4-isopropyl-1,4-cyclohexadiene; 1-Methyl-4-isopropylcyclohexadiene-1,4; 1,4-p-Menthadiene; 1,4-Cyclohexadiene, 1-methyl-4-isopropyl-; 4-Isopropyl-1-methyl-1,4-cyclohexadiene; Terpinene, γ-; 1-Isopropyl-4-methyl-cyclohexa-1,4-diene; NSC 21448; 1-isopropyl-4-methyl-1,4-cyclohexadiene (γ-terpinene); γ-Terpinolene; Gamma-terpinene
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Normal alkane RI, non-polar column, temperature ramp

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Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	HP-1	RTX-1	RTX-1
Column length (m)	30.	60.	30.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	300.	250.	240.	230.	230.
Heat rate (K/min)	4.	3.	3.	2.	2.
Initial hold (min)	3.	1.
Final hold (min)	15.	20.		5.	5.
I	1061.	1060.	1044.	1051.	1051.
Reference	Bertuzzi, Tirillini, et al., 2013	Sardashti, Valizadeh, et al., 2013	Alizadeh and Shaabani, 2012	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Mega-5	HP-5 MS	HP-5 MS	Polydimethyl siloxane with 5 % Ph	HP-5
Column length (m)	25.	30.	30.	30.	25.
Carrier gas	Helium	Helium	Helium	Helium	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25		0.32
Phase thickness (μm)	0.25	0.25	0.25		0.52
T_start (C)	50.	40.	50.	80.	40.
T_end (C)	220.	250.	180.	200.	280.
Heat rate (K/min)	3.	3.	2.	5.	4.
Initial hold (min)	1.	1.
Final hold (min)	5.	3.		25.	10.
I	1061.	1062.	1059.	1058.	1054.
Reference	Dell'Agli, Sanna, et al., 2012	Jian-Yu, Zhu, et al., 2012	Phungpanya, Thongpoon, et al., 2012	Priya, Prathapan, et al., 2012	Velickovic, Ristic, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	RTX-1	HP-5 MS	CP-Sil 5 CB
Column length (m)	25.	25.	60.	30.	25.
Carrier gas	Hydrogen	Hydrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.32	0.22	0.25	0.25
Phase thickness (μm)	0.52	0.52	0.25	0.25	0.15
T_start (C)	40.	40.	60.	50.	50.
T_end (C)	280.	280.	230.	250.	220.
Heat rate (K/min)	4.	4.	2.	7.
Initial hold (min)				1.
Final hold (min)	10.	10.	45.	5.
I	1054.	1055.	1044.	1060.	1057.
Reference	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Yapi, Boti, et al., 2012	Zouari, Ayadi, et al., 2012	Ameen, Usman, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	CP-Sil 5 CB	DB-1	HP-5 MS
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	Helium	Helium	Hydrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15	0.25	0.25
T_start (C)	60.	40.	50.	40.	50.
T_end (C)	240.	250.	230.	210.	180.
Heat rate (K/min)	3.	3.	3.	5.	2.
Initial hold (min)		5.
Final hold (min)		20.
I	1060.	1083.	1057.	1064.	1050.
Reference	Bertoli, Lepnardi, et al., 2011	Cao, Li, et al., 2011	Esseien, Aboaba, et al., 2011	Fathi, Sahari, et al., 2011	Hammami, Kamoun, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	VF-5 MS	VF-5 MS	SE-30 MS	DB-1	CP-Sil 5 CB
Column length (m)	60.	60.	30.	50.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.26
T_start (C)	30.	30.	50.	60.	45.
T_end (C)	260.	260.	250.	250.	280.
Heat rate (K/min)	2.	2.	5.	8.	3.
Initial hold (min)			5.
Final hold (min)	28.	28.	10.		22.
I	1059.	1062.	1059.	1050.	1051.
Reference	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011	Menichini, Tundis, et al., 2011	Misharina T., 2011	Mothana, Hasson, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methylsiloxane + 5 % Ph-groups	RTX-5	HP-5	HP-5	ZB-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	230.	210.	280.	300.	290.
Heat rate (K/min)	7.	3.	5.	50.	5.
Initial hold (min)	2.		1.	5.
Final hold (min)	20.		1.	5.
I	1062.	1051.	1059.	1060.	1057.
Reference	Nadim, Malik, et al., 2011	Prasad, Moulekhi, et al., 2011	Tekaya-Karoui, Boughalleb, et al., 2011	Bi Kouame, Bedi, et al., 2010	Boix, Victorio, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5 MS	HP-5	DB-5 MS	DB-5 MS	RTx-1
Column length (m)	30.	30.	25.	25.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.252	0.30	0.30	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	290.	240.	240.	240.	230.
Heat rate (K/min)	5.	3.	3.	3.	2.
Initial hold (min)
Final hold (min)					35.
I	1061.	1056.	1058.	1058.	1051.
Reference	Boix, Victorio, et al., 2010	Cavar, Maksimovic, et al., 2010	Chalchat, Figueredo, et al., 2010	Chalchat, Figueredo, et al., 2010	Dib, Bendahou, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	70.	40.
T_end (C)	280.	265.	250.	290.	260.
Heat rate (K/min)	3.	2.5	2.	5.	4.
Initial hold (min)		1.
Final hold (min)		20.			5.
I	1055.	1053.	1060.	1062.	1058.
Reference	Georgiou, Koutsaviti, et al., 2010	Hajimahdipoor, Samadi, et al., 2010	Ho, Wang, et al., 2010	Lazarevic, Radulovic, et al., 2010	Miyazawa, Kawauchi, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Hydrogen	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	100.	70.	70.
T_end (C)	240.	240.	220.	290.	290.
Heat rate (K/min)	3.	4.	2.	5.	5.
Initial hold (min)	5.	2.
Final hold (min)		10.			10.
I	1056.	1058.	1056.	1062.	1059.
Reference	Monsef-Esfahani, Miri, et al., 2010	Pino, Marquez, et al., 2010	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Dordevic, et al., 2010	Radulovic, Dordevic, et al., 2010, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	SLB-5 MS	SLB-5 MS	DB-5	DB-1-MS
Column length (m)	30.	10.	10.	30.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.10	0.10	0.25	0.25
Phase thickness (μm)	0.25	0.10	0.10	0.25	0.25
T_start (C)	60.	50.	50.	40.	30.
T_end (C)	220.	250.	250.	240.	200.
Heat rate (K/min)	6.	10.	10.	3.	2.
Initial hold (min)	3.			1.	4.
Final hold (min)					35.
I	1055.	1059.	1065.	1034.	1049.
Reference	Safaei-Ghomi and Batooli, 2010	Scandinaro, Tranchida, et al., 2010	Scandinaro, Tranchida, et al., 2010	de Souza, Lopes, et al., 2010	Takeoka, Hobbs, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	DB-5	HP-5MS	SE-54
Column length (m)	25.	30.	30.	30.	30.
Carrier gas		Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	80.	40.	50.	60.
T_end (C)	230.	240.	250.	250.	260.
Heat rate (K/min)	3.	3.	10.	7.	2.
Initial hold (min)			1.	1.	5.
Final hold (min)		2.	3.	5.	999.
I	1057.	1055.	1060.	1064.	1059.
Reference	Usman, Zubair, et al., 2010	Vahirua-Lechat, Mitermite, et al., 2010	Yang, Zhang, et al., 2010	Zouari, Zouari, et al., 2010	Dayisoylu and Alma, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	ZB-5	SPB-5	SPB-5	DB-5
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.35	0.53	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.50	0.25
T_start (C)	60.	50.	60.	50.	50.
T_end (C)	250.	240.	230.	210.	250.
Heat rate (K/min)	2.	3.	4.	3.	5.
Initial hold (min)	8.			5.	2.
Final hold (min)	15.	1.	40.	45.
I	1063.	1031.	1062.	1065.	1060.
Reference	Farhat, Ginies, et al., 2009	Gardini, Beletti, et al., 2009	Gauvin-Bialecki and Marodon, 2009	Gilani, Shah, et al., 2009	Ho, Wang, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5MS	HP-5	RTX-1
Column length (m)	50.	30.	60.	25.	60.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.20	0.22
Phase thickness (μm)	0.32	0.25	0.25	0.33	0.25
T_start (C)	60.	50.	70.	60.	60.
T_end (C)	220.	250.	250.	240.	230.
Heat rate (K/min)	5.	5.	3.	3.	2.
Initial hold (min)	3.
Final hold (min)				7.	30.
I	1062.	1041.	1064.	1057.	1050.
Reference	Kazemi and Akhavani, 2009	Koba, Catherine, et al., 2009	Males, Plazibat, et al., 2009	Maridass, 2009	Museli, Pau, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5	DB-5	5 % Phenyl methyl siloxane	Mega 5 MS
Column length (m)	60.	30.	30.	60.	60.
Carrier gas	Helium	Helium	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	45.	40.	90.	40.
T_end (C)	230.	250.	250.	225.	240.
Heat rate (K/min)	2.	3.	3.	3.	3.
Initial hold (min)		3.	1.		2.
Final hold (min)	30.	5.	10.	3.
I	1051.	1060.	1052.	1062.	1051.
Reference	Museli, Pau, et al., 2009	Porto, Decorti, et al., 2009	Rahmi-Nasrabadi, Gholivand, et al., 2009	Retta, Gattuso, et al., 2009	Romeo, Verzera, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1 MS	DB-5	DB-5	HP-5MS
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	Nitrogen	Helium	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	40.	40.	60.	40.	50.
T_end (C)	230.	250.	220.	240.	240.
Heat rate (K/min)	2.	6.	5.	3.	5.
Initial hold (min)		1.	3.	1.
Final hold (min)		4.	5.
I	1063.	1050.	1062.	1034.	1062.
Reference	Scrivanti, Anton, et al., 2009	Seo, Kim, et al., 2009	Shafaghat and Sadeghi, 2009	de Souza, Lopes, et al., 2009	Wannes, Mhamdi, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5 MS	HP-5	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium		N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	50.	50.	60.	60.
T_end (C)	325.	280.	280.	280.	220.
Heat rate (K/min)	10.	4.	9.	3.	5.
Initial hold (min)	6.		3.		10.
Final hold (min)	10.		3.
I	1057.	1058.	1062.	1056.	1063.
Reference	Zaibunnisa, Norashikin, et al., 2009	Zhao, Zeng, et al., 2009	Aicha, Ines, et al., 2008	Baziou, Couladis, et al., 2008	Flamini, Tebano, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	SLB-5 MS	ZB-1	DB-5	DB-5 MS
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	Helium	Helium	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	45.	60.	50.
T_end (C)	300.	250.	230.	250.	300.
Heat rate (K/min)	3.	3.	3.	5.	5.
Initial hold (min)		2.			5.
Final hold (min)	30.	10.		10.	5.
I	1058.	1058.	1043.	1064.	1054.
Reference	Isidorov, Lech, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008	Mosayebi, Amin, et al., 2008	Noudogbessi, Yedomonhan, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	RTX-5	HP-5	OV-1	HP-5
Column length (m)	7.5	20.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.10	0.18	0.25	0.25	0.25
Phase thickness (μm)	10.	0.20	0.25	0.25	0.32
T_start (C)	60.	50.	60.	65.	60.
T_end (C)	240.	280.	240.	260.	250.
Heat rate (K/min)	3.	4.	4.	6.	5.
Initial hold (min)		1.	2.		30.
Final hold (min)
I	1067.	1064.	1064.	1065.	1064.
Reference	Shellie, 2008	Skalicka-Wozniak, Los, et al., 2008	Verdian-rizi, 2008	Wang, Yi, et al., 2008	Yassa and Akhani, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5	HP-5 MS	CP Sil 5 CB	HP-5MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	N2	He
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	230.	220.	200.	300.	280.
Heat rate (K/min)	3.	5.	4.	4.	3.
Initial hold (min)	10.	3.
Final hold (min)	10.	5.	20.
I	1062.	1057.	1058.	1048.	1055.
Reference	Adams, Beauchamp, et al., 2007	Amiri, 2007	Araque, Rojas, et al., 2007	Baran, von Reuss, et al., 2007	Basta, Tzakou, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-52	DB-5	HP-5MS	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	He	Helium	N2
Substrate
Column diameter (mm)	0.25	0.26	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	50.
T_end (C)	220.	240.	280.	280.	240.
Heat rate (K/min)	3.	3.	3.	4.	5.
Initial hold (min)	1.			5.	1.
Final hold (min)	5.				4.
I	1047.	1055.	1061.	1055.	1062.
Reference	Bicchi, Cordero, et al., 2007	Bos, Woerdenbag, et al., 2007	Bozin B., Mlmica-Dukic N., et al., 2007	Capetanos, Saroglou, et al., 2007	Cheraif, Ben Jannet, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	HP-5MS	ZP-5
Column length (m)	60.	30.	30.	30.	60.
Carrier gas	He	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.26	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.26	0.25	0.25
T_start (C)	40.	60.	60.	60.	40.
T_end (C)	220.	290.	240.	250.	260.
Heat rate (K/min)	3.	3.	4.	2.	6.
Initial hold (min)			2.	8.	7.
Final hold (min)			20.	15.	1.
I	1066.	1055.	1058.	1056.	1071.
Reference	Chyau, Tsai, et al., 2007	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007	Ferhat, Tigrine-Kordjani, et al., 2007	Füssel, Dötterl, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	Col-Elite 5MS	DBP-5	RTX-5 MS
Column length (m)	60.	30.	30.	25.	30.
Carrier gas	Nitrogen	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.22	0.25
T_start (C)	60.	60.	30.	40.	45.
T_end (C)	250.	210.	246.	250.	210.
Heat rate (K/min)	4.	30.	3.	3.	3.
Initial hold (min)	1.	3.		1.
Final hold (min)	10.			10.
I	1053.	1057.	1067.	1031.	1058.
Reference	Ghasempour, Shirinpour, et al., 2007	Ghasemi, Yamini, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Heravi and Sereshti, 2007	Hudaib and Aburjai, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SE-30	HP-5	DB-5MS	ZB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	60.	60.
T_end (C)	300.	250.	250.	280.	220.
Heat rate (K/min)	3.	5.	5.	3.	4.
Initial hold (min)		5.	5.		5.
Final hold (min)		10.	10.	30.	20.
I	1050.	1059.	1057.	1031.	1065.
Reference	Limberger, Scopel, et al., 2007	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007	Marongiu B., Piras A., et al., 2007	Mohottalage, Tabacchi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-1	SPB-1	SPB-5
Column length (m)	30.	25.	50.	30.	30.
Carrier gas	Helium	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.2	0.25
T_start (C)	50.	60.	95.	70.	50.
T_end (C)	260.	240.	240.	220.	250.
Heat rate (K/min)	2.5	3.	4.	3.	2.
Initial hold (min)	1.
Final hold (min)	20.			15.
I	1044.	1062.	1058.	1047.	1054.
Reference	Monser-Esfahani, Karamkhani, et al., 2007	Oliveira, Leitão, et al., 2007	Pala-Paul, Brophy, et al., 2007	Pinto, Salgueiro, et al., 2007	Raal, Orav, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	DB-1	HP-5 MS	DB-1	DB-1
Column length (m)	50.	60.	60.	60.	60.
Carrier gas	He	Nitrogen	Hydrogen		He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	300.	250.	260.	250.	250.
Heat rate (K/min)	4.	4.	4.	5.	5.
Initial hold (min)	1.	1.
Final hold (min)	10.	10.	20.
I	1068.	1053.	1052.	1066.	1050.
Reference	Rali, Wossa, et al., 2007	Reza, Ebrahim, et al., 2007	Rojas, Velasco, et al., 2007	Salehi, Asghari, et al., 2007	Salehi, Fakhari, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DBP-5	DB-5	DB-5	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.22	0.25	0.25	0.25
T_start (C)	50.	40.	60.	40.	40.
T_end (C)	240.	250.	320.	210.	250.
Heat rate (K/min)	4.	3.	10.	2.	2.
Initial hold (min)		1.
Final hold (min)		10.	4.	33.	33.
I	1058.	1031.	1062.	1066.	1066.
Reference	Sefidkon, Abbasi, et al., 2007	Sereshti and Samadi, 2007	Smelcerovic, Spiteller, et al., 2007	Sylvestre, Longtin, et al., 2007	Sylvestre, Pichette, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Elite-5MS	HP-5 MS	HP-5MS	HP-5 MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	Helium	He	Helium	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	40.
T_end (C)	280.	280.	280.	280.	250.
Heat rate (K/min)	4.	3.	3.	3.	3.
Initial hold (min)	5.				5.
Final hold (min)	10.				10.
I	1056.	1062.	1023.	1060.	1055.
Reference	Tava, Pecetti, et al., 2007	Tsokou, Georgopoulos, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	CP Sil 5 CB	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	N2	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25		0.25
Phase thickness (μm)	0.32	0.25	0.25		0.25
T_start (C)	60.	50.	50.	80.	50.
T_end (C)	250.	280.	280.	270.	265.
Heat rate (K/min)	5.	9.	9.	10.	2.5
Initial hold (min)	30.	3.	3.		1.
Final hold (min)		3.	3.		20.
I	1064.	1057.	1058.	1051.	1060.
Reference	Yassa and Akhani, 2007	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006	Ayoub, Al-Azizi, et al., 2006	Bazargani, Almasirad, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	ZB-5	AT-5	BP-1	HP-5MS
Column length (m)	50.	30.	60.	50.	30.
Carrier gas	N2		He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	250.	300.	200.	220.	280.
Heat rate (K/min)	2.	2.	4.	2.	3.
Initial hold (min)
Final hold (min)	20.		20.	20.
I	1050.	1060.	1063.	1045.	1060.
Reference	Berlioz, Cordella, et al., 2006	Biondi, Sari, et al., 2006	Borges, Rojas, et al., 2006	Boti, Muselli, et al., 2006	Bozin, Mimicá-Dukic, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-1	HP-1	SPB-1	DB-1
Column length (m)	50.	50.	50.	30.	60.
Carrier gas	He	He	He	Helium	Nitrogen
Substrate
Column diameter (mm)	0.2	0.2	0.2	0.20	0.25
Phase thickness (μm)	0.33	0.33	0.33	0.20
T_start (C)	60.	60.	60.	70.	40.
T_end (C)	250.	250.	250.	220.	200.
Heat rate (K/min)	2.	2.	2.	3.	2.
Initial hold (min)	4.	4.	4.		1.
Final hold (min)	30.	30.	30.	15.	9.
I	1043.	1048.	1049.	1046.	1049.
Reference	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006, 2	Cavaleiro, Pinto, et al., 2006	Chen, Sheu, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-5MS	DB-5	BP-1
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	He			Helium	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.26	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	246.	230.	280.	290.	220.
Heat rate (K/min)	3.	3.	4.	3.	2.
Initial hold (min)
Final hold (min)		15.			20.
I	1059.	1062.	1065.	1055.	1047.
Reference	Coronel, Cerda-Garcia-Rojas, et al., 2006	Damjanovic, Skala, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006	Fanciullino, Tomi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-5MS	HP-5	HP-1	DB-1
Column length (m)	50.	30.	30.	50.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	60.	50.	50.	60.	60.
T_end (C)	220.	250.	300.	250.	240.
Heat rate (K/min)	2.	2.	5.	2.	5.
Initial hold (min)			5.		2.
Final hold (min)	20.		5.	40.
I	1047.	1062.	1062.	1049.	1056.
Reference	Fanciullino, Tomi, et al., 2006	Farah, Afifi, et al., 2006	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	DB-1	DB-5
Column length (m)	30.	60.	30.	60.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	240.	240.	240.	250.	250.
Heat rate (K/min)	5.	5.	5.	5.	3.
Initial hold (min)	2.	2.	2.
Final hold (min)				10.	10.
I	1062.	1056.	1062.	1050.	1059.
Reference	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006	Hadian, Sonboli, et al., 2006	Havlik, Kokoska, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5	DB-5	CP Sil 5 CB	HP-5MS
Column length (m)	30.	30.	30.	25.	30.
Carrier gas		He	Helium		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	40.	60.	60.	50.	50.
T_end (C)	220.	240.	260.	230.	280.
Heat rate (K/min)	3.	4.	3.	3.	5.
Initial hold (min)					4.
Final hold (min)	3.				10.
I	1060.	1062.	1059.	1052.	1063.
Reference	Hymete, Rohloff, et al., 2006	Ibañez and Usubillaga, 2006	Javidnia, Miri, et al., 2006	Kasali, Ekundayo, et al., 2006	Kim, Abd El-Aty, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	Methyl Silicone	RTX-1	CP Sil 5 CB	DB-1
Column length (m)	30.	25.	30.	30.	60.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	90.	60.	60.	70.
T_end (C)	280.	220.	300.	300.	230.
Heat rate (K/min)	5.	7.	4.	5.	2.
Initial hold (min)	4.	2.		4.	2.
Final hold (min)	10.				20.
I	1064.	1048.	1047.	1049.	1053.
Reference	Kim, El-Aty, et al., 2006	Kitchlu, Bakshi, et al., 2006	Kula, Izydorczyk, et al., 2006	Kurowska and Galazka, 2006	Lan Phi N.T., Nishiyama C., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	5 % Phenyl methyl siloxane	BP-1	DB-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	N2	Helium	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.3	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	60.	70.	60.	60.
T_end (C)	200.	280.	220.	220.	220.
Heat rate (K/min)	5.	3.	4.	4.	4.
Initial hold (min)			2.		5.
Final hold (min)		30.	10.
I	1050.	1030.	1057.	1063.	1063.
Reference	Martin, Joseph, et al., 2006	Marongiu, Piras, et al., 2006	Moody, Gundidza, et al., 2006	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP-Sil 5 CB	NB-30	DB-5	SE-52
Column length (m)	30.	25.	30.	25.	50.
Carrier gas		Hydrogen	He	N2	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.15	0.25	0.15
T_start (C)	50.	50.	50.	50.	50.
T_end (C)	265.	230.	250.	200.	240.
Heat rate (K/min)	2.5	3.	2.	4.	3.
Initial hold (min)	0.5			3.
Final hold (min)
I	1054.	1052.	1050.	1055.	1062.
Reference	Nickavar B., Kamalinejad M., et al., 2006	Olawore, Usman, et al., 2006	Orav, Raal, et al., 2006	Ouamba, Ouabonzi, et al., 2006	Ozcan, Chalchat, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-5	DB-5	DB-5
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	N2	He	Hydrogen	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	60.	70.	70.	70.
T_end (C)	240.	220.	280.	280.	280.
Heat rate (K/min)	4.	5.	4.	4.	4.
Initial hold (min)		10.	4.	4.	4.
Final hold (min)
I	1053.	1060.	1061.	1062.	1061.
Reference	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Pintore G., Chessa M., et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	H2		He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	280.	240.	250.	200.	260.
Heat rate (K/min)	3.	3.	10.	2.	5.
Initial hold (min)			5.
Final hold (min)				60.
I	1023.	1062.	1060.	1061.	1058.
Reference	Pitarokili, Tzakou, et al., 2006	Potzernheim, Bizzo, et al., 2006	Robinson, 2006	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	DB-1	FSOT-RSL-200	DB-5	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He		Hydrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	70.	40.	50.	50.
T_end (C)	300.	230.	280.	240.	240.
Heat rate (K/min)	2.	2.	6.	4.	4.
Initial hold (min)		2.	5.
Final hold (min)		20.	5.
I	1060.	1054.	1059.	1059.	1057.
Reference	Sari M., Biondi D.M., et al., 2006	Sawamura, Onishi, et al., 2006	Schmidt, Jirovetz, et al., 2006	Sefidkon, Abbasi, et al., 2006	Sefidkon, Abbasi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5	DB-5	CP Sil 5 CB
Column length (m)	30.	60.	25.	30.	25.
Carrier gas	He	He	N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.20	0.25
Phase thickness (μm)	0.25		0.33	0.18
T_start (C)	40.	40.	30.	60.	50.
T_end (C)	240.	250.	280.	240.	230.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)
Final hold (min)
I	1061.	1048.	1063.	1059.	1057.
Reference	Sefidkon and Jamzad, 2006	Sefidkon, Jamzad, et al., 2006	Shafi, Jose, et al., 2006	Silva, Oliveira, et al., 2006	Tesso, Kubeczka, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	Methyl Silicone	SPB-5	DB-5	DB-1
Column length (m)	30.	25.	60.	30.	50.
Carrier gas	Helium	N2	He	N2	N2
Substrate
Column diameter (mm)	0.25	0.3	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.15	1.	0.25	0.25
T_start (C)	60.	50.	40.	60.	90.
T_end (C)	250.	210.	230.	240.	240.
Heat rate (K/min)	2.	2.	3.	4.	4.
Initial hold (min)	8.	5.	5.
Final hold (min)	15.		2.
I	1056.	1066.	1070.	1062.	1040.
Reference	Tigrine-Kordiani, Meklati, et al., 2006	Tonzibo, Coffy, et al., 2006	Tornambe, Cornu, et al., 2006	Trilles, Bombarda, et al., 2006	Velasco-Negueruela, Pérez-Alonso, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	SPB-1	SPB-1	DB-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	60.	50.	50.	40.	40.
T_end (C)	250.	220.	250.	250.	250.
Heat rate (K/min)	10.	4.	4.	4.	4.
Initial hold (min)	2.	1.	1.
Final hold (min)	10.	10.	10.
I	1065.	1047.	1043.	1037.	1051.
Reference	Wang, Yang, et al., 2006	Wong, Lim, et al., 2006	Wong, Sivasothy, et al., 2006	Yadegarinia, Gachkar, et al., 2006	Yadegarinia, Gachkar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	HP-1	DB-5	DB-1
Column length (m)	30.	30.	50.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.249	0.25
Phase thickness (μm)	0.25	0.25	0.5	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	210.	280.	250.	290.	250.
Heat rate (K/min)	3.	3.	2.	3.	3.
Initial hold (min)	5.				3.
Final hold (min)			60.
I	1060.	1053.	1050.	1055.	1056.
Reference	Askari and Sefidkon, 2005	Basta, Tzakou, et al., 2005	Bendimerad and Bendiab, 2005	Bos, Stojanova, et al., 2005	Cégiéla-Carlioz, Bessière, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	SPB-5	DB-1	HP-1	HP-5
Column length (m)	60.	60.	60.	50.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.3	0.32	0.25	0.2	0.25
Phase thickness (μm)		1.	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	50.
T_end (C)	240.	230.	250.	250.	300.
Heat rate (K/min)	3.	3.	5.	2.	5.
Initial hold (min)		5.		60.	5.
Final hold (min)					5.
I	1054.	1067.	1046.	1047.	1062.
Reference	Chalchat and Özcan, 2005	Cornu, Kondjoyan, et al., 2005	Fakhari, Salehi, et al., 2005	Fernandez, Lizzani-Cuvelier, et al., 2005	Figuérédo, Cabassu, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	RSL-200	DB-5	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	N2		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25			0.25
T_start (C)	60.	40.	60.	60.	30.
T_end (C)	250.	280.	240.	240.	260.
Heat rate (K/min)	5.	6.	3.	3.	2.
Initial hold (min)		2.			2.
Final hold (min)	10.	10.			28.
I	1055.	1055.	1064.	1064.	1056.0
Reference	Jassbi, Mehrdad, et al., 2005	Jirovetz, Buchbauer, et al., 2005	Khayyat and Karimi, 2005	Khayyat and Karimi, 2005	Leffingwell and Alford, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	CP Sil 5 CB	CP Sil 5 CB	HP-5
Column length (m)	30.	30.	25.	25.	30.
Carrier gas	He	He			He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15	0.15	0.25
T_start (C)	60.	60.	50.	50.	70.
T_end (C)	230.	220.	230.	230.	240.
Heat rate (K/min)	3.	4.	3.	3.	5.
Initial hold (min)		5.
Final hold (min)
I	1052.	1060.	1052.	1052.	1057.
Reference	Limberger, Sobral, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005	Ogunwande, Olawore, et al., 2005	Olawore, Ogunwande, et al., 2005	Oyedeji, Yani, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	RTX-5 MS	HP-5MS	SPB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	N2	He		He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	40.	95.	50.	60.	60.
T_end (C)	250.	240.	280.	280.	250.
Heat rate (K/min)	5.	4.	8.	3.	4.
Initial hold (min)	0.5		2.		2.
Final hold (min)	2.		2.		20.
I	1074.	1058.	1063.	1060.	1062.
Reference	Özel, Gögüs, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005	Pellati, Benvenuti, et al., 2005	Petrakis, Roussis, et al., 2005	Pino, Marbot, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB	DB-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.32	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	40.	60.
T_end (C)	250.	220.	220.	220.	200.
Heat rate (K/min)	5.	4.	4.	4.	2.
Initial hold (min)	3.	1.	1.	1.
Final hold (min)					80.
I	1062.	1060.	1060.	1060.	1065.
Reference	Pourmortazavi, Ghadiri, et al., 2005	Rohloff and Bones, 2005	Rohloff and Bones, 2005	Rohloff and Bones, 2005	Rout, Misra, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	HP-5MS	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	220.	280.	275.	280.
Heat rate (K/min)	5.	6.	4.	4.	4.
Initial hold (min)		3.
Final hold (min)
I	1062.	1067.	1060.	1057.	1058.
Reference	Saeidnia, Gohari, et al., 2005	Safaei-Ghomi, Bamoniri, et al., 2005	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005	Sajjadi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	HP-5MS	DB-5MS
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	220.	250.	240.	280.	240.
Heat rate (K/min)	3.	5.	4.	3.	3.
Initial hold (min)	4.			5.
Final hold (min)		10.
I	1058.	1053.	1061.	1063.	1062.
Reference	Salehi, Sefidkon, et al., 2005	Salehi, Sonboli, et al., 2005	Sefidkon and Jamzad, 2005	Setzer, Noletto, et al., 2005	da Silva, Andrade, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	RTX-1	RTX-1	DB-1
Column length (m)	30.	30.	60.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	230.	280.	250.	25.	250.
Heat rate (K/min)	3.	3.	5.	5.	5.
Initial hold (min)
Final hold (min)	20.		10.	10.	10.
I	1060.	1056.	1052.	1051.	1050.
Reference	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005	Sonboli A., Fakhari A.R., et al., 2005	Sonboli, Salehi, et al., 2005	Sonboli, Salehi, et al., 2005, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-5 MS	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.50	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	240.	285.	260.	280.	280.
Heat rate (K/min)	3.	4.3	3.	3.	3.
Initial hold (min)	3.
Final hold (min)			20.
I	1061.	1062.	1055.	1023.	1030.
Reference	Tepe B., Sokmen M., et al., 2005	Tesevic, Nikicevic, et al., 2005	Topçu, Barla, et al., 2005	Tzakou, Bazos, et al., 2005	Tzakou and Constantinidis, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5MS	SPB-1	CP Sil 5 CB
Column length (m)	50.	50.	30.	50.	30.
Carrier gas	N2			He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	90.	60.	40.	50.	50.
T_end (C)	240.	240.	220.	220.	200.
Heat rate (K/min)	4.	3.	3.	4.	5.
Initial hold (min)			5.	3.
Final hold (min)			10.	30.
I	1040.	1035.	1055.	1050.	1047.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2	Vichi, Riu-Aumatell, et al., 2005	Wong, Lee, et al., 2005	Agnaniet, Menut, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	SE-52	HP-1	RTX-1
Column length (m)	30.	50.	25.	50.	60.
Carrier gas	He		N2	N2	He
Substrate
Column diameter (mm)	0.25	0.22	0.32	0.2	0.22
Phase thickness (μm)	0.25	0.25	0.15	0.33	0.25
T_start (C)	90.	60.	45.	60.	60.
T_end (C)	220.	220.	200.	250.	230.
Heat rate (K/min)	7.	2.	3.	2.	2.
Initial hold (min)	2.		5.
Final hold (min)	5.	20.	30.	20.	45.
I	1049.	1048.	1065.	1043.	1049.
Reference	Agnihotri, Thappa, et al., 2004	Blanc, Muselli, et al., 2004	Cakir, Kordali, et al., 2004	Cavalli, Fernandez, et al., 2004	Cavalli, Tomi, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5 MS	HP-5MS	DB-1
Column length (m)	60.	30.	30.	30.	25.
Carrier gas	N2	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	60.	60.	60.
T_end (C)	230.	240.	275.	275.	180.
Heat rate (K/min)	2.	2.	4.	4.	3.
Initial hold (min)	2.				10.
Final hold (min)	20.				10.
I	1022.	1060.	1063.	1058.	1062.
Reference	Choi, 2004	Cicció, 2004	Ghannadi, Sajjadi, et al., 2004	Hajhashemi V., Ghannadi A., et al., 2004	bin Jantan, Ayop, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	RTX-1	SE-54	HP-5MS
Column length (m)	25.	60.	30.	30.	30.
Carrier gas	Nitrogen	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	50.
T_end (C)	240.	280.	300.	260.	230.
Heat rate (K/min)	3.	4.	4.	2.	5.
Initial hold (min)		4.		5.	2.
Final hold (min)					10.
I	1061.	1059.	1053.	1059.	1055.
Reference	JAvidnia, Mojab, et al., 2004	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004	Li and Jiang, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5MS	HP-5MS	NB-30	NB-30
Column length (m)	30.	30.	30.	50.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	280.	280.	275.	250.	250.
Heat rate (K/min)	3.	3.	4.	2.	2.
Initial hold (min)
Final hold (min)		30.
I	1058.	1027.	1062.	1051.	1051.
Reference	Malencic, Couladis, et al., 2004	Marongiu, Piras, et al., 2004	Mehrabani, Asadipour, et al., 2004	Orav, Stulova, et al., 2004	Orav, Stulova, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	NB-30	NB-30	DB-5
Column length (m)	50.	50.	50.	50.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.2	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	95.	50.	50.	35.
T_end (C)	220.	240.	250.	250.	220.
Heat rate (K/min)	4.	4.	2.	2.	2.5
Initial hold (min)
Final hold (min)					6.
I	1050.	1050.	1050.	1050.	1060.
Reference	Palá-Paúl, García-Jiménez, et al., 2004	Palá-Paúl, Velasco-Negueruela, et al., 2004	Raal, Arak, et al., 2004	Raal, Paaver, et al., 2004	Rohloff, Mordal, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	HP-5 MS	HP-5MS	HP-5MS	DB-1
Column length (m)	60.	30.	30.	30.	60.
Carrier gas	He	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	70.
T_end (C)	200.	200.	280.	280.	230.
Heat rate (K/min)	4.	4.	4.	4.	2.
Initial hold (min)	1.	1.			2.
Final hold (min)	20.	20.			20.
I	1053.	1053.	1056.	1061.	1022.
Reference	Rojas, Usubillaga, et al., 2004	Royas, Usubillaga, et al., 2004	Sadeghpour, Asghari, et al., 2004	Sajjadi and Shahpiri, 2004	Sawamura, Son, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-1	HP-1	HP-5
Column length (m)	60.	30.	60.	30.	25.
Carrier gas	Nitrogen		He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.5
T_start (C)	70.	50.	40.	40.	30.
T_end (C)	230.	250.	280.	260.	280.
Heat rate (K/min)	2.	3.	4.	2.	3.
Initial hold (min)	2.	5.	5.	5.
Final hold (min)				20.
I	1022.	1061.	1050.	1049.	1063.
Reference	Sawamura, Sou, et al., 2004	Sefidkon, Jamzad, et al., 2004	Sefidkon and Shaabani, 2004	Senatore, Napolitano, et al., 2004	Shafi, Nambiar, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	DB-5	BPX-5	CP Sil 8 CB
Column length (m)	30.	20.	30.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	1.	0.25
T_start (C)	60.	100.	60.	60.	50.
T_end (C)	240.	270.	300.	250.	200.
Heat rate (K/min)	3.	8.	3.	3.	10.
Initial hold (min)		2.		5.	3.
Final hold (min)				10.	2.
I	1060.	1047.	1060.	1069.	1055.
Reference	Tellez, Khan, et al., 2004	Thappa, Bakshi, et al., 2004	Tirillini, Pellegrino, et al., 2004	Vilaseca, Guy, et al., 2004	Wang and Guo-Y. -L., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 8 CB	DB-5	HP-5MS	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	He	N2	He
Substrate
Column diameter (mm)	0.32	0.249	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	200.	300.	275.	220.	240.
Heat rate (K/min)	5.	3.	4.	5.	4.
Initial hold (min)	5.			10.
Final hold (min)
I	1062.	1055.	1061.	1057.	1055.
Reference	Wang, Guo, et al., 2004	Woerdenbag, Windono, et al., 2004	Afsharypuor and Jahromy, 2003	Bertoli, Menichini, et al., 2003	Cabanillas, Lopez, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	DB-1	DB-1	RTX-5Sil
Column length (m)	60.	30.	60.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25			0.25
T_start (C)	70.	60.	50.	50.	70.
T_end (C)	230.	280.	250.	250.	200.
Heat rate (K/min)	2.	3.	4.	4.	4.
Initial hold (min)	2.
Final hold (min)	20.				10.
I	1022.	1059.	1047.	1048.	1059.
Reference	Choi, 2003	Couladis, Özcan, et al., 2003	Dabiri and Sefidkon, 2003	Dabiri and Sefidkon, 2003, 2	Dudai, Larkov, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5MS	DB-1
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)				0.25	0.25
T_start (C)	50.	50.	50.	60.	50.
T_end (C)	220.	200.	220.	220.	200.
Heat rate (K/min)	3.	3.	3.	5.	5.
Initial hold (min)				20.
Final hold (min)				20.
I	1060.	1060.	1074.	1066.	1058.
Reference	Edris and Farrag, 2003	Edris, Shalaby, et al., 2003	Edris, Shalaby, et al., 2003, 2	Feizbaksh, Saber Tehrani, et al., 2003	Fekam Boyom, Ngouana, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-5	HP-5MS	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	40.
T_end (C)	275.	280.	275.	275.	280.
Heat rate (K/min)	4.	4.	4.	4.	6.
Initial hold (min)					5.
Final hold (min)					5.
I	1058.	1062.	1062.	1062.	1054.
Reference	Ghannadi, Aghazari, et al., 2003	Ghasemi, Asghari, et al., 2003	Ghannadi and Zolfaghari, 2003	Hajhashemi, Ghannadi, et al., 2003	Jirovetz, Buchbauer, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RSL-200	DB-5	SE-30	CP Sil 5 CB
Column length (m)	30.	30.	50.	12.	25.
Carrier gas	H2	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.3	0.25
T_start (C)	40.	40.	50.	70.	35.
T_end (C)	280.	280.	220.	220.	280.
Heat rate (K/min)	6.	6.	3.	3.	5.
Initial hold (min)	2.	5.	2.		2.5
Final hold (min)	10.	5.	10.
I	1055.	1055.	1061.	1043.	1047.
Reference	Jirovetz, Buchbauer, et al., 2003, 2	Jirovetz, Buchbauer, et al., 2003, 3	Juteau, Jerkovic, et al., 2003	Kambouche and El-Abed, 2003	Kanjilal, Kotoky, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	DB-5	ZB-1	DB-1
Column length (m)	30.	30.	50.	30.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	45.	50.
T_end (C)	240.	240.	220.	230.	270.
Heat rate (K/min)	3.	3.	3.	3.	4.
Initial hold (min)			2.
Final hold (min)
I	1063.	1062.	1059.	1043.	1058.
Reference	Machado, Zoghbi, et al., 2003	Maia, Taveira, et al., 2003	Masotti, Juteau, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003	Mirza, Nik, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	OV-101	CP Sil 5 CB	DB-1	DB-5
Column length (m)	30.	50.	25.	50.	30.
Carrier gas	Helium	He	H2	N2	H2
Substrate
Column diameter (mm)	0.32	0.2	0.25	0.25	0.25
Phase thickness (μm)		0.5	0.15	0.25	0.25
T_start (C)	70.	50.	50.	95.	60.
T_end (C)	210.	250.	230.	240.	280.
Heat rate (K/min)	2.	2.	3.	4.	4.
Initial hold (min)					10.
Final hold (min)	60.				40.
I	1060.	1048.	1054.	1052.	1062.
Reference	Mookdasanit, Tamura, et al., 2003	Orav, Kailas, et al., 2003	Oyedeji, Ekundayo, et al., 2003	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	NB-30	DB-1	DB-1
Column length (m)	30.	60.	50.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.5	0.25	0.25
T_start (C)	60.	50.	50.	40.	40.
T_end (C)	280.	250.	250.	220.	220.
Heat rate (K/min)	3.	4.	2.	4.	4.
Initial hold (min)
Final hold (min)
I	1043.	1047.	1050.	1048.	1055.
Reference	Pitarokili, Tzakou, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003	Raal, Arak, et al., 2003	Rasooli and Mirmostafa, 2003	Rasooli and Mirmostafa, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-1	DB-5	HP-5
Column length (m)	30.	30.	60.	30.	60.
Carrier gas	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	60.	40.
T_end (C)	230.	280.	280.	240.	250.
Heat rate (K/min)	2.	4.	4.	3.	5.
Initial hold (min)					15.
Final hold (min)
I	1045.	1060.	1055.	1063.	1061.
Reference	Rotman, Ahumada, et al., 2003	Sajjadi and Mehregan, 2003	Shahmir, Ahmadi, et al., 2003	da Silva, Luz, et al., 2003	Stashenko, Jaramillo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	DB-1	HP-5	HP-5	HP-5
Column length (m)	50.	50.	25.	25.	25.
Carrier gas	He	N2	H2	H2	Helium
Substrate
Column diameter (mm)	0.2	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.5	0.25	0.53	0.53	0.53
T_start (C)	60.	90.	40.	40.	40.
T_end (C)	220.	240.	280.	280.	280.
Heat rate (K/min)	2.	4.	4.	4.	4.
Initial hold (min)
Final hold (min)	40.
I	1046.	1053.	1060.	1060.	1055.
Reference	Valette, Fernandez, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5	DB-5
Column length (m)	25.	25.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.53	0.53	0.53	0.32	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	280.	280.	280.	250.	240.
Heat rate (K/min)	4.	4.	4.	5.	3.
Initial hold (min)				30.
Final hold (min)
I	1055.	1056.	1060.	1068.	1059.
Reference	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Yassa, Akhani, et al., 2003	Zoghbi, Andrade, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	CP Sil 5 CB	DB-1	DB-5
Column length (m)	25.	60.	25.	60.	30.
Carrier gas	N2	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.249
Phase thickness (μm)	0.25	0.25	0.4	0.25	0.25
T_start (C)	50.	50.	60.	60.	60.
T_end (C)	250.	280.	260.	220.	300.
Heat rate (K/min)	4.	4.	5.	4.	3.
Initial hold (min)
Final hold (min)	10.		40.		5.
I	1062.	1049.	1048.	1049.	1055.
Reference	Zrira, Elamrani, et al., 2003	Ahmadi, Mirza, et al., 2002	Azaz. D., Demirci, et al., 2002	Baher, Mirza, et al., 2002	Bos, Koulman, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5	HP-1	5 % Phenyl methyl siloxane	DB-1
Column length (m)	25.	30.	30.	30.	60.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.32
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	50.	60.	70.	75.	50.
T_end (C)	200.	280.	220.	200.	200.
Heat rate (K/min)	5.	3.	3.	3.	3.
Initial hold (min)				4.	6.
Final hold (min)		30.	15.	8.
I	1045.	1046.	1046.	1060.	1059.
Reference	Boyom, Keumedjio, et al., 2002	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002	Cicció and Gómez-Laurito, 2002	Cimanga, Apers, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5MS	BP-1	DB-5	HP-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.50	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	280.	280.	220.	250.	250.
Heat rate (K/min)	3.	3.	5.	4.	4.
Initial hold (min)					5.
Final hold (min)			10.
I	1056.	1056.	1050.	1062.	1062.
Reference	Congiu, Falconieri, et al., 2002	Congiu, Falconieri, et al., 2002	Das, Ram, et al., 2002	Farah, Fechtal, et al., 2002	Farah, Fechtal. M., et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	PTE-5	BP-1	SE-30
Column length (m)	30.	30.	60.	25.	50.
Carrier gas	H2	He	H2	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.32	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.30	0.1	0.25
T_start (C)	40.	60.	60.	40.	70.
T_end (C)	245.	275.	285.	250.	240.
Heat rate (K/min)	3.	4.	4.3	8.	4.
Initial hold (min)	20.			5.
Final hold (min)
I	1044.	1055.	1062.	1042.	1054.
Reference	Gancel, Ollé, et al., 2002	Ghannadi, Sajjadi, et al., 2002	Gudzic, Djokovic, et al., 2002	Hayes R.A., Richardson B.J., et al., 2002	Iñigo, Palá-Paúl, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RSL-200	CP Sil 8 CB	DB-1	SPB-5
Column length (m)	30.	30.	30.	25.	60.
Carrier gas	H2	H2	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.23	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	40.	50.	50.	50.	50.
T_end (C)	280.	280.	220.	200.	240.
Heat rate (K/min)	6.	6.	3.	3.	5.
Initial hold (min)	5.	5.	2.	3.	3.
Final hold (min)	5.	5.		30.	10.
I	1052.	1055.	1060.	1063.	1073.
Reference	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Ngassoum, et al., 2002	Juteau, Masotti, et al., 2002	Khallouki, Younos, et al., 2002	Kim and Lee, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	OV-101	DB-5	HP-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	35.	50.	40.	60.
T_end (C)	240.	280.	200.	290.	275.
Heat rate (K/min)	3.	3.	5.	7.	4.
Initial hold (min)		2.			4.
Final hold (min)		15.
I	1062.	1060.	1045.	1070.	1051.
Reference	Kobaisy, Tellez, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002	Kuiate, Bessière, et al., 2002	Lin, Rouseff, et al., 2002	Lockwood, Asghari, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	OV-101	HP-5	HP-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	240.	240.	200.	240.	240.
Heat rate (K/min)	3.	3.	5.	3.	3.
Initial hold (min)
Final hold (min)
I	1063.	1058.	1051.	1063.	1064.
Reference	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Menut, Bessière, et al., 2002	Novak, Langbehn, et al., 2002	Novak, Langbehn, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	SPB-5	DB-5	DB-1
Column length (m)	50.	50.	30.	30.	60.
Carrier gas	He	N2	Helium	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25
T_start (C)	50.	80.	60.	60.	40.
T_end (C)	250.	225.	250.	300.	250.
Heat rate (K/min)	2.	4.	4.	2.	4.
Initial hold (min)			2.
Final hold (min)			20.
I	1047.	1046.	1062.	1055.	1045.
Reference	Orav, Kailas, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Pino, Marbot, et al., 2002	Ruberto, Biondi, et al., 2002	Sefidkon, Dabiri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	DB-1	HP-5
Column length (m)	60.	60.	50.	50.	30.
Carrier gas	He	He	N2	N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	95.	60.	40.
T_end (C)	280.	280.	240.	240.	280.
Heat rate (K/min)	4.	4.	4.	3.	4.
Initial hold (min)	5.	5.
Final hold (min)
I	1050.	1048.	1040.	1035.	1062.
Reference	Sefidkon, Jalili, et al., 2002	Sefidkon, 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002, 2	Velickovic, Randjelovic, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5MS	DB-5	SPB-5	DB-1
Column length (m)	60.	30.	30.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	50.	60.	60.	40.	40.
T_end (C)	250.	270.	240.	220.	280.
Heat rate (K/min)	4.	3.	3.	3.	4.
Initial hold (min)	5.			5.	5.
Final hold (min)				15.
I	1048.	1056.	1058.	1060.	1039.
Reference	Yamini, Sefidkon, et al., 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5MS	HP-5	OV-1	HP-5
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	He	He	N2	H2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.3	0.25
T_start (C)	40.	35.	60.	50.	60.
T_end (C)	280.	250.	220.	250.	220.
Heat rate (K/min)	4.	3.	5.	3.	5.
Initial hold (min)	5.	5.	10.	1.	10.
Final hold (min)				20.
I	1049.	1073.	1063.	1049.	1064.
Reference	Dabiri and Sefidkon, 2001	Fernando and Grün, 2001	Flamini, Cioni, et al., 2001	Gallori, Bilia, et al., 2001	Gallori, Flamini, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	SPB-5	BP-1	CBP-1	DB-5MS
Column length (m)	30.	60.	50.	25.	30.
Carrier gas	N2	Helium	He	Nitrogen	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	50.	60.
T_end (C)	300.	240.	230.	210.	240.
Heat rate (K/min)	4.	3.	2.	3.	3.
Initial hold (min)		3.		2.
Final hold (min)		10.	35.		30.
I	1055.	1103.	1048.	1048.	1062.
Reference	Kalemba, Marschall, et al., 2001	Kim and Lee, 2001	Lota, de Rocca Serra, et al., 2001	Ly, Yamauchi, et al., 2001	Marongiu, Porcedda, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	RSL-200	OV-101	OV-101	DB-5
Column length (m)	60.	30.	50.	50.	60.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.5
T_start (C)	50.	40.	50.	50.	50.
T_end (C)	270.	280.	250.	250.	250.
Heat rate (K/min)	4.	6.	2.	2.	3.
Initial hold (min)		5.			5.
Final hold (min)		5.
I	1047.	1050.	1047.	1048.	1061.
Reference	Mirza, Ahmadi, et al., 2001	Ngassoum, Jirovetz, et al., 2001	Orav, Kailas, et al., 2001	Orav and Kann, 2001	Rousis, Papadogianni, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	PTE-5	DB-5	OV-101
Column length (m)	30.	30.	60.	30.	50.
Carrier gas	H2	Helium	H2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.3	0.25
T_start (C)	60.	50.	60.	60.	80.
T_end (C)	285.	250.	285.	240.	200.
Heat rate (K/min)	3.	5.	4.3	3.	2.
Initial hold (min)		2.
Final hold (min)		5.
I	1055.	1053.	1062.	1061.	1054.
Reference	Santos-Gomes and Fernandes-Ferreira, 2001	Shang, Hu, et al., 2001	Stojanovic, Palic, et al., 2001	Tellez M., Estell R., et al., 2001	Yang, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	SPB-1	RSL-200	HP-5
Column length (m)	50.	60.	30.	60.	30.
Carrier gas	N2	N2	He	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.25
Phase thickness (μm)		0.25	0.2	0.25
T_start (C)	80.	60.	80.	40.	80.
T_end (C)	200.	220.	300.	250.	200.
Heat rate (K/min)	2.	3.	5.	6.	9.
Initial hold (min)		5.	3.
Final hold (min)		22.			10.
I	1054.	1059.	1063.	1057.	1056.
Reference	Yang, 2001, 2	Bailac, Dellacasa, et al., 2000	Fraternale, Giamperi, et al., 2000	Jirovetz, Puschmann, et al., 2000	Lis-Balchin and Roth, 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	BP-1	HP-5
Column length (m)	30.	25.	30.	25.	30.
Carrier gas	He	Nitrogen	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.50	0.22	0.33	0.25
Phase thickness (μm)	0.25	0.25	0.25	1.0	0.25
T_start (C)	60.	60.	70.	60.	60.
T_end (C)	240.	220.	230.	275.	275.
Heat rate (K/min)	3.	5.	4.	4.	4.
Initial hold (min)			2.
Final hold (min)			20.
I	1057.	1053.	1068.	1060.	1062.
Reference	Maia, Zoghbi, et al., 2000	Mallavarapu, Rao, et al., 2000	Mitiku, Sawamura, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	DB-5	SE-30	Methyl Silicone
Column length (m)	30.	50.	30.	25.	60.
Carrier gas	He	Nitrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25		0.25		0.25
T_start (C)	40.	40.	60.	60.	40.
T_end (C)	260.	200.	240.	230.	220.
Heat rate (K/min)	2.	2.	3.	3.	5.
Initial hold (min)	5.	10.			10.
Final hold (min)	2.
I	1050.	1052.	1062.	1063.	1050.80
Reference	Senatore, Napolitano, et al., 2000	Tamura, Boonbumrung, et al., 2000	Tellez, Dayan, et al., 2000	Ali N.A.M. and Jantan, 1999	Baraldi, Rapparini, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	SPB-1	OV-101	DB-1	RTX-1
Column length (m)	25.	50.	52.	60.	30.
Carrier gas	Hydrogen		Helium	He	N2
Substrate
Column diameter (mm)	0.32	0.2	0.26	0.25	0.25
Phase thickness (μm)	0.30	0.33	0.13	0.25	0.25
T_start (C)	50.	60.	50.	50.	60.
T_end (C)	200.	260.	220.	230.	300.
Heat rate (K/min)	3.	4.	3.	4.	4.
Initial hold (min)	1.		0.
Final hold (min)	10.		0.
I	1041.	1051.	1050.	1056.	1054.
Reference	Bicchi, Binello, et al., 1999	Choo, Wong, et al., 1999	Dzumayev, Tkachenko, et al., 1999	Eikani, Goodarznia, et al., 1999	Kalemba, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	CBP-1	BP-1	OV-101	DB-5
Column length (m)	25.	25.	25.	50.	30.
Carrier gas		He	N2	N2
Substrate
Column diameter (mm)	0.32	0.3	0.50	0.2	0.32
Phase thickness (μm)			0.25		1.
T_start (C)	50.	60.	60.	80.	40.
T_end (C)	200.	240.	220.	200.	200.
Heat rate (K/min)	5.	4.	5.	1.	3.
Initial hold (min)					5.
Final hold (min)			10.	20.
I	1045.	1055.	1050.	1061.	1059.
Reference	Kuiate, Zollo, et al., 1999	Labuckas, Zygadlo, et al., 1999	Mallavarapu, Kulkarni, et al., 1999	Menon, Chacko, et al., 1999	Meynier, Novelli, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SE-30	OV-1	CP Sil 5 CB	OV-101
Column length (m)	30.	25.	25.	25.	50.
Carrier gas	He	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)			0.25		0.25
T_start (C)	40.	60.	40.	50.	70.
T_end (C)	230.	230.	220.	230.	220.
Heat rate (K/min)	4.	3.	3.	3.	2.
Initial hold (min)	1.	10.	5.		5.
Final hold (min)			5.
I	1060.	1063.	1047.	1053.	1052.
Reference	Mockute and Bernotiene, 1999	Mohd and Jantan, 1999	Oberhofer, Nikiforov, et al., 1999	Oyedeji, Olawore, et al., 1999	Pateira, Nogueira, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	CP Sil 5 CB	DB-1	DB-5	DB-1
Column length (m)	30.	25.	60.	30.	60.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.20	0.39	0.25	0.25	0.25
T_start (C)	60.	60.	40.	40.	50.
T_end (C)	200.	220.	280.	220.	220.
Heat rate (K/min)	3.	5.	4.	4.	4.
Initial hold (min)	4.	5.	5.	5.
Final hold (min)		20.
I	1054.	1054.	1051.	1057.	1057.
Reference	Prikhod'ko, Klyuev, et al., 1999	Rustaiyan, Masoudi, et al., 1999	Sefidkon, Dabiri, et al., 1999	Sefidkon and Khajavi, 1999	Sefidkon and Mirza, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	SPB-5	CP Sil 5 CB
Column length (m)	60.	30.	30.	60.	25.
Carrier gas	He	H2	He	He	N2
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32
Phase thickness (μm)			0.25	1.	0.39
T_start (C)	60.	32.	60.	40.	60.
T_end (C)	230.	260.	240.	200.	220.
Heat rate (K/min)	3.	7.	3.	3.	5.
Initial hold (min)		5.		5.
Final hold (min)	5.	5.		2.
I	1055.	1067.	1061.	1067.	1055.
Reference	Shafiee, Javidnia, et al., 1999	Sun and Petracek, 1999	Tellez, Canel, et al., 1999	Viallon C., Verdier-Metz I., et al., 1999	Weyerstahl, Marschall, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5	DB-5MS	SPB-5	DB-5
Column length (m)	25.	30.	30.	50.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.32	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	80.	60.	60.	60.	60.
T_end (C)	240.	240.	240.	240.	240.
Heat rate (K/min)	6.	3.	3.	3.	3.
Initial hold (min)
Final hold (min)				20.
I	1049.	1059.	1058.	1059.	1066.
Reference	Zenkevich, Kosman, et al., 1999	Zoghbi, Andrade, et al., 1999	Zoghbi, Andrade, et al., 1999, 2	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	OV-1	DB-5	HP-5	HP-1
Column length (m)	25.	50.	30.	25.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.32	0.25	0.2	0.25
Phase thickness (μm)		0.25	0.25	0.33	0.25
T_start (C)	60.	50.	60.	70.	50.
T_end (C)	180.	250.	240.	290.	280.
Heat rate (K/min)	3.	10.	3.	3.	4.
Initial hold (min)	10.	5.		8.	5.
Final hold (min)		20.		20.
I	1056.	1055.	1060.	1060.	1048.
Reference	Jantan, Ahmad, et al., 1998	Kökdil, Kurucu, et al., 1998	Maia, Zohhbi, et al., 1998	Poiana, Sicari, et al., 1998	Stashenko, Cervantes, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	CP Sil 5 CB	OV-1	SPB-Sulfur	SPB-Sulfur
Column length (m)	25.	25.	30.	30.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.32	0.32	0.32
Phase thickness (μm)		0.25	0.25	4.	4.
T_start (C)	50.	60.	40.	45.	45.
T_end (C)	200.	300.	270.	240.	240.
Heat rate (K/min)	5.	6.	2.	5.	5.
Initial hold (min)			4.	13.	13.
Final hold (min)				5.	5.
I	1054.	1047.	1061.	1063.	1064.
Reference	Zollo, Biyiti, et al., 1998	Bos, Woerdenbag, et al., 1997	Kökdil, Kurucu, et al., 1997	Mariaca, Berger, et al., 1997	Mariaca, Berger, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	DB-5	CBP-1
Column length (m)	30.		30.	30.	25.
Carrier gas	He		Helium	He	He
Substrate
Column diameter (mm)	0.25		0.25	0.25	0.22
Phase thickness (μm)	0.25		0.25
T_start (C)	50.	80.	60.	60.	60.
T_end (C)	250.	220.	240.	240.	240.
Heat rate (K/min)	2.	6.	3.	4.	5.
Initial hold (min)	5.
Final hold (min)
I	1056.	1035.	1061.	1088.	1055.
Reference	Reverchon, Porta, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Zunino, Novillo-Newton, et al., 1997	Zygadlo, Ariza-Espinar, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	OV-101	OV-101	DB-1	HP-1
Column length (m)	23.	50.	50.	60.	25.
Carrier gas	He	N2	He	He	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.17	0.17		0.50	0.25
T_start (C)	60.	50.	50.	50.	60.
T_end (C)	250.	220.	250.	250.	220.
Heat rate (K/min)	5.	5.	2.	8.	4.
Initial hold (min)	3.			1.	2.
Final hold (min)	30.			6.	20.
I	1047.	1056.	1047.	1057.	1047.
Reference	Ayedoun, Adeoti, et al., 1996	Chacko, Jayalekshmy, et al., 1996	Orav, Kailas, et al., 1996	Sagrero-Nieves and Bartley, 1996	Thanh, Dung, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5	HP-5	OV-101	DB-1
Column length (m)	50.			50.	60.
Carrier gas	He			He	He
Substrate
Column diameter (mm)	0.2			0.2	0.25
Phase thickness (μm)	0.33			0.5	0.25
T_start (C)	40.	35.	35.	70.	70.
T_end (C)	200.	200.	200.	180.	270.
Heat rate (K/min)	3.	6.	6.	1.	2.5
Initial hold (min)	3.	2.	2.		5.
Final hold (min)	30.
I	1049.	1066.	1065.	1045.	1051.
Reference	Wong and Lai, 1996	Larsen and Frisvad, 1995	Larsen and Frisvad, 1995, 2	Orav, Kuningas, et al., 1995	Tirado, Stashenko, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	OV-1	HP-5	HP-5
Column length (m)	60.		50.
Carrier gas	He		N2
Substrate
Column diameter (mm)	0.25		0.27
Phase thickness (μm)	0.25		0.2
T_start (C)	70.	35.	80.	40.	40.
T_end (C)	270.	200.	240.	210.	210.
Heat rate (K/min)	2.5	6.	3.	2.	2.
Initial hold (min)	5.	2.
Final hold (min)
I	1051.	1065.	1051.	1066.	1067.
Reference	Tirado, Stashenko, et al., 1995	Larsen and Frisvad, 1994	Ramanoelina, Viano, et al., 1994	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-101	Methyl Silicone	Methyl Silicone	CP Sil 5 CB	Methyl Silicone
Column length (m)	50.	50.	50.	25.	25.
Carrier gas	H2	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.50
Phase thickness (μm)	0.3	0.17	0.17
T_start (C)	65.	80.	80.	60.	60.
T_end (C)	300.	200.	200.	280.	220.
Heat rate (K/min)	2.	2.	3.	5.	5.
Initial hold (min)	5.
Final hold (min)
I	1045.	1057.	1055.	1054.	1057.
Reference	Demarne and van der Walt, 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Kaul, Singh, et al., 1993	Mallavarapu, Ramesh, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	OV-101	DB-1	SPB-5
Column length (m)	30.	30.	52.	60.	30.
Carrier gas	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.26	0.32
Phase thickness (μm)	0.25	0.25		1.2	1.0
T_start (C)	50.	50.	40.	30.	50.
T_end (C)	240.	240.	200.	240.	250.
Heat rate (K/min)	5.	5.	3.	3.	8.
Initial hold (min)	3.	3.	0.	10.
Final hold (min)			0.
I	1049.	1051.	1047.	1056.	1088.
Reference	Shiota, 1993	Shiota, 1993	Tkachenko and Zenkevich, 1993	Ciccioli, Cecinato, et al., 1992	King and Knight, 1992
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	DB-1	BP-1	OV-101	OV-101
Column length (m)	30.	30.	25.	50.	50.
Carrier gas	Hydrogen	N2		N2	N2
Substrate
Column diameter (mm)	0.25		0.33	0.25	0.25
Phase thickness (μm)	0.25
T_start (C)	60.	80.	45.	80.	80.
T_end (C)	250.	220.	180.	200.	200.
Heat rate (K/min)	2.	4.	3.	2.	2.
Initial hold (min)	5.		3.
Final hold (min)	2.
I	1059.	1031.	1050.	1053.	1055.
Reference	Kollmannsberger, Nitz, et al., 1992	Velasco-Negueruela, Pérez Alonso, et al., 1991	Wyllie, Brophy, et al., 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	SE-30	OV-101	OV-101	OV-101
Column length (m)	50.	40.	50.	50.	50.
Carrier gas	H2	He	N2	N2	N2
Substrate
Column diameter (mm)	0.30	0.50	0.25	0.25	0.25
Phase thickness (μm)		0.75
T_start (C)	40.	30.	80.	80.	80.
T_end (C)	250.	220.	200.	200.	200.
Heat rate (K/min)	10.	3.	2.	2.	2.
Initial hold (min)	1.
Final hold (min)
I	1050.	1047.	1053.	1053.	1056.
Reference	Brophy, Davies, et al., 1989	de Pooter, de Buyck, et al., 1989	Sugisawa, Yamamoto, et al., 1989	Sugisawa, Yang, et al., 1989	Sugisawa, Yang, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-1	OV-101	OV-101	OV-101
Column length (m)	60.	60.	50.	50.	50.
Carrier gas	He	Helium
Substrate
Column diameter (mm)	0.315	0.50	0.30	0.30	0.30
Phase thickness (μm)	0.25	1.2
T_start (C)	50.	40.	40.	40.	40.
T_end (C)	250.	220.	230.	230.	230.
Heat rate (K/min)	4.	2.	3.5	3.5	3.5
Initial hold (min)			5.	5.	5.
Final hold (min)
I	1048.	1046.	1049.	1055.	1063.
Reference	Engel, Flath, et al., 1988	Wahab, Aboutabl, et al., 1987	Nykanen, 1986	Nykanen, 1986	Nykanen, 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	OV-1	OV-101	DB-1	DB-1
Column length (m)	40.		30.	50.	50.
Carrier gas	He	He	He
Substrate
Column diameter (mm)	0.5		0.5	0.32	0.32
Phase thickness (μm)	0.75		0.8
T_start (C)	30.	40.	40.	0.	50.
T_end (C)	220.	220.	220.	250.	250.
Heat rate (K/min)	3.	2.	2.	3.	3.
Initial hold (min)
Final hold (min)
I	1048.	1048.	1045.	1048.	1046.
Reference	de Pooter, de Buyck, et al., 1986	De Pooter, De Buyck, et al., 1986	De Pooter and Schamp, 1986	Habu, Flath, et al., 1985	Habu, Flath, et al., 1985
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	SE-30	SE-30	SE-30+Igepal	SE-30+Igepal
Column length (m)	50.	50.		100.	100.
Carrier gas	He	He	Helium
Substrate
Column diameter (mm)	0.31	0.5		0.25	0.25
Phase thickness (μm)
T_start (C)	0.	40.	70.	70.	70.
T_end (C)	225.	170.	170.	170.	170.
Heat rate (K/min)	3.	3.	2.	1.	1.
Initial hold (min)	1.	3.
Final hold (min)
I	1044.	1049.	1046.	1024.	1025.
Reference	del Rosario, de Lumen, et al., 1984	Heydanek and McGorrin, 1981	Alves and Jennings, 1979	Shibamoto and Jennings, 1977	Shibamoto and Jennings, 1977
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Bertuzzi, Tirillini, et al., 2013
Bertuzzi, G.; Tirillini, B.; Angelini, P.; Venanzoni, R., Antioxidative action of Citrus limonum essential oil on scin, Eur. J. Medicinal Plants, 2013, 3, 1, 1-9, https://doi.org/10.9734/EJMP/2013/1987 . [all data]

Sardashti, Valizadeh, et al., 2013
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Alizadeh and Shaabani, 2012
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Dell'Agli, Sanna, et al., 2012
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Priya, Prathapan, et al., 2012
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Yapi, T.A.; Boti, J.B.; Attioua, B.K.; Ahibo, A.C.; Bighelli, A.; Casanova, J.; Tomi, F., Three new natural compounds from the root bark essential oil from Xylopia aethiopica, Phytochem. Anal., 2012, 1-6. [all data]

Zouari, Ayadi, et al., 2012
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Kim and Lee, 2002
Kim, N.-S.; Lee, D.-S., Comparison of different extraction methods for the analysis of fragrances from Lavandula species by gas chromatography-mass spectrometry, J. Chromatogr. A, 2002, 982, 1, 31-47, https://doi.org/10.1016/S0021-9673(02)01445-0 . [all data]

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Lin, J.; Rouseff, R.L.; Barros, S.; Naim, M., Aroma composition changes in early season grapefruit juice produced from thermal concentration, J. Agric. Food Chem., 2002, 50, 4, 813-819, https://doi.org/10.1021/jf011154g . [all data]

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Maia, J.G.S.; da Silva, M.H.L.; Andrade, E.H.A.; Zoghbi, M.G.B.; Carreira, L.M.M., Essential oils from Astronium urundeuva (Allemao) Engl. and A. fraxinifolium Schott ex Spreng., Flavour Fragr. J., 2002, 17, 1, 72-74, https://doi.org/10.1002/ffj.1046 . [all data]

Maia, Zoghbi, et al., 2002
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Sefidkon, F.; Dabiri, M.; Alamshahi, A., Analysis of the essential oil of Nepeta fissa C.A. Mey from Iran, Flavour Fragr. J., 2002, 17, 2, 89-90, https://doi.org/10.1002/ffj.1045 . [all data]

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Sefidkon, 2002
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Yamini, Y.; Sefidkon, F.; Pourmortazavi, S.M., Comparison of essential oil composition of Iranian fennel (Foeniculum vulgare) obtained by supercritical carbon dioxide extraction and hydrodistillation methods, Flavour Fragr. J., 2002, 17, 5, 345-348, https://doi.org/10.1002/ffj.1117 . [all data]

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Cornu, A.; Carnat, A.-P.; Martin, B.; Coulon, J.-B.; Lamaison, J.-L.; Berdagué, J.-L., Solid-phase microextraction of volatile components from natural grassland plants, J. Agric. Food Chem., 2001, 49, 1, 203-209, https://doi.org/10.1021/jf0008341 . [all data]

Dabiri and Sefidkon, 2001
Dabiri, M.; Sefidkon, F., Analysis of the essential oil from aerial parts of Perovskia atriplicifolia Benth. at different stages of plant growth, Flavour Fragr. J., 2001, 16, 6, 435-438, https://doi.org/10.1002/ffj.988 . [all data]

Fernando and Grün, 2001
Fernando, L.N.; Grün, I.U., Headspace-SPME analysis of volatiles of the ridge gourd (Luffa acutangula) and bitter gourd (Momordica charantia) flowers, Flavour Fragr. J., 2001, 16, 4, 289-293, https://doi.org/10.1002/ffj.999 . [all data]

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Gallori, S.; Bilia, A.R.; Mulinacci, N.; Bicchi, C.; Rubiolo, P.; Vincieri, F.F., Identification of volatile constituents of Tambourissa leptophylla, Planta Medica, 2001, 67, 3, 290-292, https://doi.org/10.1055/s-2001-12001 . [all data]

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Kalemba, Marschall, et al., 2001
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Kim and Lee, 2001
Kim, N.-S.; Lee, D.-S., Characterization of Rosemary fragrances by solid phase microextraction and GC-MS, Analyt. Sci., 2001, 17, Supplement, a383-a386. [all data]

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Lis-Balchin and Roth, 2000
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Kalemba, 1999
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Sefidkon and Khajavi, 1999
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Sun and Petracek, 1999
Sun, D.; Petracek, P.D., Grapefruit gland oil composition is affected by wax application, storage temperature, and storage time, J. Agric. Food Chem., 1999, 47, 5, 2067-2069, https://doi.org/10.1021/jf981064k . [all data]

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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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