α-Phellandrene

Formula: C₁₀H₁₆
Molecular weight: 136.2340
IUPAC Standard InChI: InChI=1S/C10H16/c1-8(2)10-6-4-9(3)5-7-10/h4-6,8,10H,7H2,1-3H3
IUPAC Standard InChIKey: OGLDWXZKYODSOB-UHFFFAOYSA-N
CAS Registry Number: 99-83-2
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
- (+)-α-phellandrene
- (+)-(4S)-α-phellandrene
Other names: 1,3-Cyclohexadiene, 2-methyl-5-(1-methylethyl)-; α-Fellandrene; p-Mentha-1,5-diene; 5-Isopropyl-2-methyl-1,3-cyclohexadiene; 2-methyl-5-(1-methylethyl)-1,3-cyclohexadiene; 4-Isopropyl-1-methyl-1,5-cyclohexadiene; 2-Methyl-5-isopropyl-1,3-cyclohexadiene; alpha-Phellandrene; 5-Isopropyl-2-methyl-cyclohexa-1,3-diene; Menthadiene; Phellandrene; L-Phellandrene; 5-isopropyl-2-methylcyclohexa-1,3-diene (α-phellandrene); (-)-α-phellandrene; α-phellanderene
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Normal alkane RI, non-polar column, temperature ramp

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Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-1	RTX-1	RTX-1	DB-5
Column length (m)	60.	30.	60.	60.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	100.
T_end (C)	250.	240.	230.	230.	260.
Heat rate (K/min)	3.	3.	2.	2.	10.
Initial hold (min)	1.				1.
Final hold (min)	20.		5.	5.	10.
I	997.	999.	1002.	1002.	1007.
Reference	Sardashti, Valizadeh, et al., 2013	Alizadeh and Shaabani, 2012	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012	Boukhris, Bouaziz, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Mega-5	HP-5 MS	Polydimethyl siloxane with 5 % Ph	HP-5 MS	HP-1
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	35.	80.	50.	60.
T_end (C)	220.	300.	200.	250.	240.
Heat rate (K/min)	3.	3.	5.	7.	3.
Initial hold (min)	1.	5.		1.
Final hold (min)	5.	15.	25.	5.
I	1003.	1005.	1004.	1006.	1002.
Reference	Dell'Agli, Sanna, et al., 2012	Kotowska, Zalikowski, et al., 2012	Priya, Prathapan, et al., 2012	Zouari, Ayadi, et al., 2012	Alizadeh, Khosh-Khui, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	VF-5 MS	VF-5 MS	SE-30 MS	CP-Sil 5 CB
Column length (m)	30.	60.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.26
T_start (C)	40.	30.	30.	50.	45.
T_end (C)	250.	260.	260.	250.	280.
Heat rate (K/min)	3.	2.	2.	5.	3.
Initial hold (min)	5.			5.
Final hold (min)	20.	28.	28.	10.	22.
I	1003.	1006.	1007.	1005.	999.
Reference	Cao, Li, et al., 2011	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011	Menichini, Tundis, et al., 2011	Mothana, Hasson, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5 MS	ZB-5 MS	DB-5 MS	DB-5 MS	RTX-1
Column length (m)	30.	30.	25.	25.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.30	0.30	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	290.	290.	240.	240.	230.
Heat rate (K/min)	5.	5.	3.	3.	2.
Initial hold (min)
Final hold (min)					30.
I	1003.	1008.	1005.	1005.	1002.
Reference	Boix, Victorio, et al., 2010	Boix, Victorio, et al., 2010	Chalchat, Figueredo, et al., 2010	Chalchat, Figueredo, et al., 2010	Dib, Djabou, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	DB-5 MS	DB-1	BP-1
Column length (m)	30.	30.	60.	25.
Carrier gas	Helium	Helium	Helium	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	40.	60.	60.
T_end (C)	280.	290.	250.	250.	220.
Heat rate (K/min)	3.	5.	5.	4.	5.
Initial hold (min)			15.	1.	10.
Final hold (min)			15.	10.	30.
I	997.	1009.	1009.	1002.	997.
Reference	Georgiou, Koutsaviti, et al., 2010	Lazarevic, Radulovic, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010	Mirjalili, Salehi, et al., 2010	Mishra, Chaudhary, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	HP-5	SLB-5 MS	SLB-5 MS
Column length (m)	30.	30.	30.	10.	10.
Carrier gas	Helium	Helium	Hydrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.10	0.10
Phase thickness (μm)	0.25	0.25	0.25	0.10	0.10
T_start (C)	40.	60.	70.	50.	50.
T_end (C)	260.	220.	290.	250.	250.
Heat rate (K/min)	4.	5.	5.	10.	10.
Initial hold (min)		10.
Final hold (min)	5.
I	1006.	1008.	1010.	1005.	1007.
Reference	Miyazawa, Kawauchi, et al., 2010	Ogunwande, Flamini, et al., 2010	Radulovic, Dordevic, et al., 2010	Scandinaro, Tranchida, et al., 2010	Scandinaro, Tranchida, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1-MS	DB-5	OV-101	OV-101
Column length (m)	30.	60.	30.	50.	50.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	30.	80.	70.	70.
T_end (C)	240.	200.	240.	220.	220.
Heat rate (K/min)	3.	2.	3.	2.	2.
Initial hold (min)	1.	4.
Final hold (min)		35.	2.
I	981.	993.	1006.	1000.	1008.
Reference	de Souza, Lopes, et al., 2010	Takeoka, Hobbs, et al., 2010	Vahirua-Lechat, Mitermite, et al., 2010	Benites, Moiteiro, et al., 2009	Benites, Moiteiro, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	ZB-5	SPB-5	SPB-5	DB-5
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.35	0.53	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.50	0.25
T_start (C)	60.	50.	60.	50.	50.
T_end (C)	250.	240.	230.	210.	250.
Heat rate (K/min)	2.	3.	4.	3.	5.
Initial hold (min)	8.			5.	2.
Final hold (min)	15.	1.	40.	45.
I	1010.	1000.	1009.	996.	1003.
Reference	Farhat, Ginies, et al., 2009	Gardini, Beletti, et al., 2009	Gauvin-Bialecki and Marodon, 2009	Gilani, Shah, et al., 2009	Ho, Wang, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	VF-1 MS	RTX-1	RTX-1
Column length (m)	50.	30.	30.	60.	60.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.22	0.22
Phase thickness (μm)	0.32	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	60.	60.	60.
T_end (C)	220.	240.	280.	230.	230.
Heat rate (K/min)	5.	5.	4.	2.	2.
Initial hold (min)	3.		5.
Final hold (min)			10.	30.	30.
I	1005.	1002.	1013.	1002.	998.
Reference	Kazemi and Akhavani, 2009	Lawal and Oyedelji, 2009	Marchesini, Prada, et al., 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	5 % Phenyl methyl siloxane	DB-1 MS
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	Helium	Nitrogen	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	45.	40.	40.	90.	40.
T_end (C)	250.	250.	250.	225.	250.
Heat rate (K/min)	3.	3.	3.	3.	6.
Initial hold (min)	3.	1.	1.		1.
Final hold (min)	5.	10.	10.	3.	4.
I	1008.	1001.	1003.	1002.	995.
Reference	Porto, Decorti, et al., 2009	Rahmi-Nasrabadi, Gholivand, et al., 2009	Rahimi-Nasrabadi, Gholivand, et al., 2009	Retta, Gattuso, et al., 2009	Seo, Kim, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5MS	HP-5 MS	HP-5 MS
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.32	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	50.	60.	50.
T_end (C)	220.	240.	240.	325.	280.
Heat rate (K/min)	5.	3.	5.	10.	4.
Initial hold (min)	3.	1.		6.
Final hold (min)	5.			10.
I	1005.	981.	1006.	1003.	1004.
Reference	Shafaghat and Sadeghi, 2009	de Souza, Lopes, et al., 2009	Wannes, Mhamdi, et al., 2009	Zaibunnisa, Norashikin, et al., 2009	Zhao, Zeng, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	SLB-5 MS	BPX-5	RTX-5
Column length (m)	30.	25.	30.	7.5	20.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.10	0.18
Phase thickness (μm)	0.25	0.25	0.25	10.	0.20
T_start (C)	50.	50.	50.	60.	50.
T_end (C)	280.	300.	250.	240.	280.
Heat rate (K/min)	9.	6.5	3.	3.	4.
Initial hold (min)	3.	2.	2.		1.
Final hold (min)	3.	7.	10.
I	1005.	1005.	1007.	1013.	1008.
Reference	Aicha, Ines, et al., 2008	Chieng, Assim, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Shellie, 2008	Skalicka-Wozniak, Los, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	HP-5	HP-5 MS	HP-5 MS	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	65.	60.	50.	60.	60.
T_end (C)	260.	250.	230.	200.	300.
Heat rate (K/min)	6.	5.	3.	4.	4.
Initial hold (min)		30.	10.
Final hold (min)			10.	20.
I	1012.	1004.	1005.	1004.	995.
Reference	Wang, Yi, et al., 2008	Yassa and Akhani, 2008	Adams, Beauchamp, et al., 2007	Araque, Rojas, et al., 2007	Baran, von Reuss, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.26	0.26	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	40.
T_end (C)	280.	240.	240.	240.	220.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)				1.
Final hold (min)				4.
I	996.	1002.	1004.	1005.	1014.
Reference	Basta, Pavlovic, et al., 2007	Bos, Woerdenbag, et al., 2007	Bos, Woerdenbag, et al., 2007	Cheraif, Ben Jannet, et al., 2007	Chyau, Tsai, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	DB-5	HP-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.26	0.26	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.26	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	290.	290.	240.	250.
Heat rate (K/min)	3.	3.	3.	4.	2.
Initial hold (min)				2.	8.
Final hold (min)				20.	15.
I	1003.	1002.	1004.	1003.	1001.
Reference	Da Silva J.K.R., Sousa P.J.C., et al., 2007	Elfami, Bos, et al., 2007	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007	Ferhat, Meklati, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	Col-Elite 5MS	RTX-5 MS	SE-30	HP-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	Nitrogen	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	30.	45.	40.	40.
T_end (C)	250.	246.	210.	250.	250.
Heat rate (K/min)	4.	3.	3.	5.	5.
Initial hold (min)	1.			5.	5.
Final hold (min)	10.			10.	10.
I	1003.	1002.	1005.	1005.	1003.
Reference	Ghasempour, Shirinpour, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Hudaib and Aburjai, 2007	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	AT-5	ZB-5	HP-5	SPB-1
Column length (m)	30.	60.	30.	25.	30.
Carrier gas	He	Helium		H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.2
T_start (C)	60.	60.	60.	60.	70.
T_end (C)	280.	260.	220.	240.	220.
Heat rate (K/min)	3.	4.	4.	3.	3.
Initial hold (min)			5.
Final hold (min)	30.		20.		15.
I	983.	994.	1005.	1006.	998.
Reference	Marongiu B., Piras A., et al., 2007	Meccia, Rojas, et al., 2007	Mohottalage, Tabacchi, et al., 2007	Oliveira, Leitão, et al., 2007	Pinto, Salgueiro, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	DB-1	HP-5	HP-5 MS	DB-1
Column length (m)	50.	60.	30.	60.	60.
Carrier gas	He	Nitrogen	Helium	Hydrogen	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	40.	60.	60.
T_end (C)	300.	250.	260.	260.	250.
Heat rate (K/min)	4.	4.	4.	4.	5.
Initial hold (min)	1.	1.
Final hold (min)	10.	10.		20.
I	1026.	1003.	998.	994.	999.
Reference	Rali, Wossa, et al., 2007	Reza, Ebrahim, et al., 2007	Ristic, Krivokuca-Dokic, et al., 2007	Rojas, Velasco, et al., 2007	Salehi, Fakhari, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5 MS	HP-5MS	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	240.	250.	280.	280.	280.
Heat rate (K/min)	4.	2.	3.	3.	3.
Initial hold (min)
Final hold (min)		33.
I	1001.	1000.	1005.	973.	1003.
Reference	Sefidkon, Abbasi, et al., 2007	Sylvestre, Pichette, et al., 2007	Tsokou, Georgopoulos, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	HP-5	HP-5	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25
T_start (C)	40.	60.	50.	50.	80.
T_end (C)	250.	250.	280.	280.	270.
Heat rate (K/min)	3.	5.	9.	9.	10.
Initial hold (min)	5.	30.	3.	3.
Final hold (min)	10.		3.	3.
I	999.	1004.	1005.	1008.	1002.
Reference	Vichi, Riu-Aumatell, et al., 2007	Yassa and Akhani, 2007	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006	Ayoub, Al-Azizi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	AT-5	HP-1	HP-1	SPB-1
Column length (m)	30.	60.	50.	50.	30.
Carrier gas		He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.2	0.20
Phase thickness (μm)	0.25	0.25	0.5	0.33	0.20
T_start (C)	40.	60.	60.	60.	70.
T_end (C)	300.	200.	250.	250.	220.
Heat rate (K/min)	2.	4.	2.	2.	3.
Initial hold (min)				4.
Final hold (min)		20.	120.	30.	15.
I	1003.	1004.	997.	997.	997.
Reference	Biondi, Sari, et al., 2006	Borges, Rojas, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Cavaleiro, Pinto, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He			Helium	Helium
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.26	0.26
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	246.	230.	280.	290.	290.
Heat rate (K/min)	3.	3.	4.	3.	3.
Initial hold (min)
Final hold (min)		15.
I	1004.	1005.	1007.	1002.	1004.
Reference	Coronel, Cerda-Garcia-Rojas, et al., 2006	Damjanovic, Skala, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006	Elfami, Komar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-1	HP-5	DB-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	250.	250.	300.	240.	240.
Heat rate (K/min)	2.	2.	5.	5.	5.
Initial hold (min)			5.	2.	2.
Final hold (min)		60.	5.
I	1005.	996.	1006.	1005.	1005.
Reference	Farah, Afifi, et al., 2006	Fernandez, Pintaric, et al., 2006	Figuérédo, Cabassu, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	HP-5	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	250.	220.	240.	260.	260.
Heat rate (K/min)	3.	3.	4.	4.	3.
Initial hold (min)
Final hold (min)	10.	3.
I	1005.	1003.	1005.	1005.	1004.
Reference	Havlik, Kokoska, et al., 2006	Hymete, Rohloff, et al., 2006	Ibañez and Usubillaga, 2006	Ibanez and Usubillaga, 2006	Javidnia, Miri, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	CP Sil 5 CB	CP Sil 8 CB	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2		N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	60.	40.	50.
T_end (C)	280.	280.	300.	250.	300.
Heat rate (K/min)	5.	5.	5.	3.	4.
Initial hold (min)	4.	4.	4.	5.
Final hold (min)	10.	10.		20.
I	1008.	1003.	997.	1006.	1004.
Reference	Kim, Abd El-Aty, et al., 2006	Kim, El-Aty, et al., 2006	Kurowska and Galazka, 2006	Li, Lee, et al., 2006	Lis and Milczarek, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5 MS	HP-5	5 % Phenyl methyl siloxane	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	Nitrogen	N2	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.52	0.25	0.25
T_start (C)	50.	50.	50.	60.	50.
T_end (C)	200.	280.	280.	280.	250.
Heat rate (K/min)	5.	5.	5.	3.	3.
Initial hold (min)					5.
Final hold (min)		5.	5.	30.
I	998.	1007.	1007.	981.	1003.
Reference	Martin, Joseph, et al., 2006	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Marongiu, Piras, et al., 2006	Mirza, Navaei, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	NB-30	SE-52	DB-1
Column length (m)	25.	30.	30.	50.	50.
Carrier gas	He	He	He	Helium	N2
Substrate
Column diameter (mm)	0.3	0.25	0.2	0.25	0.25
Phase thickness (μm)		0.25	0.25		0.25
T_start (C)	70.	60.	50.	50.	95.
T_end (C)	220.	220.	250.	240.	240.
Heat rate (K/min)	4.	4.	2.	3.	4.
Initial hold (min)	2.	5.
Final hold (min)	10.
I	1002.	1004.	999.	1005.	1006.
Reference	Moody, Gundidza, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Orav, Raal, et al., 2006	Ozcan, Chalchat, et al., 2006	Pala-Paul J., Perez-Alonso M.J., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DB-5	HP-5	HP-5MS
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	Hydrogen	Hydrogen	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	70.	60.	50.
T_end (C)	220.	280.	280.	240.	250.
Heat rate (K/min)	5.	4.	4.	3.	10.
Initial hold (min)	10.	4.	4.		5.
Final hold (min)
I	1008.	1004.	1000.	1007.	1001.
Reference	Pintore G., Chessa M., et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Potzernheim, Bizzo, et al., 2006	Robinson, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	ZB-5	DB-1	FSOT-RSL-200	DB-5
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	He		Hydrogen	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	70.	40.	50.
T_end (C)	260.	300.	230.	280.	240.
Heat rate (K/min)	5.	2.	2.	6.	4.
Initial hold (min)			2.	5.
Final hold (min)			20.	5.
I	1010.	1003.	999.	1002.	1006.
Reference	Sabulal, Dan, et al., 2006	Sari M., Biondi D.M., et al., 2006	Sawamura, Onishi, et al., 2006	Schmidt, Jirovetz, et al., 2006	Sefidkon, Abbasi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	CP Sil 5 CB	Methyl Silicone
Column length (m)	30.	30.	25.	25.	25.
Carrier gas	He	He	N2		N2
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.3
Phase thickness (μm)	0.25	0.25	0.33		0.15
T_start (C)	50.	40.	30.	50.	50.
T_end (C)	240.	240.	280.	230.	210.
Heat rate (K/min)	4.	4.	3.	3.	2.
Initial hold (min)					5.
Final hold (min)
I	1008.	1004.	1009.	1003.	1016.
Reference	Sefidkon, Abbasi, et al., 2006	Sefidkon and Jamzad, 2006	Shafi, Jose, et al., 2006	Tesso, Kubeczka, et al., 2006	Tonzibo, Coffy, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	DB-1	HP-5	SPB-1
Column length (m)	60.	30.	50.	30.	50.
Carrier gas	He	N2	N2	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.2
Phase thickness (μm)	1.	0.25	0.25	0.25	0.33
T_start (C)	40.	60.	90.	60.	50.
T_end (C)	230.	240.	240.	250.	220.
Heat rate (K/min)	3.	4.	4.	10.	4.
Initial hold (min)	5.			2.	1.
Final hold (min)	2.			10.	10.
I	1014.	1003.	989.	1009.	995.
Reference	Tornambe, Cornu, et al., 2006	Trilles, Bombarda, et al., 2006	Velasco-Negueruela, Pérez-Alonso, et al., 2006	Wang, Yang, et al., 2006	Wong, Lim, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5MS	DB-5MS	DB-1	DB-5
Column length (m)	30.	30.	30.	25.	50.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.3
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	250.	280.	240.	250.	240.
Heat rate (K/min)	4.	3.	3.	3.	2.
Initial hold (min)	1.			3.
Final hold (min)	10.
I	992.	1001.	1008.	1003.	1005.
Reference	Wong, Sivasothy, et al., 2006	Basta, Tzakou, et al., 2005	Busman, Zoghbi, et al., 2005	Cégiéla-Carlioz, Bessière, et al., 2005	Chagonda and Chalchat, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	SPB-5	DB-1	DB-1	HP-1
Column length (m)	60.	60.	60.	60.	50.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.3	0.32	0.25	0.25	0.2
Phase thickness (μm)		1.	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	240.	230.	250.	250.	250.
Heat rate (K/min)	3.	3.	5.	5.	2.
Initial hold (min)		5.			60.
Final hold (min)				10.
I	1005.	1013.	1003.	1005.	996.
Reference	Chalchat and Özcan, 2005	Cornu, Kondjoyan, et al., 2005	Fakhari, Salehi, et al., 2005	Fakhari A.R., Sonboli A., et al., 2005	Fernandez, Lizzani-Cuvelier, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	CP Sil 5 CB	RSL-200	DB-1
Column length (m)	30.	25.	30.	30.	60.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	50.	60.	40.	50.
T_end (C)	300.	250.	250.	280.	250.
Heat rate (K/min)	5.	3.	5.	6.	4.
Initial hold (min)	5.	3.		2.	5.
Final hold (min)	5.	10.	10.	10.
I	1006.	1006.	1005.	1002.	1004.
Reference	Figuérédo, Cabassu, et al., 2005	Ghasemi Y., Faridi P., et al., 2005	Jassbi, Mehrdad, et al., 2005	Jirovetz, Buchbauer, et al., 2005	Khajeh, Yamini, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	CP Sil 5 CB	HP-5	DB-1
Column length (m)	30.	25.	25.	30.	50.
Carrier gas	He			He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.15	0.15	0.25	0.25
T_start (C)	60.	50.	50.	70.	95.
T_end (C)	220.	230.	230.	240.	240.
Heat rate (K/min)	4.	3.	3.	5.	4.
Initial hold (min)	4.
Final hold (min)
I	1004.	1002.	1002.	1002.	1005.
Reference	Morteza-Semnani and Saeedi, 2005	Ogunwande, Olawore, et al., 2005	Olawore, Ogunwande, et al., 2005	Oyedeji, Yani, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	DB-1	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	50.	30.	60.	30.	30.
Carrier gas	N2		He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	95.	60.	50.	40.	40.
T_end (C)	240.	280.	250.	220.	220.
Heat rate (K/min)	4.	3.	4.	4.	4.
Initial hold (min)				1.	1.
Final hold (min)
I	1027.	1003.	995.	1003.	1003.
Reference	Pala-Paul, Perez-Alonso, et al., 2005	Petrakis, Roussis, et al., 2005	Rasooli and Owlia, 2005	Rohloff and Bones, 2005	Rohloff and Bones, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	DB-1	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	40.
T_end (C)	240.	275.	220.	265.	240.
Heat rate (K/min)	5.	4.	3.	2.5	4.
Initial hold (min)			4.	1.
Final hold (min)				20.
I	1005.	1006.	1001.	990.	1004.
Reference	Saeidnia, Gohari, et al., 2005	Sajjadi and Ghannadi, 2005	Salehi, Sefidkon, et al., 2005	Sarkhail, Amin, et al., 2005	Sefidkon and Jamzad, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	RTX-1	DB-5	HP-5MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	50.
T_end (C)	280.	230.	25.	210.	240.
Heat rate (K/min)	3.	3.	5.	2.	3.
Initial hold (min)	5.			2.	3.
Final hold (min)		20.	10.	33.
I	1003.	1003.	1001.	1002.	994.
Reference	Setzer, Noletto, et al., 2005	Skoula and Grayer, 2005	Sonboli, Salehi, et al., 2005	Stevanovic, Garneau, et al., 2005	Tepe B., Sokmen M., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	DB-5	DB-1	DB-1
Column length (m)	30.	30.	30.	50.	50.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.50	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	90.	60.
T_end (C)	260.	280.	280.	240.	240.
Heat rate (K/min)	3.	3.	3.	4.	3.
Initial hold (min)
Final hold (min)	20.
I	1003.	966.	988.	989.	987.
Reference	Topçu, Barla, et al., 2005	Tzakou, Bazos, et al., 2005	Tzakou and Constantinidis, 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	CP Sil 5 CB	DB-5	BP-1	SE-52
Column length (m)	50.	30.	30.	50.	25.
Carrier gas	He	N2	He		N2
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.22	0.32
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.15
T_start (C)	50.	50.	90.	60.	45.
T_end (C)	220.	200.	220.	220.	200.
Heat rate (K/min)	4.	5.	7.	2.	3.
Initial hold (min)	3.		2.		5.
Final hold (min)	30.		5.	20.	30.
I	999.	1003.	995.	997.	1012.
Reference	Wong, Lee, et al., 2005	Agnaniet, Menut, et al., 2004	Agnihotri, Thappa, et al., 2004	Blanc, Muselli, et al., 2004	Cakir, Kordali, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	DB-1	DB-5
Column length (m)	60.	30.	30.	25.	25.
Carrier gas	N2	He	N2		Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	40.	60.	60.
T_end (C)	230.	240.	230.	180.	240.
Heat rate (K/min)	2.	2.	2.	3.	3.
Initial hold (min)	2.			10.
Final hold (min)	20.			10.
I	1004.	1003.	1005.	1001.	1006.
Reference	Choi, 2004	Cicció, 2004	González, Guerra, et al., 2004	bin Jantan, Ayop, et al., 2004	JAvidnia, Mojab, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	DB-5	RTX-1	SE-54	HP-5MS
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	50.
T_end (C)	260.	280.	300.	260.	230.
Heat rate (K/min)	6.	4.	4.	2.	5.
Initial hold (min)	4.6	4.		5.	2.
Final hold (min)	1.				10.
I	1016.	1001.	1001.	1002.	994.
Reference	Jürgens and Dötterl, 2004	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004	Li and Jiang, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5	HP-5MS	DB-5MS	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2		He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	300.	210.	280.	280.	280.
Heat rate (K/min)	4.	2.	3.	3.	3.
Initial hold (min)		2.
Final hold (min)		33.		30.	30.
I	1004.	1000.	1002.	982.	979.
Reference	Lis, Boczek, et al., 2004	Lopez Arze, Collin, et al., 2004	Malencic, Couladis, et al., 2004	Marongiu, Piras, et al., 2004	Marongiu, Porcedda, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	NB-30	DB-1	DB-1	DB-1
Column length (m)	50.	50.	50.	50.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.2	0.2	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	70.	95.	50.
T_end (C)	250.	250.	220.	240.	250.
Heat rate (K/min)	2.	2.	4.	4.	4.
Initial hold (min)
Final hold (min)
I	1002.	999.	1003.	994.	995.
Reference	Orav, Stulova, et al., 2004	Orav, Stulova, et al., 2004	Palá-Paúl, García-Jiménez, et al., 2004	Palá-Paúl, Velasco-Negueruela, et al., 2004	Rasooli and Razzaghi Abyaneh, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	HP-5 MS	HP-5MS	DB-1	DB-1
Column length (m)	60.	30.	30.	60.	60.
Carrier gas	He	Helium	He		Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	70.	70.
T_end (C)	200.	200.	280.	230.	230.
Heat rate (K/min)	4.	4.	4.	2.	2.
Initial hold (min)	1.	1.		2.	2.
Final hold (min)	20.	20.		20.
I	1001.	1001.	1006.	1006.	1006.
Reference	Rojas, Usubillaga, et al., 2004	Royas, Usubillaga, et al., 2004	Sajjadi and Shahpiri, 2004	Sawamura, Son, et al., 2004	Sawamura, Sou, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	HP-5	HP-5	CP Sil 5 CB
Column length (m)	30.	30.	25.	25.	20.
Carrier gas		He	N2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.25
Phase thickness (μm)	0.25	0.33	0.5	0.52	0.25
T_start (C)	50.	40.	30.	40.	100.
T_end (C)	250.	260.	280.	240.	270.
Heat rate (K/min)	3.	2.	3.	4.	8.
Initial hold (min)	5.	5.			2.
Final hold (min)		20.
I	1004.	998.	1009.	1003.	998.
Reference	Sefidkon, Jamzad, et al., 2004	Senatore, Napolitano, et al., 2004	Shafi, Nambiar, et al., 2004	Simic, Sokovic, et al., 2004	Thappa, Bakshi, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	CP Sil 8 CB	CP Sil 8 CB	DB-5	HP-5MS
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.22	0.25	0.32	0.249	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	60.	60.
T_end (C)	250.	200.	200.	300.	275.
Heat rate (K/min)	3.	10.	5.	3.	4.
Initial hold (min)	5.	3.	5.
Final hold (min)	10.	2.
I	1017.	1003.	1009.	1004.	1004.
Reference	Vilaseca, Guy, et al., 2004	Wang and Guo-Y. -L., 2004	Wang, Guo, et al., 2004	Woerdenbag, Windono, et al., 2004	Afsharypuor and Jahromy, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	RTX-5Sil	HP-5MS	HP-5MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	70.	60.	60.
T_end (C)	230.	280.	200.	220.	280.
Heat rate (K/min)	2.	3.	4.	5.	4.
Initial hold (min)	2.			20.
Final hold (min)	20.		10.	20.
I	1006.	1005.	1009.	1010.	1005.
Reference	Choi, 2003	Couladis, Özcan, et al., 2003	Dudai, Larkov, et al., 2003	Feizbaksh, Saber Tehrani, et al., 2003	Ghasemi, Asghari, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RSL-200	RSL-200	RSL-200	DB-5
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	He	H2	H2	H2	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.32	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	40.	50.
T_end (C)	275.	280.	280.	280.	220.
Heat rate (K/min)	4.	6.	6.	6.	3.
Initial hold (min)		5.	2.	5.	2.
Final hold (min)		5.	10.	5.	10.
I	1003.	998.	1002.	999.	995.
Reference	Ghannadi and Zolfaghari, 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2	Jirovetz, Buchbauer, et al., 2003, 3	Juteau, Jerkovic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	HP-5	OV-101	CP Sil 5 CB
Column length (m)	25.	25.	30.	50.	25.
Carrier gas	He		Helium	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.2	0.25
Phase thickness (μm)	0.25	0.39		0.5	0.15
T_start (C)	35.	60.	70.	50.	50.
T_end (C)	280.	220.	210.	250.	230.
Heat rate (K/min)	5.	5.	2.	2.	3.
Initial hold (min)	2.5
Final hold (min)			60.
I	994.	999.	1003.	995.	995.
Reference	Kanjilal, Kotoky, et al., 2003	Mazloomifar, Saber-Tehrani, et al., 2003	Mookdasanit, Tamura, et al., 2003	Orav, Kailas, et al., 2003	Oyedeji, Ekundayo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	DB-5	DB-1
Column length (m)	50.	30.	30.	30.	60.
Carrier gas	N2	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	60.	60.	75.	40.
T_end (C)	240.	280.	280.	220.	220.
Heat rate (K/min)	4.	4.	3.	3.	4.
Initial hold (min)		10.		4.
Final hold (min)		40.
I	1015.	1005.	990.	1003.	1006.
Reference	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003	Priestap, van Baren, et al., 2003	Rasooli and Mirmostafa, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	HP-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	40.
T_end (C)	230.	275.	280.	280.	260.
Heat rate (K/min)	2.	4.	4.	4.	2.
Initial hold (min)					5.
Final hold (min)
I	1005.	1005.	1006.	1005.	1002.
Reference	Rotman, Ahumada, et al., 2003	Sadraei, Ghannadi, et al., 2003	Sajjadi and Mehregan, 2003	Sajjadi and Mehregan, 2003, 2	Senatore and Bruno, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-1	DB-1	Cross-Linked Methylsilicone
Column length (m)	60.	60.	60.	60.	25.
Carrier gas	He		N2	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	50.	40.	70.	70.	70.
T_end (C)	280.	250.	230.	230.	250.
Heat rate (K/min)	4.	5.	2.	2.	4.
Initial hold (min)		15.	2.	2.
Final hold (min)			20.	20.
I	996.	1009.	1003.	1012.	989.
Reference	Shahmir, Ahmadi, et al., 2003	Stashenko, Jaramillo, et al., 2003	Tu, Onishi, et al., 2003	Tu, Onishi, et al., 2003, 2	Velasco-Negueruela, Pérez-Alonso, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	DB-5	DB-1
Column length (m)	25.	25.	30.	25.	60.
Carrier gas	H2	H2	He	N2	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.53	0.53	0.32	0.25	0.25
T_start (C)	40.	40.	60.	50.	60.
T_end (C)	280.	280.	250.	250.	220.
Heat rate (K/min)	4.	4.	5.	4.	4.
Initial hold (min)			30.
Final hold (min)				10.
I	1003.	989.	1014.	1006.	999.
Reference	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003	Yassa, Akhani, et al., 2003	Zrira, Elamrani, et al., 2003	Baher, Mirza, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-101	DB-5	HP-1	5 % Phenyl methyl siloxane
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.249	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	50.	60.	70.	75.
T_end (C)	300.	200.	280.	220.	200.
Heat rate (K/min)	3.	5.	3.	3.	3.
Initial hold (min)					4.
Final hold (min)	5.		30.	15.	8.
I	1004.	1000.	999.	998.	1003.
Reference	Bos, Koulman, et al., 2002	Boyom, Keumedjio, et al., 2002	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002	Cicció and Gómez-Laurito, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5MS	BP-1	DB-5	HP-5
Column length (m)	60.	30.	25.	30.	30.
Carrier gas	He	He	N2	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.50	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	50.
T_end (C)	200.	280.	220.	250.	250.
Heat rate (K/min)	3.	3.	5.	4.	4.
Initial hold (min)	6.				5.
Final hold (min)			10.
I	1027.	1010.	997.	1005.	1006.
Reference	Cimanga, Apers, et al., 2002	Congiu, Falconieri, et al., 2002	Das, Ram, et al., 2002	Farah, Fechtal, et al., 2002	Farah, Fechtal. M., et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5	SE-30	HP-5
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	70.	50.
T_end (C)	240.	245.	275.	240.	200.
Heat rate (K/min)	3.	3.	4.	4.	3.
Initial hold (min)		20.
Final hold (min)
I	1007.	984.	1003.	1007.	1007.
Reference	Flamini, Ertugrul, et al., 2002	Gancel, Ollé, et al., 2002	Ghannadi, Sajjadi, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Isidorov and Jdanova, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RSL-200	DB-1	DB-5	OV-101
Column length (m)	30.	30.	25.	30.	25.
Carrier gas	H2	H2	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.23	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.20	0.25
T_start (C)	40.	50.	50.	35.	50.
T_end (C)	280.	280.	200.	280.	200.
Heat rate (K/min)	6.	6.	3.	3.	5.
Initial hold (min)	5.	5.	3.	2.
Final hold (min)	5.	5.	30.	15.
I	998.	1001.	1008.	1004.	1000.
Reference	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Ngassoum, et al., 2002	Khallouki, Younos, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002	Kuiate, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	OV-101	DB-1	DB-1
Column length (m)	30.	30.	50.	50.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.5	0.25	0.25
T_start (C)	60.	60.	50.	80.	40.
T_end (C)	250.	240.	250.	225.	280.
Heat rate (K/min)	3.	3.	2.	4.	4.
Initial hold (min)					5.
Final hold (min)
I	989.	1005.	993.	992.	999.
Reference	Limberger, Simões-Pires, et al., 2002	Maia, Zoghbi, et al., 2002	Orav, Kailas, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Sefidkon, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	DB-5MS	DB-5
Column length (m)	50.	50.	60.	30.	30.
Carrier gas	N2	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	60.	50.	60.	60.
T_end (C)	240.	240.	250.	270.	240.
Heat rate (K/min)	4.	3.	4.	3.	3.
Initial hold (min)			5.
Final hold (min)
I	989.	987.	1000.	1005.	1008.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002, 2	Yamini, Sefidkon, et al., 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	DB-1	OV-1	HP-5
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	He	He	H2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.32	0.25
Phase thickness (μm)		0.25	0.25	0.3	0.25
T_start (C)	40.	40.	40.	50.	60.
T_end (C)	220.	280.	280.	250.	220.
Heat rate (K/min)	3.	4.	4.	3.	5.
Initial hold (min)	5.	5.	5.	1.	10.
Final hold (min)	15.			20.
I	1003.	988.	993.	995.	1007.
Reference	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Gallori, Bilia, et al., 2001	Gallori, Flamini, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-1	DB-5	DB-5	DB-1
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	N2	N2	He	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25		0.25
T_start (C)	60.	80.	50.	60.	60.
T_end (C)	300.	225.	250.	285.	240.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)			5.
Final hold (min)
I	998.	991.	1004.	1004.	1009.0
Reference	Kalemba, Marschall, et al., 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Rousis, Papadogianni, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001	Santos, Moreira, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP-Sil 5 CB	HP-5 MS	DB-5	OV-101
Column length (m)	25.	25.	30.	30.	50.
Carrier gas	He	Nitrogen	Helium	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.39	0.39	0.25	0.25
T_start (C)	60.	60.	50.	60.	80.
T_end (C)	220.	220.	250.	240.	200.
Heat rate (K/min)	5.	5.	5.	3.	2.
Initial hold (min)			2.
Final hold (min)			5.
I	998.	998.	1000.	1004.	1002.
Reference	Sayyah, Kamalinejad, et al., 2001	Sayyah, Kamalinejad, et al., 2001, 2	Shang, Hu, et al., 2001	Tellez M., Estell R., et al., 2001	Yang, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	CP Sil 5 CB	SPB-1	DB-1	RSL-200
Column length (m)	50.	25.	30.	30.	60.
Carrier gas	N2		He		H2
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.32
Phase thickness (μm)		0.15	0.2	0.25	0.25
T_start (C)	80.	50.	80.	45.	40.
T_end (C)	200.	230.	300.	300.	250.
Heat rate (K/min)	2.	3.	5.	15.	6.
Initial hold (min)			3.	2.
Final hold (min)				5.
I	1002.	1002.	1007.	1005.	1007.
Reference	Yang, 2001, 2	Asekun and Ekundayo, 2000	Fraternale, Giamperi, et al., 2000	Hedin, McKibben, et al., 2000	Jirovetz, Puschmann, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5	DB-1	OV-101
Column length (m)	30.	25.	30.	30.	50.
Carrier gas	He	Nitrogen	He	He	Nitrogen
Substrate
Column diameter (mm)	0.25	0.50	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	40.
T_end (C)	240.	220.	275.	260.	200.
Heat rate (K/min)	3.	5.	4.	2.	2.
Initial hold (min)				5.	10.
Final hold (min)				2.
I	1006.	997.	1004.	994.	1002.
Reference	Maia, Zoghbi, et al., 2000	Mallavarapu, Rao, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Senatore, Napolitano, et al., 2000	Tamura, Boonbumrung, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	SPB-1	OV-101	DB-1	RTX-1
Column length (m)	25.	50.	52.	60.	30.
Carrier gas	He		Helium	He	N2
Substrate
Column diameter (mm)	0.2	0.2	0.26	0.25	0.25
Phase thickness (μm)		0.33	0.13	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	230.	260.	220.	230.	300.
Heat rate (K/min)	3.	4.	3.	4.	4.
Initial hold (min)			0.
Final hold (min)			0.
I	993.	997.	1000.	1002.	999.
Reference	Ali N.A.M. and Jantan, 1999	Choo, Wong, et al., 1999	Dzumayev, Tkachenko, et al., 1999	Eikani, Goodarznia, et al., 1999	Kalemba, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	SE-30	DB-1	OV-101
Column length (m)	25.	30.	25.	50.	50.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.25	0.25
Phase thickness (μm)	0.25	1.		0.25	0.25
T_start (C)	50.	40.	60.	70.	70.
T_end (C)	290.	200.	230.	240.	220.
Heat rate (K/min)	4.	3.	3.	4.	2.
Initial hold (min)		5.	10.		5.
Final hold (min)
I	1004.	1000.	993.	992.	1001.
Reference	Koulman, 1999	Meynier, Novelli, et al., 1999	Mohd and Jantan, 1999	Palá-Paúl, Pérez-Alonso, et al., 1999	Pateira, Nogueira, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-1	DB-5	DB-1	DB-5
Column length (m)	25.	60.	30.	60.	30.
Carrier gas	N2	He	He	He	H2
Substrate
Column diameter (mm)	0.5	0.25	0.25	0.32	0.32
Phase thickness (μm)		0.25	0.25
T_start (C)	60.	40.	40.	60.	32.
T_end (C)	220.	280.	220.	230.	260.
Heat rate (K/min)	5.	4.	4.	3.	7.
Initial hold (min)		5.	5.		5.
Final hold (min)	10.			5.	5.
I	996.	997.	1000.	999.	1009.
Reference	Rao, Bhattacharya, et al., 1999	Sefidkon, Dabiri, et al., 1999	Sefidkon and Khajavi, 1999	Shafiee, Javidnia, et al., 1999	Sun and Petracek, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	DB-5MS	SPB-5	SE-30
Column length (m)	60.	30.	30.	50.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.32	0.2
Phase thickness (μm)	1.	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	200.	240.	240.	240.	180.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)	5.				10.
Final hold (min)	2.			20.
I	1012.	1006.	1003.	1008.	998.
Reference	Viallon C., Verdier-Metz I., et al., 1999	Zoghbi, Andrade, et al., 1999	Zoghbi, Andrade, et al., 1999, 2	Doneanu and Anitescu, 1998	Jantan, Ahmad, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	OV-101	CP Sil 5 CB	SPB-Sulfur
Column length (m)	30.	60.	25.	25.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.32
Phase thickness (μm)	0.25	0.25		0.25	4.
T_start (C)	60.	50.	50.	60.	45.
T_end (C)	240.	280.	200.	300.	240.
Heat rate (K/min)	3.	4.	5.	6.	5.
Initial hold (min)		5.			13.
Final hold (min)					5.
I	1005.	993.	1001.	993.	1013.
Reference	Maia, Zohhbi, et al., 1998	Stashenko, Cervantes, et al., 1998	Zollo, Biyiti, et al., 1998	Bos, Woerdenbag, et al., 1997	Mariaca, Berger, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-Sulfur	DB-1	DB-5	DB-5	HP-1
Column length (m)	30.		30.	30.	23.
Carrier gas	He		Helium	He	He
Substrate
Column diameter (mm)	0.32		0.25	0.25	0.32
Phase thickness (μm)	4.		0.25		0.17
T_start (C)	45.	80.	60.	60.	60.
T_end (C)	240.	220.	240.	240.	250.
Heat rate (K/min)	5.	6.	3.	4.	5.
Initial hold (min)	13.				3.
Final hold (min)	5.				30.
I	1013.	1000.	1004.	1005.	994.
Reference	Mariaca, Berger, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Zunino, Novillo-Newton, et al., 1997	Ayedoun, Adeoti, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-101	BP-1	BP-1	BP-1
Column length (m)	30.	50.	25.	25.	25.
Carrier gas		He	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.50	0.50	0.50
Phase thickness (μm)	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	300.	250.	220.	220.	220.
Heat rate (K/min)	4.	2.	5.	5.	5.
Initial hold (min)	2.
Final hold (min)	5.
I	1007.1	995.	1000.	997.	997.
Reference	Gawdzik, Mardarowicz, et al., 1996	Orav, Kailas, et al., 1996	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SPB-1	OV-101	DB-1	DB-1
Column length (m)	60.	50.	50.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.5	0.25	0.25
T_start (C)	50.	40.	70.	70.	70.
T_end (C)	250.	200.	180.	270.	270.
Heat rate (K/min)	2.5	3.	1.	2.5	2.5
Initial hold (min)	5.	3.		5.	5.
Final hold (min)		30.
I	992.	994.	995.	994.	994.
Reference	Stashenko, Puertas, et al., 1996	Wong and Lai, 1996	Orav, Kuningas, et al., 1995	Tirado, Stashenko, et al., 1995	Tirado, Stashenko, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	HP-101	Methyl Silicone	Methyl Silicone	CP Sil 5 CB
Column length (m)	50.	50.	50.	50.	25.
Carrier gas	N2	H2	N2	N2
Substrate
Column diameter (mm)	0.27	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.2	0.3	0.17	0.17
T_start (C)	80.	65.	80.	80.	60.
T_end (C)	240.	300.	200.	200.	280.
Heat rate (K/min)	3.	2.	2.	3.	5.
Initial hold (min)		5.
Final hold (min)
I	1000.	997.	1002.	990.	999.
Reference	Ramanoelina, Viano, et al., 1994	Demarne and van der Walt, 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Kaul, Singh, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	SPB-5	SE-54	DB-1	DB-1
Column length (m)	25.	30.	30.	30.	60.
Carrier gas			Hydrogen	N2
Substrate
Column diameter (mm)	0.50		0.25		0.32
Phase thickness (μm)		1.0	0.25
T_start (C)	60.	50.	60.	80.	50.
T_end (C)	220.	250.	250.	220.	230.
Heat rate (K/min)	5.	8.	2.	4.	4.
Initial hold (min)			5.
Final hold (min)			2.		10.
I	1000.	1002.	1002.	996.	996.
Reference	Mallavarapu, Ramesh, et al., 1993	King and Knight, 1992	Kollmannsberger, Nitz, et al., 1992	Velasco-Negueruela, Pérez Alonso, et al., 1991	Binder, Benson, et al., 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 8 CB	BP-1	OV-101	OV-101	BP-1
Column length (m)	25.	25.	50.	50.	50.
Carrier gas			N2	N2	H2
Substrate
Column diameter (mm)	0.20	0.33	0.25	0.25	0.30
Phase thickness (μm)
T_start (C)	60.	45.	80.	80.	40.
T_end (C)	230.	180.	200.	200.	250.
Heat rate (K/min)	3.	3.	2.	2.	10.
Initial hold (min)	10.	3.			1.
Final hold (min)
I	1007.	988.	1003.	1005.	998.
Reference	Jantan and Goh, 1990	Wyllie, Brophy, et al., 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990	Brophy, Davies, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	OV-101	OV-101	OV-101	DB-1
Column length (m)	40.	50.	50.	50.	60.
Carrier gas	He	N2	N2	N2	He
Substrate
Column diameter (mm)	0.50	0.25	0.25	0.25	0.315
Phase thickness (μm)	0.75				0.25
T_start (C)	30.	80.	80.	80.	50.
T_end (C)	220.	200.	200.	200.	250.
Heat rate (K/min)	3.	2.	2.	2.	4.
Initial hold (min)
Final hold (min)
I	993.	1003.	1004.	1005.	996.
Reference	de Pooter, de Buyck, et al., 1989	Sugisawa, Yamamoto, et al., 1989	Sugisawa, Yang, et al., 1989	Sugisawa, Yang, et al., 1989	Engel, Flath, et al., 1988
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-1	OV-1	OV-101	OV-101
Column length (m)	50.	40.		30.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.30	0.5		0.5	0.5
Phase thickness (μm)		0.75		0.8	0.8
T_start (C)	40.	30.	40.	40.	40.
T_end (C)	230.	220.	220.	220.	220.
Heat rate (K/min)	3.5	3.	2.	2.	2.
Initial hold (min)	5.
Final hold (min)
I	994.	994.	992.	993.	993.
Reference	Nykanen, 1986	de Pooter, de Buyck, et al., 1986	De Pooter, De Buyck, et al., 1986	De Pooter and Schamp, 1986	De Pooter and Schamp, 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary
Active phase	SE-30+Igepal	SE-30+Igepal
Column length (m)	100.	100.
Carrier gas
Substrate
Column diameter (mm)	0.25	0.25
Phase thickness (μm)
T_start (C)	70.	70.
T_end (C)	170.	170.
Heat rate (K/min)	1.	1.
Initial hold (min)
Final hold (min)
I	1002.	1005.
Reference	Shibamoto and Jennings, 1977	Shibamoto and Jennings, 1977
Comment	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Sefidkon, F.; Khajavi, M.S., Chemical composition of the essential oils of two Salvia species from Iran: Salvia verticillata L. and Salvia santolinifolia Boiss., Flavour Fragr. J., 1999, 14, 2, 77-78, https://doi.org/10.1002/(SICI)1099-1026(199903/04)14:2<77::AID-FFJ726>3.0.CO;2-9 . [all data]

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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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