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Carveol


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-1HP-5Methyl SiliconeOV-1
Column length (m) 30.60.50.25.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.20.5
Phase thickness (mum) 0.250.250.250.30.8
Tstart (C) 50.50.50.40.40.
Tend (C) 260.250.250.200.220.
Heat rate (K/min) 2.2.52.52.2.
Initial hold (min) 3.5.5.  
Final hold (min) 5.    
I 1188.1201.1217.1222.1196.
ReferenceDob T., Berramdane T., et al., 2005Guilliard, Delgado, et al., 2001Guilliard, Delgado, et al., 2001Píry, Príbela, et al., 1995De Pooter, Omar, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1
Column length (m) 30.30.30.
Carrier gas HeHeHe
Substrate    
Column diameter (mm) 0.50.50.5
Phase thickness (mum) 0.80.80.8
Tstart (C) 40.40.40.
Tend (C) 220.220.220.
Heat rate (K/min) 2.2.2.
Initial hold (min)    
Final hold (min)    
I 1202.1208.1217.
ReferenceDe Pooter, Omar, et al., 1985De Pooter, Omar, et al., 1985De Pooter, Omar, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Dob T., Berramdane T., et al., 2005
Dob T.; Berramdane T.; Chelghoum C., Analysis of essential oil from the needles of Pinus pinaster growing in Algeria, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 5, 545-548, https://doi.org/10.1007/s10600-005-0202-z . [all data]

Guilliard, Delgado, et al., 2001
Guilliard, M.; Delgado, W.; Martínez, J.R.; Stashenko, E., Determination of the enantiomeric purity of carvone, main component of Colombian Lippia alba (Mill) oil by means of bidimensional gas chromatography (23rd International Symposium on Capillary Chromatography), 2001, retrieved from http://www.richrom.com/assets/CD23PDF/i01.pdf. [all data]

Píry, Príbela, et al., 1995
Píry, J.; Príbela, A.; Durcanská, J.; Farkas, P., Fractionation of volatiles from blackcurrant (Ribes nigrum L.) by different extractive methods, Food Chem., 1995, 54, 1, 73-77, https://doi.org/10.1016/0308-8146(95)92665-7 . [all data]

De Pooter, Omar, et al., 1985
De Pooter, H.L.; Omar, M.N.; Coolsaet, B.A.; Schamp, N.M., The Essential Oil of Greater Galanga (Alpinia Galanga) from Malaysia, Phytochemistry, 1985, 24, 1, 93-96, https://doi.org/10.1016/S0031-9422(00)80814-6 . [all data]


Notes

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