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Acetophenone

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryPackedPackedPacked
Active phase OV-101SE-30OV-101OV-101OV-101
Column length (m) 50.40.5.5.5.
Carrier gas He N2N2N2
Substrate   Chromosorb G HPChromosorb G HPChromosorb G HP
Column diameter (mm) 0.30.35   
Phase thickness (mum) 0.40.35   
Temperature (C) 110.100.100.110.80.
I 1077.1038.41033.41040.21028.3
ReferenceTerenina, Zhuravieva, et al., 1997Tudor, 1997Righezza, Hassani, et al., 1996Righezza, Hassani, et al., 1996Righezza, Hassani, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 5.5.5.5.5.
Carrier gas N2N2N2N2N2
Substrate Chromosorb G HPChromosorb G HPChromosorb G HPChromosorb G HPChromosorb G HP
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 90.120.130.140.120.
I 1030.51043.11044.71058.51043.1
ReferenceRighezza, Hassani, et al., 1996Righezza, Hassani, et al., 1996Righezza, Hassani, et al., 1996Righezza, Hassani, et al., 1996Hassani and Meklati, 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase OV-101OV-101SE-30SE-30SE-30
Column length (m) 5.2.3.1.1.
Carrier gas N2N2Ar  
Substrate Chromosorb G HPChromosorb G HPGas Chrom Q (80-100 mesh)Chromaton N-AW-GMDSChromaton N-AW-GMDS
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 160.150.150.150.160.
I 1066.11060.31065.1049.1047.
ReferenceHassani and Meklati, 1992Maeck, Touabet, et al., 1989Tiess, 1984Vylegzhanina and Keiser, 1976Vylegzhanina and Keiser, 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPacked
Active phase SE-30SE-30Apiezon L
Column length (m) 2.2.2.25
Carrier gas N2N2 
Substrate Chromosorb W-AWChromosorb W-AWCelite
Column diameter (mm)    
Phase thickness (mum)    
Temperature (C) 150.170.130.
I 1068.1076.1067.
ReferenceTibor and Anna, 1971Tibor and Anna, 1971Wehrli and Kováts, 1959
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Terenina, Zhuravieva, et al., 1997
Terenina, M.B.; Zhuravieva, I.L.; Golovnya, R.V., Peculiar features of sorption of positional isomers of formyl-, acetyl-, and aminopyridines in capillary gas-liquid chromatography, Russ. Chem. Bull. (Engl. Transl.), 1997, 46, 1, 86-89, https://doi.org/10.1007/BF02495353 . [all data]

Tudor, 1997
Tudor, E., Temperature dependence of the retention index for perfumery compounds on a SE-30 glass capillary column. I. Linear equations, J. Chromatogr. A, 1997, 779, 1-2, 287-297, https://doi.org/10.1016/S0021-9673(97)00453-6 . [all data]

Righezza, Hassani, et al., 1996
Righezza, M.; Hassani, A.; Meklati, B.Y.; Chrétien, J.R., Quantitative structure-retention relationships (QSRR) of congeneric aromatics series studied on phenyl OV phases in gas chromatography, J. Chromatogr. A, 1996, 723, 1, 77-91, https://doi.org/10.1016/0021-9673(95)00816-0 . [all data]

Hassani and Meklati, 1992
Hassani, A.; Meklati, B.Y., Gas chromatographic behaviour of monosubstituted benzenes, benzaldehydes and acetophenones on OV polymethylphenyl-silicone stationary phases, Chromatographia, 1992, 33, 5/6, 267-271, https://doi.org/10.1007/BF02276193 . [all data]

Maeck, Touabet, et al., 1989
Maeck, M.; Touabet, A.; Badjah Hadj Ahmed, A.Y.; Meklati, B.Y., A numerical interpolation of Kováts indices without dead time correction, Chromatographia, 1989, 27, 5/6, 205-208, https://doi.org/10.1007/BF02260447 . [all data]

Tiess, 1984
Tiess, D., Gaschromatographische Retentionsindices von 125 leicht- bis mittelflüchtigen organischen Substanzen toxikologisch-analytischer Relevanz auf SE-30, Wiss. Z. Wilhelm-Pieck-Univ. Rostock Math. Naturwiss. Reihe, 1984, 33, 6-9. [all data]

Vylegzhanina and Keiser, 1976
Vylegzhanina, G.F.; Keiser, L.S., Determination of the heats of solution of the insecticide gardona and its metabolites in the stationary phase and their Kovats retention indices, Zh. Anal. Khim., 1976, 31, 1, 171-173. [all data]

Tibor and Anna, 1971
Tibor, T.; Anna, B., Gázkromatográfiás retenció és a kémiai szerkezet, I., Magy. Kem. Foly., 1971, 77, 576-587. [all data]

Wehrli and Kováts, 1959
Wehrli, A.; Kováts, E., Gas-chromatographische Charakterisierung ogranischer Verbindungen. Teil 3: Berechnung der Retentionsindices aliphatischer, alicyclischer und aromatischer Verbindungen, Helv. Chim. Acta, 1959, 7, 7, 2709-2736, https://doi.org/10.1002/hlca.19590420745 . [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References