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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-1RTX-1RTX-1
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.230.240.230.230.
Heat rate (K/min) 4.3.3.2.2.
Initial hold (min) 3.    
Final hold (min) 15.  5.5.
I 1189.1200.1184.1176.1176.
ReferenceBertuzzi, Tirillini, et al., 2013Pripdeevech and Saansoomchai, 2013Alizadeh and Shaabani, 2012Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSPolydimethyl siloxane with 5 % PhDP-5DP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 100.40.80.80.80.
Tend (C) 260.250.200.300.300.
Heat rate (K/min) 10.3.5.4.4.
Initial hold (min) 1.1. 1.1.
Final hold (min) 10.3.25.40.40.
I 1197.1190.1187.1143.1143.
ReferenceBoukhris, Bouaziz, et al., 2012Jian-Yu, Zhu, et al., 2012Priya, Prathapan, et al., 2012Vijayakumar, Duraipandiyan, et al., 2012Vijayakumar, Duraipandiyan, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5 MSHP-1CP-Sil 5 CBHP-5
Column length (m) 60.30.30.25.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (mum) 0.250.250.250.150.25
Tstart (C) 60.50.60.50.60.
Tend (C) 230.250.240.220.240.
Heat rate (K/min) 2.7.3. 3.
Initial hold (min)  1.   
Final hold (min) 45.5.   
I 1167.1189.1177.1188.1189.
ReferenceYapi, Boti, et al., 2012Zouari, Ayadi, et al., 2012Alizadeh, Khosh-Khui, et al., 2011Ameen, Usman, et al., 2011Bertoli, Lepnardi, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSHP-5VF-5 MSVF-5 MS
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.50.60.30.30.
Tend (C) 210.180.240.260.260.
Heat rate (K/min) 5.2.3.2.2.
Initial hold (min)   2.  
Final hold (min)    28.28.
I 1192.1188.1190.1197.1198.
ReferenceFathi, Sahari, et al., 2011Hammami, Kamoun, et al., 2011Kahriman, Tosun, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30 MSHP-5 MSCP-Sil 5 CBMethylsiloxane + 5 % Ph-groupsDB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeliumNitrogenHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.260.250.32
Tstart (C) 50.40.45.60.60.
Tend (C) 250.260.280.230.220.
Heat rate (K/min) 5.4.3.7.5.
Initial hold (min) 5.  2.3.
Final hold (min) 10.5.22.20.5.
I 1189.1195.1177.1189.1190.
ReferenceMenichini, Tundis, et al., 2011Miyazawa, Marumoto, et al., 2011Mothana, Hasson, et al., 2011Nadim, Malik, et al., 2011Salimi, Shafaghat, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5ZB-5 MSZB-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.252
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 280.300.290.290.240.
Heat rate (K/min) 5.50.5.5.3.
Initial hold (min) 1.5.   
Final hold (min) 1.5.   
I 1185.1193.1194.1198.1189.
ReferenceTekaya-Karoui, Boughalleb, et al., 2011Bi Kouame, Bedi, et al., 2010Boix, Victorio, et al., 2010Boix, Victorio, et al., 2010Cavar, Maksimovic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-5 MSOV-1DB-5OV-1
Column length (m) 25.25.50.30.30.
Carrier gas HeliumHelium HeliumHelium
Substrate      
Column diameter (mm) 0.300.300.320.250.25
Phase thickness (mum) 0.250.250.500.250.25
Tstart (C) 50.50.40.50.50.
Tend (C) 240.240.270.250.250.
Heat rate (K/min) 3.3.2.2.5.
Initial hold (min)     3.
Final hold (min)   10. 2.
I 1198.1198.1177.1189.1172.
ReferenceChalchat, Figueredo, et al., 2010Chalchat, Figueredo, et al., 2010Da Costa, Yang, et al., 2010Ho, Wang, et al., 2010Hu, Liang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSBP-1HP-5SPB-1
Column length (m) 30.30. 30.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.320.25 0.250.20
Phase thickness (mum) 0.250.25 0.250.20
Tstart (C) 60.70.60.40.70.
Tend (C) 240.290.220.260.220.
Heat rate (K/min) 3.5.5.4.3.
Initial hold (min) 2. 10.  
Final hold (min)   30.5.15.
I 1190.1196.1176.1190.1168.
ReferenceKahriman, Tosun, et al., 2010Lazarevic, Radulovic, et al., 2010Mishra, Chaudhary, et al., 2010Miyazawa, Kawauchi, et al., 2010Neves, Rosa, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5 MSHP-5 MSSLB-5 MS
Column length (m) 30.30.30.30.10.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.10
Phase thickness (mum) 0.250.250.250.250.10
Tstart (C) 50.70.70.60.50.
Tend (C) 240.290.290.220.250.
Heat rate (K/min) 4.5.5.6.10.
Initial hold (min) 2.  3. 
Final hold (min) 10.10.10.  
I 1190.1196.1199.1178.1195.
ReferencePino, Marquez, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Safaei-Ghomi and Batooli, 2010Scandinaro, Tranchida, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSDB-5DB-1-MSCP Sil 5 CBDB-5
Column length (m) 10.30.60.25.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.100.250.250.250.25
Phase thickness (mum) 0.100.250.250.150.25
Tstart (C) 50.40.30.50.80.
Tend (C) 250.240.200.230.240.
Heat rate (K/min) 10.3.2.3.3.
Initial hold (min)  1.4.  
Final hold (min)   35. 2.
I 1196.1152.1168.1188.1195.
ReferenceScandinaro, Tranchida, et al., 2010de Souza, Lopes, et al., 2010Takeoka, Hobbs, et al., 2010Usman, Zubair, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5MSDB-5SE-54
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.50.60.60.
Tend (C) 220.250.250.240.260.
Heat rate (K/min) 4.10.7.3.2.
Initial hold (min) 2.1.1. 5.
Final hold (min) 2.3.5. 999.
I 1168.1187.1200.1189.1187.
ReferenceXu, Tang, et al., 2010Yang, Zhang, et al., 2010Zouari, Zouari, et al., 2010Alim, Goze, et al., 2009Dayisoylu and Alma, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSSPB-5DB-5DB-5DB-5 MS
Column length (m) 30.60.30.50.30.
Carrier gas HeliumNitrogenHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.350.250.200.25
Phase thickness (mum) 0.250.250.250.320.25
Tstart (C) 60.60.50.60.50.
Tend (C) 250.230.250.220.250.
Heat rate (K/min) 2.4.5.5.2.
Initial hold (min) 8. 2.3.5.
Final hold (min) 15.40.   
I 1204.1197.1189.1189.1207.
ReferenceFarhat, Ginies, et al., 2009Gauvin-Bialecki and Marodon, 2009Ho, Wang, et al., 2009Kazemi and Akhavani, 2009Koba, Sanda, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5RTX-1RTX-1BP-1
Column length (m) 60.25.60.60.50.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.200.220.220.22
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 250.240.230.230.220.
Heat rate (K/min) 3.3.2.2.2.
Initial hold (min)      
Final hold (min)  7.30.30.20.
I 1196.1188.1176.1179.1169.
ReferenceMales, Plazibat, et al., 2009Maridass, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Ottavioli, Bighelli, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-5HP-5 MSDB-55 % Phenyl methyl siloxane
Column length (m) 60.30.30.30.60.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.45.70.40.90.
Tend (C) 330.250.290.250.225.
Heat rate (K/min) 2.3.5.3.3.
Initial hold (min) 12.3. 1. 
Final hold (min) 30.5.10.10.3.
I 1186.1196.1196.1176.1188.
ReferencePatil, Jayaprakasha, et al., 2009Porto, Decorti, et al., 2009Radulovic, Blagojevic, et al., 2009Rahmi-Nasrabadi, Gholivand, et al., 2009Retta, Gattuso, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Mega 5 MSDB-5DB-1 MSDB-5DB-5
Column length (m) 60.30.30.50.30.
Carrier gas HeliumNitrogenHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (mum) 0.250.250.250.320.25
Tstart (C) 40.40.40.60.40.
Tend (C) 240.230.250.220.240.
Heat rate (K/min) 3.2.6.5.3.
Initial hold (min) 2. 1.3.1.
Final hold (min)   4.5. 
I 1179.1189.1170.1189.1152.
ReferenceRomeo, Verzera, et al., 2009Scrivanti, Anton, et al., 2009Seo, Kim, et al., 2009Shafaghat and Sadeghi, 2009de Souza, Lopes, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5 MSHP-5 MSHP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 50.60.50.50.70.
Tend (C) 240.325.280.280.220.
Heat rate (K/min) 5.10.4.9.3.
Initial hold (min)  6. 3.1.
Final hold (min)  10. 3. 
I 1189.1191.1192.1189.1177.
ReferenceWannes, Mhamdi, et al., 2009Zaibunnisa, Norashikin, et al., 2009Zhao, Zeng, et al., 2009Aicha, Ines, et al., 2008Awadi Ali, Wurster, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Ultra 2HP-5HP-5 MSSPB-1
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeliumN2HeliumHelium
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (mum) 0.250.110.250.251.0
Tstart (C) 60.60.60.50.60.
Tend (C) 220.230.220.230.250.
Heat rate (K/min) 3.2.5.4.5.
Initial hold (min)  5.10.4.5.
Final hold (min)  30. 10. 
I 1189.1189.1190.1190.1181.
ReferenceBastos, Ishimoto, et al., 2008Byun and Shin, 2008Flamini, Tebano, et al., 2008Forero, Quijano, et al., 2008Frerot, Velluz, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1SLB-5 MSZB-1DB-5
Column length (m) 30.30.30.30.60.
Carrier gas NitrogenHeHeliumNitrogenNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.30.50.45.60.
Tend (C) 240.210.250.230.250.
Heat rate (K/min) 3.5.3.3.5.
Initial hold (min) 1. 2.  
Final hold (min) 9. 10. 10.
I 1197.1183.1195.1166.1198.
ReferenceJardin, Jham, et al., 2008Kumazawa, Itobe, et al., 2008Lo Presti, Sciarrone, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Mosayebi, Amin, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSRTX-1Elite-1HP-5 MSHP-5 MS
Column length (m) 30.60.30.30.30.
Carrier gas HeliumHeHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.50.
Tend (C) 300.230.246.250.240.
Heat rate (K/min) 5.2.3.2.3.
Initial hold (min) 5.  8. 
Final hold (min) 5.35. 15. 
I 1191.1172.1190.1189.1189.
ReferenceNoudogbessi, Yedomonhan, et al., 2008Paolini, Tomi, et al., 2008Raj, Baby, et al., 2008Sahraoui, Vian, et al., 2008Sarikurkcu, Tepe, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5HP-5DB-5 MSOV-1HP-5
Column length (m) 7.525.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.100.250.250.250.25
Phase thickness (mum) 10.0.250.250.250.32
Tstart (C) 60.60.60.65.60.
Tend (C) 240.240.270.260.250.
Heat rate (K/min) 3.4.3.6.5.
Initial hold (min)  2.  30.
Final hold (min)      
I 1217.1190.1200.1196.1186.
ReferenceShellie, 2008Verdian-rizi, 2008Victorio, Alviano, et al., 2008Wang, Yi, et al., 2008Yassa and Akhani, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5HP-5DB-5CP Sil 5 CB
Column length (m) 30.50.30.50.30.
Carrier gas HeliumNitrogenHeHeN2
Substrate      
Column diameter (mm) 0.250.200.250.320.32
Phase thickness (mum) 0.250.32 0.250.25
Tstart (C) 50.60.70.50.60.
Tend (C) 230.220.240.280.300.
Heat rate (K/min) 3.5.5.5.4.
Initial hold (min) 10.3. 2. 
Final hold (min) 10.5. 10. 
I 1189.1192.1195.1201.1177.
ReferenceAdams, Beauchamp, et al., 2007Amiri, 2007Asekun, Olusegun, et al., 2007Baranauskiene R., Bylaite E., et al., 2007Baran, von Reuss, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5DB-5DB-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.260.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.40.70.
Tend (C) 240.280.240.220.310.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min)   1. 5.
Final hold (min)   4. 20.
I 1189.1188.1189.1196.1170.
ReferenceBos, Woerdenbag, et al., 2007Bozin B., Mlmica-Dukic N., et al., 2007Cheraif, Ben Jannet, et al., 2007Chyau, Tsai, et al., 2007Coelho, Grosso, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5HP-5MSZP-5DB-1
Column length (m) 30.30.30.60.60.
Carrier gas HeHeliumHeHeNitrogen
Substrate      
Column diameter (mm) 0.250.260.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 240.290.250.260.250.
Heat rate (K/min) 3.3.2.6.4.
Initial hold (min)   8.7.1.
Final hold (min)   15.1.10.
I 1189.1189.1187.1202.1178.
ReferenceDa Silva J.K.R., Sousa P.J.C., et al., 2007Elfami, Bos, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Füssel, Dötterl, et al., 2007Ghasempour, Shirinpour, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Col-Elite 5MSRTX-5 MSDB-5SE-30
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 1.00.250.250.250.25
Tstart (C) 35.30.45.60.40.
Tend (C) 240.246.210.300.250.
Heat rate (K/min) 15.3.3.3.5.
Initial hold (min) 7.   5.
Final hold (min) 10.   10.
I 1195.1190.1189.1181.1189.
ReferenceGogus, Ozel, et al., 2007Gudaityte and Venskutonis R.P., 2007Hudaib and Aburjai, 2007Limberger, Scopel, et al., 2007Loizzo, Tundis, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5MSAT-5ZB-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 250.240.280.260.220.
Heat rate (K/min) 5.3.3.4.4.
Initial hold (min) 5.   5.
Final hold (min) 10. 30. 20.
I 1183.1187.1163.1193.1190.
ReferenceLoizzo, Tundis, et al., 2007Machado, Bastos, et al., 2007Marongiu B., Piras A., et al., 2007Meccia, Rojas, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5HP-5Methyl Silicone
Column length (m) 30.30.30.25.50.
Carrier gas HeliumHeliumHeliumH2Helium
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.250.33 
Tstart (C) 50.60.60.60.50.
Tend (C) 260.300.220.240.240.
Heat rate (K/min) 2.53.4.3.3.
Initial hold (min) 1.    
Final hold (min) 20.    
I 1165.1161.1191.1192.1195.
ReferenceMonser-Esfahani, Karamkhani, et al., 2007Moreno, Lima, et al., 2007Morteza-Semnani, Saeedi, et al., 2007Oliveira, Leitão, et al., 2007Ozcan and Chalchat, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5 MSSPB-1SPB-5
Column length (m) 50.25.25.30.30.
Carrier gas HeHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.320.250.20.25
Phase thickness (mum) 0.250.520.250.20.25
Tstart (C) 95.40.100.70.50.
Tend (C) 240.280.280.220.250.
Heat rate (K/min) 4.4.4.3.2.
Initial hold (min)   3.  
Final hold (min)   5.15. 
I 1183.1190.1198.1169.1190.
ReferencePala-Paul, Brophy, et al., 2007Pavlovic, Petrovic, et al., 2007Phutdhawong, Kawaree, et al., 2007Pinto, Salgueiro, et al., 2007Raal, Orav, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSDB-1DB-5RTX-5
Column length (m) 60.60.60.30.10.
Carrier gas NitrogenHydrogenHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.18
Phase thickness (mum) 0.250.250.250.250.2
Tstart (C) 60.60.60.50.40.
Tend (C) 250.260.250.240.275.
Heat rate (K/min) 4.4.5.4.50.
Initial hold (min) 1.   0.5
Final hold (min) 10.20.  0.5
I 1178.1191.1178.1188.1210.
ReferenceReza, Ebrahim, et al., 2007Rojas, Velasco, et al., 2007Salehi, Fakhari, et al., 2007Sefidkon, Abbasi, et al., 2007Setkova, Risticevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas He  HeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.25  
Tstart (C) 60.40.40.60.60.
Tend (C) 320.210.250.200.200.
Heat rate (K/min) 10.2.2.2.2.
Initial hold (min)      
Final hold (min) 4.33.33.20.20.
I 1202.1187.1188.1180.1189.
ReferenceSmelcerovic, Spiteller, et al., 2007Sylvestre, Longtin, et al., 2007Sylvestre, Pichette, et al., 2007Tiwary, Nail, et al., 2007Tiwary, Nail, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5 MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeliumHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.40.
Tend (C) 280.280.280.250.240.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min)    5.3.
Final hold (min)    10.10.
I 1193.1153.1189.1186.1194.
ReferenceTsokou, Georgopoulos, et al., 2007Tzakou, Bazos, et al., 2007Vagionas, Graikou, et al., 2007Vichi, Riu-Aumatell, et al., 2007Wenguang, Wenlai, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-5ZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2He 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.320.250.250.250.25
Tstart (C) 60.50.50.60.40.
Tend (C) 250.280.280.300.300.
Heat rate (K/min) 5.9.9.3.2.
Initial hold (min) 30.3.3.  
Final hold (min)  3.3.  
I 1186.1192.1196.1181.1193.
ReferenceYassa and Akhani, 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Apel, Sobral, et al., 2006Biondi, Sari, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-5BP-1HP-5MSHP-1HP-1
Column length (m) 60.50.30.50.50.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.20.2
Phase thickness (mum) 0.250.250.250.50.33
Tstart (C) 60.60.60.60.60.
Tend (C) 200.220.280.250.250.
Heat rate (K/min) 4.2.3.2.2.
Initial hold (min)     4.
Final hold (min) 20.20. 120.30.
I 1191.1172.1188.1169.1169.
ReferenceBorges, Rojas, et al., 2006Boti, Yao, et al., 2006Bozin, Mimicá-Dukic, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-1DB-5HP-5DB-5
Column length (m) 30.60.30.30.30.
Carrier gas HeliumNitrogenN2He 
Substrate      
Column diameter (mm) 0.200.250.250.320.32
Phase thickness (mum) 0.20 0.250.250.25
Tstart (C) 70.40.70.60.60.
Tend (C) 220.200.230.246.230.
Heat rate (K/min) 3.2.2.3.3.
Initial hold (min)  1.2.  
Final hold (min) 15.9.20. 15.
I 1169.1169.1184.1190.1189.
ReferenceCavaleiro, Pinto, et al., 2006Chen, Sheu, et al., 2006Choi, 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Damjanovic, Skala, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5BP-1BP-1HP-5MS
Column length (m) 30.30.50.50.30.
Carrier gas  HeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.260.220.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 280.290.220.220.250.
Heat rate (K/min) 4.3.2.2.2.
Initial hold (min)      
Final hold (min)   20.20. 
I 1193.1189.1172.1172.1189.
ReferenceEbrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006Fanciullino, Tomi, et al., 2006Fanciullino, Tomi, et al., 2006Farah, Afifi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5HP-1DB-1CP Sil 5 CB
Column length (m) 50.30.50.60.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.20.250.20.250.25
Phase thickness (mum) 0.330.250.330.250.25
Tstart (C) 60.50.60.60.40.
Tend (C) 250.300.250.250.220.
Heat rate (K/min) 2.5.2.5.3.
Initial hold (min)  5.   
Final hold (min) 60.5.40.10.3.
I 1176.1195.1171.1178.1199.
ReferenceFernandez, Pintaric, et al., 2006Figuérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006Hadian, Sonboli, et al., 2006Hymete, Rohloff, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5DB-1DB-1
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHe  
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.100.70.70.
Tend (C) 260.260.240.230.230.
Heat rate (K/min) 3.5.5.2.2.
Initial hold (min)  2.2.2.2.
Final hold (min)  13.5.20.20.
I 1192.1196.1189.1172.1173.
ReferenceJavidnia, Miri, et al., 2006Kucuk, Gulec, et al., 2006Lago, Soares, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101CP Sil 8 CBCP Sil 5 CBCP Sil 5 CBHP-5 MS
Column length (m) 25.30.30.30.30.
Carrier gas He N2N2Nitrogen
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 100.40.50.50.50.
Tend (C) 250.250.300.200.280.
Heat rate (K/min) 8.3.4.5.5.
Initial hold (min)  5.   
Final hold (min)  20.  5.
I 1183.1197.1179.1182.1198.
ReferenceLattoo, Dhar, et al., 2006Li, Lee, et al., 2006Lis and Milczarek, 2006Martin, Joseph, et al., 2006Marzouk, Mansour, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-55 % Phenyl methyl siloxaneHP-101DB-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas N2HeliumHeHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.20.250.32
Phase thickness (mum) 0.520.250.20.250.25
Tstart (C) 50.60.70.50.40.
Tend (C) 280.280.200.250.240.
Heat rate (K/min) 5.3.3.3.4.
Initial hold (min)   2.5. 
Final hold (min) 5.30.15. 5.
I 1198.1163.1188.1188.1192.
ReferenceMarzouk, Neffati, et al., 2006Marongiu, Piras, et al., 2006Mastelic, Jerkovic, et al., 2006Mirza, Navaei, et al., 2006Miyazawa and Kawata, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5DB-5DB-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.30.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 220.220.220.260.220.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min) 2. 5.4.5.
Final hold (min) 10.    
I 1185.1191.1192.1192.1191.
ReferenceMoody, Gundidza, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani K., Akbarzadeh M., et al., 2006Morteza-Semnani, Saeedi, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBNB-30DB-5DB-5DB-1
Column length (m) 25.30.25.30.50.
Carrier gas HydrogenHeN2HeN2
Substrate      
Column diameter (mm) 0.250.20.250.320.25
Phase thickness (mum) 0.150.250.150.250.25
Tstart (C) 50.50.50.60.95.
Tend (C) 230.250.200.280.240.
Heat rate (K/min) 3.2.4.5.4.
Initial hold (min)   3.0.5 
Final hold (min)    2. 
I 1178.1177.1198.1195.1180.
ReferenceOlawore, Usman, et al., 2006Orav, Raal, et al., 2006Ouamba, Ouabonzi, et al., 2006Ozel, Gogus, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHydrogenHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.70.70.70.
Tend (C) 220.250.280.280.280.
Heat rate (K/min) 5.4.4.4.4.
Initial hold (min) 10.2.4.4.4.
Final hold (min)  20.   
I 1189.1189.1188.1185.1189.
ReferencePintore G., Chessa M., et al., 2006Pino, Marquez, et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.50.60.60.
Tend (C) 280.280.250.200.260.
Heat rate (K/min) 4.3.10.2.5.
Initial hold (min) 2. 5.  
Final hold (min) 10.  60. 
I 1189.1154.1192.1194.1195.
ReferencePino, Sauri-Duch, et al., 2006Pitarokili, Tzakou, et al., 2006Robinson, 2006Rout, Naik, et al., 2006Sabulal, Dan, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSZB-5DB-1FSOT-RSL-200DB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHe HydrogenHe
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.70.40.40.
Tend (C) 243.300.230.280.240.
Heat rate (K/min) 3.2.2.6.4.
Initial hold (min)   2.5. 
Final hold (min)   20.5. 
I 1190.1193.1174.1188.1189.
ReferenceSabulal, Dan, et al., 2006, 2Sari M., Biondi D.M., et al., 2006Sawamura, Onishi, et al., 2006Schmidt, Jirovetz, et al., 2006Sefidkon and Jamzad, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSHP-5DB-5DB-1
Column length (m) 60.30.25.30.60.
Carrier gas HeHeN2HeHelium
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum)  0.250.330.250.25
Tstart (C) 40.60.30.40.60.
Tend (C) 250.280.280.250.250.
Heat rate (K/min) 4.3.3.4.5.
Initial hold (min)  5. 2. 
Final hold (min)    10.10.
I 1169.1190.1197.1210.1175.
ReferenceSefidkon, Jamzad, et al., 2006Setzer, Noletto, et al., 2006Shafi, Jose, et al., 2006Shen X., Gao Y., et al., 2006Sonboli, Mirjalili, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5Methyl SiliconeDB-5DB-1HP-5
Column length (m)  25.30.50.30.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm)  0.30.250.250.25
Phase thickness (mum)  0.150.250.250.25
Tstart (C) 50.50.60.90.60.
Tend (C) 250.210.240.240.250.
Heat rate (K/min) 5.2.4.4.10.
Initial hold (min) 3.5.  2.
Final hold (min) 15.   10.
I 1189.1211.1189.1169.1201.
ReferenceStojanovic, Palic, et al., 2006Tonzibo, Coffy, et al., 2006Trilles, Bombarda, et al., 2006Velasco-Negueruela, Pérez-Alonso, et al., 2006Wang, Yang, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5SPB-1SPB-1DB-5SE-30
Column length (m) 50.50.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.220.20.250.25 
Phase thickness (mum) 1.0.330.250.25 
Tstart (C) 70.50.50.40.90.
Tend (C) 280.220.250.250.220.
Heat rate (K/min) 4.4.4.4.7.
Initial hold (min)  1.1. 2.
Final hold (min) 4.10.10.  
I 1229.1170.1167.1180.1170.
ReferenceWohlmuth, Smith, et al., 2006Wong, Lim, et al., 2006Wong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006Ahuja, Bakshi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5DB-5DB-5
Column length (m) 30.25.50.25.30.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.2490.250.30.250.25
Phase thickness (mum) 0.250.250.250.150.25
Tstart (C) 60.50.60.40.60.
Tend (C) 290.250.240.220.240.
Heat rate (K/min) 3.3.2.3.3.
Initial hold (min)  3. 5. 
Final hold (min)      
I 1189.1181.1215.1194.1191.
ReferenceBos, Stojanova, et al., 2005Cégiéla-Carlioz, Bessière, et al., 2005Chagonda and Chalchat, 2005Chagonda and Chalchat, 2005, 2Chaverri and Cicció, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeBPX5HP-5DB-1DB-1
Column length (m) 60.25.25.30.60.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.30.220.20.250.25
Phase thickness (mum)  0.250.330.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 240.320.240.250.250.
Heat rate (K/min) 3.5.3.5.5.
Initial hold (min)  5. 5. 
Final hold (min)   7.15. 
I 1190.1206.1187.1186.1180.
ReferenceChalchat and Özcan, 2005Dickschat, Bode, et al., 2005Duarte, Figueira, et al., 2005Facundo, Pinto, et al., 2005Fakhari, Salehi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1HP-5HP-5HP-5MS
Column length (m) 30.50.30.30.25.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.60.50.50.
Tend (C) 300.250.30.300.250.
Heat rate (K/min) 3.2.4.5.3.
Initial hold (min) 3.60.3.5.3.
Final hold (min)   15.5.10.
I 1183.1170.1190.1195.1192.
ReferenceFerraz, Limberger, et al., 2005Fernandez, Lizzani-Cuvelier, et al., 2005Ferretti, Maggi, et al., 2005Figuérédo, Cabassu, et al., 2005Ghasemi Y., Faridi P., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200DB-1DB-5DB-5SPB-5
Column length (m) 30.30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.53
Phase thickness (mum) 0.250.25   
Tstart (C) 40.50.60.60.100.
Tend (C) 280.265.240.240.250.
Heat rate (K/min) 6.2.53.3.5.
Initial hold (min) 2.1.   
Final hold (min) 10.30.   
I 1187.1165.1187.1186.1210.
ReferenceJirovetz, Buchbauer, et al., 2005Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Khayyat and Karimi, 2005Khayyat and Karimi, 2005Kilic, Kollmannsberger, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.15
Tstart (C) 60.60.60.60.50.
Tend (C) 230.220.220.220.230.
Heat rate (K/min) 3.4.4.4.3.
Initial hold (min)  5.5.4. 
Final hold (min)      
I 1184.1189.1189.1190.1175.
ReferenceLimberger, Sobral, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005, 2Morteza-Semnani and Saeedi, 2005Ogunwande, Olawore, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-1RTX-5 MS
Column length (m) 30.30.30.50.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 40.70.40.95.50.
Tend (C) 220.240.250.240.280.
Heat rate (K/min) 4.5.5.4.8.
Initial hold (min) 1. 0.5 2.
Final hold (min)   2. 2.
I 1183.1195.1195.1183.1198.
Referencede Oliveira, Dias, et al., 2005Oyedeji, Yani, et al., 2005Özel, Gögüs, et al., 2005Pala-Paul, Perez-Alonso, et al., 2005Pellati, Benvenuti, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSCP Sil 5 CBDB-5HP-5
Column length (m) 30.30.30.25.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum)  0.320.250.25 
Tstart (C) 60.60.40.60.60.
Tend (C) 280.250.220.200.240.
Heat rate (K/min) 3.5.4.2.5.
Initial hold (min)  3.1.  
Final hold (min)    80. 
I 1189.1172.1189.1208.1189.
ReferencePetrakis, Roussis, et al., 2005Pourmortazavi, Ghadiri, et al., 2005Rohloff and Bones, 2005Rout, Misra, et al., 2005Saeidnia, Gohari, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSDB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.60.50.40.
Tend (C) 280.275.280.265.240.
Heat rate (K/min) 4.4.4.2.54.
Initial hold (min)    1. 
Final hold (min)    20. 
I 1191.1194.1190.1164.1189.
ReferenceSajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005Sajjadi, 2005Sarkhail, Amin, et al., 2005Sefidkon and Jamzad, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5PE-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 260.280.300.230.230.
Heat rate (K/min) 2.3.3.5.3.
Initial hold (min) 5.5. 2. 
Final hold (min) 20.  4.20.
I 1190.1189.1184.1201.1189.
ReferenceSenatore, Apostolides Arnold, et al., 2005Setzer, Noletto, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Singh, Raina, et al., 2005Skoula and Grayer, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSRTX-1RTX-1DB-1DB-5
Column length (m) 30.60.60.60.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 280.250.25.250.210.
Heat rate (K/min) 3.5.5.5.2.
Initial hold (min)     2.
Final hold (min)  10.10.10.33.
I 1194.1178.1177.1176.1191.
ReferenceSlavkovska, Couladis, et al., 2005Sonboli A., Fakhari A.R., et al., 2005Sonboli, Salehi, et al., 2005Sonboli, Salehi, et al., 2005, 2Stevanovic, Garneau, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5MSHP-5MSHP-5 MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.500.25
Tstart (C) 60.50.60.60.60.
Tend (C) 290.240.285.260.280.
Heat rate (K/min) 3.3.4.33.3.
Initial hold (min) 5.3.   
Final hold (min)    20. 
I 1192.1224.1189.1188.1162.
ReferenceSuárez, Vásquez, et al., 2005Tepe B., Sokmen M., et al., 2005Tesevic, Nikicevic, et al., 2005Topçu, Barla, et al., 2005Tzakou, Bazos, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1HP-5MSSPB-1
Column length (m) 30.50.50.30.50.
Carrier gas HeN2  He
Substrate      
Column diameter (mm) 0.320.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 60.90.60.40.50.
Tend (C) 280.240.240.220.220.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min)    5.3.
Final hold (min)    10.30.
I 1163.1169.1163.1186.1176.
ReferenceTzakou and Constantinidis, 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2Vichi, Riu-Aumatell, et al., 2005Wong, Lee, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5HP-5HP-5HP-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.20.320.320.320.32
Phase thickness (mum) 0.330.250.250.250.25
Tstart (C) 50.40.40.40.40.
Tend (C) 220.250.250.250.250.
Heat rate (K/min) 4.5.5.5.5.
Initial hold (min) 3.2.2.2.2.
Final hold (min) 30.5.5.5.5.
I 1172.1177.1180.1186.1193.
ReferenceWong and Tan, 2005N/AN/AN/AN/A
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5BP-1DB-1SPB-5
Column length (m) 30.30.50.60.60.
Carrier gas N2He N2He
Substrate      
Column diameter (mm) 0.250.250.220.250.32
Phase thickness (mum) 0.250.250.250.251.
Tstart (C) 50.90.60.70.60.
Tend (C) 200.220.220.230.200.
Heat rate (K/min) 5.7.2.2.4.
Initial hold (min)  2. 2. 
Final hold (min)  5.20.20.30.
I 1179.1172.1171.1182.1194.
ReferenceAgnaniet, Menut, et al., 2004Agnihotri, Thappa, et al., 2004Blanc, Muselli, et al., 2004Choi, 2004Gauvin, Ravaomanarivo, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSDB-1DB-5ZB-5
Column length (m) 30.30.25.25.60.
Carrier gas HeliumHe NitrogenHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 275.275.180.240.260.
Heat rate (K/min) 4.4.3.3.6.
Initial hold (min)   10. 4.6
Final hold (min)   10. 1.
I 1199.1184.1188.1190.1204.
ReferenceGhannadi, Sajjadi, et al., 2004Hajhashemi V., Ghannadi A., et al., 2004bin Jantan, Ayop, et al., 2004JAvidnia, Mojab, et al., 2004Jürgens and Dötterl, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1SE-54DB-5MSDB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 280.300.260.240.300.
Heat rate (K/min) 4.4.2.3.3.
Initial hold (min) 4. 5.  
Final hold (min)      
I 1188.1178.1188.1189.1184.
ReferenceKalvandi, Sefidkon, et al., 2004Kalemba and Thiem, 2004Kilic, Hafizoglu, et al., 2004paz Lima, Silva, et al., 2004Limberger, Sobral, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5MSDB-5DB-5NB-30
Column length (m) 30.30.30.50.50.
Carrier gas HeHeHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.25  0.25
Tstart (C) 60.60.60.60.50.
Tend (C) 280.275.240.240.250.
Heat rate (K/min) 3.4.2.2.2.
Initial hold (min)      
Final hold (min) 30. 999.999. 
I 1160.1194.1192.1192.1177.
ReferenceMarongiu, Piras, et al., 2004Mehrabani, Asadipour, et al., 2004Miyazawa, Fuhita, et al., 2004Miyazawa, Fujita, et al., 2004Orav, Stulova, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-1DB-1DB-1DB-1
Column length (m) 50.50.60.60.60.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.250.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.95.35.35.35.
Tend (C) 250.240.230.230.230.
Heat rate (K/min) 2.4.2.2.2.
Initial hold (min)   4.4.4.
Final hold (min)   25.25.25.
I 1176.1174.1165.1167.1167.
ReferenceOrav, Stulova, et al., 2004Palá-Paúl, Velasco-Negueruela, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1NB-30NB-30DB-5Methyl Silicone
Column length (m) 60.50.50.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.20.200.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.50.50.35.60.
Tend (C) 230.250.250.220.200.
Heat rate (K/min) 2.2.2.2.54.
Initial hold (min) 4.   1.
Final hold (min) 25.  6.20.
I 1170.1177.1177.1189.1186.
ReferencePark, Lee, et al., 2004Raal, Arak, et al., 2004Raal, Paaver, et al., 2004Rohloff, Mordal, et al., 2004Rojas, Usubillaga, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5MSDB-1DB-1
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeHe Nitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.70.70.
Tend (C) 200.280.280.230.230.
Heat rate (K/min) 4.4.4.2.2.
Initial hold (min) 1.  2.2.
Final hold (min) 20.  20. 
I 1186.1187.1190.1184.1184.
ReferenceRoyas, Usubillaga, et al., 2004Sadeghpour, Asghari, et al., 2004Sajjadi and Shahpiri, 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-1DB-5HP-5
Column length (m) 30.60.30.30.25.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.330.250.5
Tstart (C) 50.40.40.40.30.
Tend (C) 250.280.260.250.280.
Heat rate (K/min) 3.4.2.2.3.
Initial hold (min) 5.5.5.5. 
Final hold (min)   20.20. 
I 1189.1171.1155.1191.1197.
ReferenceSefidkon, Jamzad, et al., 2004Sefidkon and Shaabani, 2004Senatore, Napolitano, et al., 2004Senatore, Rigano, et al., 2004Shafi, Nambiar, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-1BPX-5CP Sil 8 CB
Column length (m) 25.30.60.25.30.
Carrier gas H2HeN2He 
Substrate      
Column diameter (mm) 0.320.250.250.220.32
Phase thickness (mum) 0.520.250.251.0.25
Tstart (C) 40.60.80.60.50.
Tend (C) 240.240.210.250.200.
Heat rate (K/min) 4.3.3.3.5.
Initial hold (min)    5.5.
Final hold (min)   15.10. 
I 1189.1190.1177.1219.1200.
ReferenceSimic, Sokovic, et al., 2004Tellez, Khan, et al., 2004Ueno, Masuda, et al., 2004Vilaseca, Guy, et al., 2004Wang, Guo, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HTHP-5MSHP-5DB-5
Column length (m) 30.27.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.2490.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 300.250.275.220.240.
Heat rate (K/min) 3.2.4.5.4.
Initial hold (min)  2. 10. 
Final hold (min)  20.   
I 1190.1192.1189.1185.1176.
ReferenceWoerdenbag, Windono, et al., 2004Yusufoglu, Celik, et al., 2004Afsharypuor and Jahromy, 2003Bertoli, Menichini, et al., 2003Cabanillas, Lopez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSMethyl SiliconeDB-1RTX-5Sil
Column length (m) 60.30.12.560.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25  0.25
Tstart (C) 70.60.50.50.70.
Tend (C) 230.280.270.250.200.
Heat rate (K/min) 2.3.4.4.4.
Initial hold (min) 2.    
Final hold (min) 20.   10.
I 1184.1187.1178.1168.1199.
ReferenceChoi, 2003Couladis, Özcan, et al., 2003Curini, Bianchi, et al., 2003Dabiri and Sefidkon, 2003Dudai, Larkov, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-5MSHP-1
Column length (m) 60.60.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum)    0.250.25
Tstart (C) 50.50.50.60.70.
Tend (C) 220.200.220.220.200.
Heat rate (K/min) 3.3.3.5.10.
Initial hold (min)    20. 
Final hold (min)    20. 
I 1200.1200.1201.1193.1179.
ReferenceEdris and Farrag, 2003Edris, Shalaby, et al., 2003Edris, Shalaby, et al., 2003, 2Feizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSRSL-200RSL-200RSL-200
Column length (m) 30.30.30.30.30.
Carrier gas N2HeH2H2H2
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.40.40.40.
Tend (C) 200.275.280.280.280.
Heat rate (K/min) 5.4.6.6.6.
Initial hold (min)   5.2.5.
Final hold (min)   5.10.5.
I 1172.1189.1182.1187.1182.
ReferenceFekam Boyom, Ngouana, et al., 2003Hajhashemi, Ghannadi, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Jirovetz, Buchbauer, et al., 2003, 3
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-30CP Sil 5 CBDB-1DB-5MS
Column length (m) 50.12.25.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.20.220.250.250.25
Phase thickness (mum) 0.250.30.250.250.25
Tstart (C) 50.70.35.80.60.
Tend (C) 220.220.280.250.240.
Heat rate (K/min) 3.3.5.4.3.
Initial hold (min) 2. 2.5  
Final hold (min) 10.    
I 1190.1174.1169.1162.1192.
ReferenceJuteau, Jerkovic, et al., 2003Kambouche and El-Abed, 2003Kanjilal, Kotoky, et al., 2003Mahalwal and Ali, 2003Maia, Taveira, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBZB-1HP-5OV-101
Column length (m) 30.25.30.30.50.
Carrier gas He N2HeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.320.2
Phase thickness (mum) 0.250.390.25 0.5
Tstart (C) 60.60.45.70.50.
Tend (C) 280.220.230.210.250.
Heat rate (K/min) 3.5.3.2.2.
Initial hold (min)      
Final hold (min) 30.  60. 
I 1184.1179.1166.1189.1174.
ReferenceMarongiu, Porcedda, et al., 2003Mazloomifar, Saber-Tehrani, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Mookdasanit, Tamura, et al., 2003Orav, Kailas, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5NB-30DB-1
Column length (m) 50.30.30.50.60.
Carrier gas N2H2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.250.50.25
Tstart (C) 95.60.60.50.40.
Tend (C) 240.280.280.250.220.
Heat rate (K/min) 4.4.3.2.4.
Initial hold (min)  10.   
Final hold (min)  40.   
I 1181.1189.1174.1177.1175.
ReferencePerez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003Raal, Arak, et al., 2003Rasooli and Mirmostafa, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-1DB-5HP-5
Column length (m) 60.30.60.30.60.
Carrier gas HeN2HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.50.60.40.
Tend (C) 220.230.280.240.250.
Heat rate (K/min) 4.2.4.3.5.
Initial hold (min)     15.
Final hold (min)      
I 1175.1189.1174.1192.1189.
ReferenceRasooli and Mirmostafa, 2003Rotman, Ahumada, et al., 2003Shahmir, Ahmadi, et al., 2003da Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-1DB-1HP-1DB-1
Column length (m) 30.60.60.50.50.
Carrier gas HeN2N2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.250.50.25
Tstart (C) 60.70.70.60.90.
Tend (C) 240.230.230.220.240.
Heat rate (K/min) 3.2.2.2.4.
Initial hold (min)  2.2.  
Final hold (min)  20.20.40. 
I 1188.1186.1182.1169.1161.
ReferenceTaveira, de Lima, et al., 2003Tu, Onishi, et al., 2003Tu, Onishi, et al., 2003, 2Valette, Fernandez, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Cross-Linked MethylsiliconeHP-5HP-5DB-5DB-5
Column length (m) 25.25.25.30.30.
Carrier gas HeH2H2HeHe
Substrate      
Column diameter (mm) 0.20.320.320.250.249
Phase thickness (mum) 0.330.530.530.250.25
Tstart (C) 70.40.40.60.60.
Tend (C) 250.280.280.240.300.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min)      
Final hold (min)     5.
I 1169.1189.1189.1190.1187.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2003, 2Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003Zoghbi, Andrade, et al., 2003Bos, Koulman, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5HP-15 % Phenyl methyl siloxaneDB-1
Column length (m) 25.30.30.30.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 50.60.70.75.50.
Tend (C) 200.280.220.200.200.
Heat rate (K/min) 5.3.3.3.3.
Initial hold (min)    4.6.
Final hold (min)  30.15.8. 
I 1179.1185.1169.1189.1158.
ReferenceBoyom, Keumedjio, et al., 2002Caredda, Marongiu, et al., 2002Cavaleiro, Salgueiro, et al., 2002Cicció and Gómez-Laurito, 2002Cimanga, Apers, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSDB-5MSBP-1DB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.500.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.60.50.60.50.
Tend (C) 280.280.280.220.250.
Heat rate (K/min) 3.3.15.5.4.
Initial hold (min)   2.  
Final hold (min)   10.10. 
I 1192.1192.1181.1178.1189.
ReferenceCongiu, Falconieri, et al., 2002Congiu, Falconieri, et al., 2002Damon, Hernández, et al., 2002Das, Ram, et al., 2002Farah, Fechtal, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-1PTE-5SE-30
Column length (m) 30.30.30.60.50.
Carrier gas N2HeH2H2He
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (mum) 0.250.250.250.300.25
Tstart (C) 50.60.40.60.70.
Tend (C) 250.240.245.285.240.
Heat rate (K/min) 4.3.3.4.34.
Initial hold (min) 5. 20.  
Final hold (min)      
I 1189.1191.1169.1189.1185.
ReferenceFarah, Fechtal. M., et al., 2002Flamini, Ertugrul, et al., 2002Gancel, Ollé, et al., 2002Gudzic, Djokovic, et al., 2002Iñigo, Palá-Paúl, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200CP Sil 8 CBDB-1SPB-5
Column length (m) 30.30.30.25.60.
Carrier gas H2H2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.230.25
Phase thickness (mum) 0.250.250.250.200.25
Tstart (C) 40.50.50.50.50.
Tend (C) 280.280.220.200.240.
Heat rate (K/min) 6.6.3.3.5.
Initial hold (min) 5.5.2.3.3.
Final hold (min) 5.5. 30.10.
I 1179.1179.1198.1193.1203.
ReferenceJirovetz, Buchbauer, et al., 2002Jirovetz, Ngassoum, et al., 2002Juteau, Masotti, et al., 2002Khallouki, Younos, et al., 2002Kim and Lee, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.35.50.60.40.
Tend (C) 240.280.200.250.290.
Heat rate (K/min) 3.3.5.3.7.
Initial hold (min)  2.   
Final hold (min)  15.   
I 1188.1195.1176.1184.1206.
ReferenceKobaisy, Tellez, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002Kuiate, Bessière, et al., 2002Limberger, Simões-Pires, et al., 2002Lin, Rouseff, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5MSDB-1HP-5
Column length (m) 25.30.30.30.30.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.230.250.250.250.25
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 250.240.240.250.240.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min)    10. 
Final hold (min)      
I 1195.1192.1190.1198.1192.
ReferenceMahmout, Bessière, et al., 2002Maia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002Norouzi-Arasi, Yavari, et al., 2002Novak, Langbehn, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5OV-101DB-1DB-5MSSPB-5
Column length (m) 30.50.50.30.30.
Carrier gas  HeN2HeHelium
Substrate      
Column diameter (mm) 0.250.20.250.320.25
Phase thickness (mum) 0.250.50.250.250.25
Tstart (C) 60.50.80.40.60.
Tend (C) 240.250.225.280.250.
Heat rate (K/min) 3.2.4.4.4.
Initial hold (min)     2.
Final hold (min)    5.20.
I 1196.1172.1180.1182.1189.
ReferenceNovak, Langbehn, et al., 2002Orav, Kailas, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002Phutdhawong, Korth, et al., 2002Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-1DB-1
Column length (m) 30.25.60.60.50.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.60.40.40.60.
Tend (C) 300.220.280.280.240.
Heat rate (K/min) 2.3.4.4.3.
Initial hold (min)   5.5. 
Final hold (min)      
I 1189.1192.1170.1169.1163.
ReferenceRuberto, Biondi, et al., 2002Schwob, Bessière, et al., 2002Sefidkon, Jalili, et al., 2002Sefidkon, 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSDB-5HP-5DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas H2HeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 280.270.240.220.240.
Heat rate (K/min) 4.3.3.5.3.
Initial hold (min)    10. 
Final hold (min)      
I 1189.1191.1190.1190.1186.
ReferenceVelickovic, Randjelovic, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Campeol, Flamini, et al., 2001Cherchi, Deidda, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-5MSHP-5BP-1
Column length (m) 60.60.60.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 40.40.35.60.60.
Tend (C) 220.280.250.220.220.
Heat rate (K/min) 3.4.3.5.5.
Initial hold (min) 5.5.5.10. 
Final hold (min) 15.    
I 1190.1170.1199.1190.1177.
ReferenceCornu, Carnat, et al., 2001Dabiri and Sefidkon, 2001Fernando and Grün, 2001Flamini, Cioni, et al., 2001Gupta, Mallavarapu, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RTX-1SPB-5BP-1CBP-1
Column length (m) 30.30.60.50.25.
Carrier gas H2N2HeliumHeNitrogen
Substrate      
Column diameter (mm) 0.320.250.250.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.60.50.
Tend (C) 280.300.240.230.210.
Heat rate (K/min) 6.4.3.2.3.
Initial hold (min) 5. 3. 2.
Final hold (min) 5. 10.35. 
I 1171.1179.1203.1172.1172.
ReferenceJirovetz L., Buchbauer G., et al., 2001Kalemba, Marschall, et al., 2001Kim and Lee, 2001Lota, de Rocca Serra, et al., 2001Ly, Yamauchi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-1OV-101OV-101OV-101
Column length (m) 30.60.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.20.2
Phase thickness (mum) 0.250.250.5  
Tstart (C) 60.50.50.50.50.
Tend (C) 240.270.250.250.250.
Heat rate (K/min) 3.4.2.2.2.
Initial hold (min)      
Final hold (min) 30.    
I 1163.1167.1172.1172.1173.
ReferenceMarongiu, Porcedda, et al., 2001Mirza, Ahmadi, et al., 2001Orav, Kailas, et al., 2001Orav and Kann, 2001Orav and Kann, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5DB-5DB-5
Column length (m) 30.30.30.60.30.
Carrier gas HeN2 HeH2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.5 0.25
Tstart (C) 60.80.35.50.60.
Tend (C) 270.225.275.250.285.
Heat rate (K/min) 3.4.6.3.3.
Initial hold (min)    5. 
Final hold (min)      
I 1192.1161.1201.1189.1189.
ReferencePalmeira, Conserva, et al., 2001Palá-Paúl, Pérez-Alonso, et al., 2001Rouseff, Jella, et al., 2001Rousis, Papadogianni, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PTE-5SPB-1OV-101OV-101Optima-1
Column length (m) 60.30.50.50.25.
Carrier gas H2HeN2N2He
Substrate      
Column diameter (mm) 0.320.320.250.250.20
Phase thickness (mum) 0.30.25  0.25
Tstart (C) 60.50.80.80.50.
Tend (C) 285.250.200.200.250.
Heat rate (K/min) 4.32.2.2.3.
Initial hold (min)     3.
Final hold (min)      
I 1189.1177.1178.1178.1181.
ReferenceStojanovic, Palic, et al., 2001Vijayanand, Rao, et al., 2001Yang, 2001Yang, 2001, 2de Beck, Bessière, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RSL-200HP-5DB-1HP-1
Column length (m) 30.60.30.25.60.
Carrier gas  H2HeNitrogenHe
Substrate      
Column diameter (mm) 0.320.320.250.500.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 45.40.80.60.60.
Tend (C) 300.250.200.220.200.
Heat rate (K/min) 15.6.9.5.4.
Initial hold (min) 2.   5.
Final hold (min) 5. 10. 25.
I 1215.1186.1182.1176.1178.
ReferenceHedin, McKibben, et al., 2000Jirovetz, Puschmann, et al., 2000Lis-Balchin and Roth, 2000Mallavarapu, Rao, et al., 2000Meccia, Rojas, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5DB-1DB-5
Column length (m) 30.25.30.30.60.
Carrier gas N2N2HeHeHydrogen or helium (He2 wrote in original paper)
Substrate      
Column diameter (mm) 0.220.330.250.250.25
Phase thickness (mum) 0.251.00.250.250.30
Tstart (C) 70.60.60.40.60.
Tend (C) 230.275.275.260.285.
Heat rate (K/min) 4.4.4.2.4.3
Initial hold (min) 2.  5. 
Final hold (min) 20.  2. 
I 1187.1189.1188.1169.1189.
ReferenceMitiku, Sawamura, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2Senatore, Napolitano, et al., 2000Simic, Andjelkovic, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5SE-30OV-101OV-1
Column length (m) 50.30.25.25.25.
Carrier gas NitrogenHeHeN2Hydrogen
Substrate      
Column diameter (mm) 0.250.250.20.250.32
Phase thickness (mum)  0.25  0.30
Tstart (C) 40.60.60.50.50.
Tend (C) 200.240.230.200.200.
Heat rate (K/min) 2.3.3.5.3.
Initial hold (min) 10.   1.
Final hold (min)     10.
I 1178.1190.1174.1181.1161.
ReferenceTamura, Boonbumrung, et al., 2000Tellez, Dayan, et al., 2000Ali N.A.M. and Jantan, 1999Ayedoun, Adéoti, et al., 1999Bicchi, Binello, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SE-30RTX-1DB-1OV-101
Column length (m) 50.30.30.25.25.
Carrier gas  N2N2He 
Substrate      
Column diameter (mm) 0.20.250.250.250.32
Phase thickness (mum) 0.330.250.250.25 
Tstart (C) 60.60.60.50.50.
Tend (C) 260.220.300.290.200.
Heat rate (K/min) 4.4.4.4.5.
Initial hold (min)  10.   
Final hold (min)      
I 1180.1177.1179.1187.1176.
ReferenceChoo, Wong, et al., 1999Jassbi, Ahmad, et al., 1999Kalemba, 1999Koulman, 1999Kuiate, Zollo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5HP-1OV-101DB-5SE-30
Column length (m) 50.25.50.30.25.
Carrier gas HeH2N2 He
Substrate      
Column diameter (mm) 0.320.320.20.320.2
Phase thickness (mum) 1.0.17 1. 
Tstart (C) 40.40.80.40.60.
Tend (C) 190.260.200.200.230.
Heat rate (K/min) 2.3.1.3.3.
Initial hold (min) 5.5. 5.10.
Final hold (min)   20.  
I 1199.1174.1181.1195.1174.
ReferenceLopez, Ferreira, et al., 1999Lopes, Koketsu, et al., 1999Menon, Chacko, et al., 1999Meynier, Novelli, et al., 1999Mohd and Jantan, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1OV-101DB-5SE-30
Column length (m) 25.50.50.30.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.250.20
Tstart (C) 50.70.70.40.60.
Tend (C) 230.240.220.250.200.
Heat rate (K/min) 3.4.2.2.3.
Initial hold (min)   5.5.4.
Final hold (min)    60. 
I 1172.1163.1173.1150.1194.
ReferenceOyedeji, Olawore, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999Pateira, Nogueira, et al., 1999Porta, Porcedda, et al., 1999Prikhod'ko, Klyuev, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 5 CBCP Sil 5 CBDB-1DB-5
Column length (m) 25.25.25.60.30.
Carrier gas N2HeN2HeHe
Substrate      
Column diameter (mm) 0.50.250.250.250.25
Phase thickness (mum)  0.390.390.250.25
Tstart (C) 60.60.60.40.40.
Tend (C) 220.220.220.280.220.
Heat rate (K/min) 5.5.5.4.4.
Initial hold (min)  5. 5.5.
Final hold (min) 10.20.   
I 1177.1177.1177.1173.1190.
ReferenceRao, Bhattacharya, et al., 1999Rustaiyan, Masoudi, et al., 1999Rustaiyan and Nadji, 1999Sefidkon, Dabiri, et al., 1999Sefidkon and Khajavi, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5OV-101CP Sil 5 CB
Column length (m) 60.30.30.25.25.
Carrier gas HeH2HeNitrogenN2
Substrate      
Column diameter (mm) 0.320.320.250.20 
Phase thickness (mum)   0.25 0.39
Tstart (C) 60.32.60.60.60.
Tend (C) 230.260.240.220.220.
Heat rate (K/min) 3.7.3.4.5.
Initial hold (min)  5. 0. 
Final hold (min) 5.5. 0. 
I 1178.1210.1189.1177.1178.
ReferenceShafiee, Javidnia, et al., 1999Sun and Petracek, 1999Tellez, Canel, et al., 1999Tropnikova, Zenkevich, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5DB-5MSSPB-5DB-5
Column length (m) 25.30.30.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.200.250.250.320.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 80.60.60.60.60.
Tend (C) 240.240.240.240.240.
Heat rate (K/min) 6.3.3.3.3.
Initial hold (min)      
Final hold (min)    20. 
I 1181.1190.1193.1192.1184.
ReferenceZenkevich, Kosman, et al., 1999Zoghbi, Andrade, et al., 1999Zoghbi, Andrade, et al., 1999, 2Doneanu and Anitescu, 1998El-Sakhawy, El-Tantawy, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5SE-30OV-1CBP-1DB-5
Column length (m) 50.25.50.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.20.320.250.25
Phase thickness (mum) 1. 0.25 0.25
Tstart (C) 40.60.50.60.60.
Tend (C) 190.180.250.240.240.
Heat rate (K/min) 2.3.10.4.3.
Initial hold (min) 5.10.5.  
Final hold (min)   20.  
I 1199.1175.1177.1179.1189.
ReferenceFerreira, Ardanuy, et al., 1998Jantan, Ahmad, et al., 1998Kökdil, Kurucu, et al., 1998Lamarque, Maestri, et al., 1998Maia, Zohhbi, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101HP-1HP-5HP-1OV-101
Column length (m) 25.25.25.60.25.
Carrier gas He HeHe 
Substrate      
Column diameter (mm) 0.20.320.20.250.32
Phase thickness (mum) 0.2 0.330.25 
Tstart (C) 70.35.70.50.50.
Tend (C) 200.250.290.280.200.
Heat rate (K/min) 3.4.3.4.5.
Initial hold (min) 2. 8.5. 
Final hold (min) 10. 20.  
I 1184.1172.1191.1190.1181.
ReferenceMilso, Mastelic, et al., 1998Ong and Acree, 1998Poiana, Sicari, et al., 1998Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBOV-1OV-1
Column length (m) 25.25.25.30.30.
Carrier gas N2N2HeHe 
Substrate      
Column diameter (mm) 0.320.320.250.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.60.40.40.
Tend (C) 290.290.300.270.270.
Heat rate (K/min) 4.4.6.2.2.
Initial hold (min)    4.4.
Final hold (min)      
I 1165.1165.1165.1187.1186.
ReferenceBos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2Kökdil, Kurucu, et al., 1997Kökdil, Tanker, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-SulfurSPB-SulfurDB-1DB-5CBP-1
Column length (m) 30.30. 30.25.
Carrier gas HeHe HeliumHe
Substrate      
Column diameter (mm) 0.320.32 0.250.22
Phase thickness (mum) 4.4. 0.25 
Tstart (C) 45.45.80.60.60.
Tend (C) 240.240.220.240.240.
Heat rate (K/min) 5.5.6.3.5.
Initial hold (min) 13.13.   
Final hold (min) 5.5.   
I 1198.1199.1159.1189.1176.
ReferenceMariaca, Berger, et al., 1997Mariaca, Berger, et al., 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1OV-101OV-101BP-1BP-1
Column length (m) 23.50.50.25.25.
Carrier gas HeN2HeN2N2
Substrate      
Column diameter (mm) 0.320.250.250.500.50
Phase thickness (mum) 0.170.17   
Tstart (C) 60.50.50.60.60.
Tend (C) 250.220.250.220.220.
Heat rate (K/min) 5.5.2.5.5.
Initial hold (min) 3.    
Final hold (min) 30.    
I 1169.1185.1172.1172.1176.
ReferenceAyedoun, Adeoti, et al., 1996Chacko, Jayalekshmy, et al., 1996Orav, Kailas, et al., 1996Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-1SPB-1OV-101
Column length (m) 60.30.25.50.15.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.320.20.32
Phase thickness (mum) 0.50 0.250.33 
Tstart (C) 50.40.60.40.35.
Tend (C) 250.210.220.200.250.
Heat rate (K/min) 8.2.4.3.6.
Initial hold (min) 1.2.2.3.3.
Final hold (min) 6.33.20.30. 
I 1179.1188.1169.1175.1185.
ReferenceSagrero-Nieves and Bartley, 1996Sohounhloue, Dangou, et al., 1996Thanh, Dung, et al., 1996Wong and Lai, 1996Chisholm, Guiher, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101HP-5DB-1DB-1DB-1
Column length (m) 52. 60.60.60.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.26 0.250.250.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 50.35.50.70.70.
Tend (C) 220.200.250.270.270.
Heat rate (K/min) 3.6.3.52.52.5
Initial hold (min)  2.5.5.5.
Final hold (min)      
I 1179.1211.1171.1179.1179.
ReferenceDzumayev, Tsibulskaya, et al., 1995Larsen and Frisvad, 1995Stashenko, Torres, et al., 1995Tirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSOV-1HP-5HP-5HP-101
Column length (m) 30.50.  50.
Carrier gas HeliumN2  H2
Substrate      
Column diameter (mm) 0.250.27  0.32
Phase thickness (mum)  0.2  0.3
Tstart (C) 50.80.40.40.65.
Tend (C) 250.240.210.210.300.
Heat rate (K/min) 4.3.2.2.2.
Initial hold (min)     5.
Final hold (min)      
I 1199.1177.1187.1188.1170.
ReferenceGomez and Ledbetter, 1994Ramanoelina, Viano, et al., 1994Collin, Deslauriers, et al., 1993Collin, Deslauriers, et al., 1993Demarne and van der Walt, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeMethyl SiliconeCP Sil 5 CBMethyl SiliconeOV-101
Column length (m) 50.50.25.25.50.
Carrier gas N2N2   
Substrate      
Column diameter (mm) 0.250.250.250.500.25
Phase thickness (mum) 0.170.17   
Tstart (C) 80.80.60.60.80.
Tend (C) 200.200.280.220.200.
Heat rate (K/min) 2.3.5.5.2.
Initial hold (min)      
Final hold (min)      
I 1185.1183.1177.1175.1177.
ReferenceGopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Kaul, Singh, et al., 1993Mallavarapu, Ramesh, et al., 1993Tamura, Yang, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101DB-1SE-54DB-1
Column length (m) 50.52.60.30.30.
Carrier gas  HeliumHeHydrogenN2
Substrate      
Column diameter (mm) 0.250.260.320.25 
Phase thickness (mum)   1.20.25 
Tstart (C) 80.40.30.60.80.
Tend (C) 200.200.240.250.220.
Heat rate (K/min) 2.3.3.2.4.
Initial hold (min)  0.10.5. 
Final hold (min)  0. 2. 
I 1178.1172.1184.1187.1168.
ReferenceTamura, Yang, et al., 1993Tkachenko and Zenkevich, 1993Ciccioli, Cecinato, et al., 1992Kollmannsberger, Nitz, et al., 1992Velasco-Negueruela, Pérez Alonso, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1CP Sil 8 CBHP-5HP-5
Column length (m) 60.60.25.50.50.
Carrier gas  He H2H2
Substrate      
Column diameter (mm)  0.250.200.30.3
Phase thickness (mum)      
Tstart (C) 30.30.60.80.80.
Tend (C) 200.200.230.250.250.
Heat rate (K/min) 4.4.3.16.16.
Initial hold (min) 25.25.10.  
Final hold (min) 30.5.   
I 1170.1170.1193.1185.1199.
ReferenceButtery, Takeoka, et al., 1990Buttery, Teranishi, et al., 1990Jantan and Goh, 1990Spadone, Takeoka, et al., 1990Spadone, Takeoka, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-101OV-101DB-1BP-1
Column length (m) 25.50.50.60.50.
Carrier gas  N2N2 H2
Substrate      
Column diameter (mm) 0.330.250.250.320.30
Phase thickness (mum)      
Tstart (C) 45.80.80.50.40.
Tend (C) 180.200.200.250.250.
Heat rate (K/min) 3.2.2.4.10.
Initial hold (min) 3.  0.11.
Final hold (min)    5. 
I 1171.1177.1178.1170.1177.
ReferenceWyllie, Brophy, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Binder and Flath, 1989Brophy, Davies, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30OV-101OV-101OV-101DB-1
Column length (m) 40.50.50.50.60.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.500.250.250.250.32
Phase thickness (mum) 0.75    
Tstart (C) 30.80.80.80.30.
Tend (C) 220.200.200.200.210.
Heat rate (K/min) 3.2.2.2.2.
Initial hold (min)     4.
Final hold (min)      
I 1176.1177.1173.1177.1169.
Referencede Pooter, de Buyck, et al., 1989Sugisawa, Yamamoto, et al., 1989Sugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Takeoka and Butter, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-54DB-5OV-1OV-1
Column length (m) 60.25.30.50.60.
Carrier gas HeN2HydrogenHeHelium
Substrate      
Column diameter (mm) 0.320.250.350.200.50
Phase thickness (mum)   1.00.201.2
Tstart (C) 30.60.45.30.40.
Tend (C) 210.260.220.220.220.
Heat rate (K/min) 2.6.2.2.2.
Initial hold (min) 4.2.   
Final hold (min)      
I 1170.1190.1197.1171.1174.
ReferenceTakeoka and Butter, 1989Bestmann, Classen, et al., 1988Georgilopoulos and Gallois, 1988de Pooter, Nicolai, et al., 1988Wahab, Aboutabl, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-1DB-1
Column length (m) 50.50.50. 50.
Carrier gas    He 
Substrate      
Column diameter (mm) 0.300.300.30 0.32
Phase thickness (mum)      
Tstart (C) 40.40.40.40.0.
Tend (C) 230.230.230.220.250.
Heat rate (K/min) 3.53.53.52.3.
Initial hold (min) 5.5.5.  
Final hold (min)      
I 1170.1179.1194.1177.1172.
ReferenceNykanen, 1986Nykanen, 1986Nykanen, 1986De Pooter, De Buyck, et al., 1986Habu, Flath, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-1SE-30+IgepalSE-30+Igepal
Column length (m) 50.60.183.100.100.
Carrier gas   N2  
Substrate      
Column diameter (mm) 0.320.320.7620.250.25
Phase thickness (mum)      
Tstart (C) 50.50.0.70.70.
Tend (C) 250.250.230.170.170.
Heat rate (K/min) 3.4.1.1.1.
Initial hold (min)  0.1   
Final hold (min)  5.   
I 1170.1169.1184.1180.1184.
ReferenceHabu, Flath, et al., 1985Flath, Mon, et al., 1983Schreyen, Dirinck, et al., 1979Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Cavar, Maksimovic, et al., 2010
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Ho, Wang, et al., 2010
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Miyazawa, Kawauchi, et al., 2010
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Pino, Marquez, et al., 2010
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Usman, Zubair, et al., 2010
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Zouari, Zouari, et al., 2010
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Alim, Goze, et al., 2009
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Dayisoylu and Alma, 2009
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Farhat, Ginies, et al., 2009
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Gauvin-Bialecki and Marodon, 2009
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Ho, Wang, et al., 2009
Ho, C.-L.; Wang, E.I.-C.; Su, Y.-C., Essential oil compositions and bioactivities of the various parts of Cinnamomum camphora Sieb. var. linallolifera Fujuta, Journal title only in Chinese, 2009, 31, 2, 77-96. [all data]

Kazemi and Akhavani, 2009
Kazemi, M.; Akhavani, S., Constituents of Artemisia tournefortiana Rchb. essential oil from Iran, J. Appl. Chem. Res., 2009, 3, 10, 1-5. [all data]

Koba, Sanda, et al., 2009
Koba, K.; Sanda, K.; Guyon, C.; Raynaud, C.; Chaumont, J.-P.; Nicod, L., In vitro cytotoxic activity of Cymbopogon citratus L. and Cymbopogon nardus L. essential oils from Togo, J. Bangladesh Pharmacological Soc., 2009, 4, 29-34. [all data]

Males, Plazibat, et al., 2009
Males, Z.; Plazibat, M.; Bucar, F., Essential oil of Portanschlagiella ramosissima from Croatia, a rich source of myristicin, Croat. Chem. Acta, 2009, 82, 4, 725-728. [all data]

Maridass, 2009
Maridass, M., Inter-generic relationships of Ocimum and Origanum based on GC-MS volatile oils data using software NTSPSpc version 2.0, Ethnobotanical Leaflets, 2009, 13, 83-88. [all data]

Museli, Pau, et al., 2009
Museli, A.; Pau, M.; Desjobert, J.-M.; Foddai, M.; Usai, M.; Costa, J., Volatile constituents of Achllea ligustica All. by HS-SPME/GC/GC-MS. Comparison with essential oils obtained by hydrodistillation from Corsica and Sardinia, Chromatographia, 2009, 69, 5/6, 575-585, https://doi.org/10.1365/s10337-008-0939-1 . [all data]

Ottavioli, Bighelli, et al., 2009
Ottavioli, J.; Bighelli, A.; Casanova, J.; Bang, B.T.; Y., GC (retention indices), GC-MS, and 13C NMR of two citral-rich Cymbopogon leaf oils: C. Flexuosus and C. tortilis, Spectroscopy Lett., 2009, 42, 8, 506-512, https://doi.org/10.1080/00387010903022350 . [all data]

Patil, Jayaprakasha, et al., 2009
Patil, J.R.; Jayaprakasha, G.K.; Murthy, K.N.C.; Tichy, S.E.; Chetti, M.B.; Patil, B.S., Apoptosis-mediated proliferation inhibition of human colon cancer cells by volatile principles of Citrus auratifolia, Food Chem., 2009, 114, 4, 1351-1358, https://doi.org/10.1016/j.foodchem.2008.11.033 . [all data]

Porto, Decorti, et al., 2009
Porto, C.Da.; Decorti, D.; Kikic, I., Flavour compounds of Lavandula angustifolia L. to use in food manufacturing: comparison of three different extraction methods, Food Chem., 2009, 112, 4, 1072-1078, https://doi.org/10.1016/j.foodchem.2008.07.015 . [all data]

Radulovic, Blagojevic, et al., 2009
Radulovic, N.S.; Blagojevic, P.D.; Palic, R.M.; Zlatkovic, B.K.; Stevanovic, B.M., Volatiles from vegetative organs of the paleoendemic resurrection plants Ramonda serbica Panc. and Ramonda nathaliae Panc. at Petrov, J. Serb. Chem. Soc., 2009, 74, 1, 35-44, https://doi.org/10.2298/JSC0901035R . [all data]

Rahmi-Nasrabadi, Gholivand, et al., 2009
Rahmi-Nasrabadi, M.; Gholivand, M.B.; Batooli, H., Chemical composition of the essential oil from leaves and flowering aerial parts of Haplophyllum robustum Bge. (Rutaceae), Digest J. Nanomaterials Biostructures, 2009, 4, 4, 819-822. [all data]

Retta, Gattuso, et al., 2009
Retta, D.; Gattuso, M.; Gattuso, S.; Lira, P. Di Leo; van Baren, C.; Ferraro, G.; Bandoni A., Essential oil composition of Achyrocline flaccida (Weinm.) DC. (Asteraceae) from different locations of Argentina, Biochem. Systematics Ecol., 2009, 36, 12, 877-881, https://doi.org/10.1016/j.bse.2008.11.001 . [all data]

Romeo, Verzera, et al., 2009
Romeo, V.; Verzera, A.; Ziino, M.; Condurao, C.; Tripodi, G., Headspace volatiles of Vicia sativa L. (Legumnodeae) by solid-phase microextraction and gas chromatography/mass spectrometry, J. Ess. Oil Res., 2009, 21, 1, 33-35, https://doi.org/10.1080/10412905.2009.9700101 . [all data]

Scrivanti, Anton, et al., 2009
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