α-Terpineol

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Normal alkane RI, polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-20M InnowaxSupelco CO Wax-10Supelco CO Wax-10Supelco CO Wax-10DB-Wax
Column length (m) 30.60.60.60.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50 0C (7 min) 20 0C/min -> 130 0C (1 min) 1 0C/min -> 150 0C 8 0C/min -> 190 0C (5 min)35 0C (6 min) 2 0C/min -> 60 0C (5 min) 5 0C/min -> 200 0C 25 0C/min -> 250 0C (6 min)not specifiednot specifiednot specified
I 1693.1701.1705.1715.1659.
ReferenceWang, Tian, et al., 2013Prompona, Kandylis, et al., 2012Prompona, Kandylis, et al., 2012Prompona, Kandylis, et al., 2012Welke, Manfroi, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxInnowax FSCHP-InnowaxSOLGel-WaxSOLGel-Wax
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0Cnot specified40 0C (2 min) 5 0C/min -> 140 0C 10 0C/min -> 250 0C (3 min)not specified
I 1668.1706.1706.1703.1718.
ReferenceWelke, Manfroi, et al., 2012Demirci, Temel, et al., 2011Feng, Cui, et al., 2011Johanningsmeier and McFeeters, 2011Johanningsmeier and McFeeters, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP InnowaxInnowaxDB-WaxFFAPHP Innowax
Column length (m) 30.60.30.25.60.
Carrier gas Nitrogen HeliumNitrogen 
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.330.250.300.33
Program 35 0C (10 min) 3 0C/min -> 205 0C 10 0C/min -> 225 0Cnot specifiednot specified36 0C 20 0C/min -> 85 0C 1 0C/min -> 145 0C 3 0C/min -> 250 0Cnot specified
I 1700.1706.1712.1706.1706.
ReferenceLaribi, Kouki, et al., 2011Noorizadeh, Farmany, et al., 2011Zeng, Xie, et al., 2011Bailly and Collin, 2010Noorizadeh and Farmany, 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCFFAPInnowax FSCCP-Wax 52 CBDB-Wax
Column length (m) 60.25.60.50.15.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.300.250.200.25
Program 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C36 0C 20 0C/min -> 85 0C 1 0C -> 145 0C 3 0C/min -> 230 0C60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C60 0C (5 min) 3 0C/min -> 250 0C (20 min) 1 0C/min -> 255 0C50 0C (5 min) 6 0C/min -> 125 0C 10 0C/min -> 170 0C
I 1706.1706.1707.1691.1671.
ReferencePolatoglu, Demirci, et al., 2010Bailly, Jerkovic, et al., 2009Baser, Demirci, et al., 2009Genisheva and Oliveira, 2009Keefover-Ring, Thompson, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxHP InnowaxCP-Wax 52 CBHP Innowax FSP
Column length (m) 15.60.50.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (μm) 0.250.500.250.250.25
Program 50 0C (5 min) 6 0C/min -> 125 0C 10 0C/min -> 170 0C40 0C (3 min) 10 0C/min -> 90 0C 2 0C/min -> 230 0C (37 min)40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)45 0C (5 min) 3 0C/min -> 150 0C 10 0C/min -> 240 0C60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C (20 min)
I 1678.1705.1706.1696.1706.
ReferenceKeefover-Ring, Thompson, et al., 2009Loscos, Hernandez-Orte, et al., 2009Mancini, Arnold, et al., 2009Romeo, Verzera, et al., 2009Wedge, Klun, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-20MInnowaxCP-Wax 52 CBDB-WaxHP-Innowax FSC
Column length (m) 25.30.50.30.60.
Carrier gas HeliumHeliumHeliumHeliumN2
Substrate      
Column diameter (mm) 0.200.250.250.320.25
Phase thickness (μm) 0.200.250.290.250.25
Program 30 0C (1 min) 50 0C/min -> 110 0C 1.5 0C/min -> 145 0C 4 0C/min -> 220 0C (10 min)not specified33 0C (1 min) 2 0C/min -> 130 0C 10 0C/min -> 220 0C40 0C (3 min) 4 0C/min -> 160 0C 7 0C/min -> 220 0C (8 min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1688.1694.1681.1718.1706.
ReferenceZellner, Amorim, et al., 2009Aicha, Ines, et al., 2008Kaack and Christensen, 2008Li, Tao, et al., 2008Baser K.H.C. and Demirci B., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10HP-InnowaxCarbowax 20MInnowax FSCDB-Wax
Column length (m) 30.50.30.60.30.
Carrier gas HeHeHeNitrogenHe
Substrate      
Column diameter (mm) 0.250.20.250.250.32
Phase thickness (μm) 0.250.20.250.250.25
Program 40C(10min) => 2C/min => 200C(1min) => 2C/min => 250C (10min)40C(5min) => 2C/min => 250C(15min) => 10C/min => 270Cnot specified60 0C (10 min) 1 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C40C(3min) => 4C/min => 160C => 7C/min => 230C (8min)
I 1710.1707.1705.1706.1718.
ReferenceBosch-Fuste, Riu-Aumatell, et al., 2007Formisano, Mignola, et al., 2007Hudaib and Aburjai, 2007Kaya, Benirci, et al., 2007Li, Tao, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-Wax EtrHP-InnowaxDB-WaxInnowax FSCHP Innowax FSP
Column length (m) 60.30.30.60.60.
Carrier gas HeHeliumHydrogenHeN2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.50.250.500.250.25
Program 40C(3min) => 10C/min => 90C => 2C/min => 230C (37min)30 0C (5 min) 5 0C/min -> 100 0C (5 min) 1 0C/min -> 130 0C 10 0C/min -> 195 0C (45 min)60 0C (3 min) 2 0C/min -> 220 0C 3 0C/min -> 245 0C (20 min)60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1705.1687.1697.1706.1706.
ReferenceLoskos, Hernandez-Orte, et al., 2007Narain, Galvao, et al., 2007Selli, 2007Tabanca, Demirci, et al., 2007Tabanca N., Demirci B., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxFFAP-CBFFAPInnowax FSC
Column length (m) 30.30.25.25.60.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.300.30.25
Program 50 0C (2 min) 6 0C/min -> 150 0C 8 0C/min -> 230 0C (15 min)40 0C (3 min) 3 0C/min -> 150 0C (2 min) 6 0C/min -> 230 0C (10 min)36 0C 20 0C/min -> 85 0C 1 0C/min -> 1345 0C 3 0C/min -> 250 0C36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C
I 1680.1687.1706.1706.1706.
ReferenceTian, Zhang, et al., 2007Wenguang, Wenlai, et al., 2007Bailly, Jerkovic, et al., 2006Bailly, Jerkovic, et al., 2006, 2Baser K.H.C., Ozek G., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-Innowax FSCInnowax FSCHP-Innowax FSCCarbowax 20M
Column length (m) 60.60.60.60.25.
Carrier gas N2HeN2HeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C40C(8min) => 3C/min => 180C => 20C/min => 230C (10min)
I 1706.1706.1706.1706.1662.
ReferenceDemirci B., Baser K.H.C., et al., 2006Erdurak, Coskun, et al., 2006Iscan, Kirimer, et al., 2006Kürkçüoglu, Hüsnü Can Baser, et al., 2006Lorenzo, Loayza, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxHP-InnowaxHP-Innowax FSCHP-Innowax FSCHP-Innowax FSC
Column length (m) 60.50.60.60.60.
Carrier gas NitrogenHeHe N2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Program 50 0C (4 min) -> 40 0C 4 0C/min -> 220 0C40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C60(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C => (10min) => 1C/min => 240C
I 1681.1706.1706.1706.1706.
ReferenceQuijano and Pino, 2006Senatore, Apostolides Arnold, et al., 2006Suleimenov Y.M., Atazhanova G.A., et al., 2006Tabanca, Demirci, et al., 2006Tabanca, Demirci, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP-InnowaxHP-Innowax FSCHP-InnowaxCarbowax 20M
Column length (m) 30.60.60.60. 
Carrier gas HeN2N2N2 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (μm) 0.250.250.250.25 
Program not specified60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified
I 1661.1706.1706.1706.1670.
ReferenceBerlinet, Ducruet, et al., 2005Demirci, Demirci, et al., 2005Demirci, Demirci, et al., 2005, 2Duman, Kartal, et al., 2005Editorial paper, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MDB-WaxInnowax FSCDB-WaxHP-Innowax FSC
Column length (m)  30.60. 60.
Carrier gas  HeHeN2He
Substrate      
Column diameter (mm)  0.250.25 0.25
Phase thickness (μm)  0.250.25 0.25
Program not specified35C(5min) => 2C/min => 173C(1min) => 15C/min => 210C(5min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1685.1667.1706.1700.1707.
ReferenceEditorial paper, 2005Giuseppe, Manuela, et al., 2005Kosar, Özek, et al., 2005Pala-Paul, Perez-Alonso, et al., 2005Sezik E., Kocakulak E., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCInnowax FSCHP-Innowax FSCHP-Innowax FSCHP-Innowax FSC
Column length (m) 60.60.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1706.1706.1706.1706.1706.
ReferenceViljoen, Subramoney, et al., 2005Baser, Özek, et al., 2004Demirci, Paper, et al., 2004Kivcak, Akay, et al., 2004Kivcak, Akay, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCCarbowax 20MCarbowax 20MInnowax FSCHP-Innowax FSC
Column length (m) 60.  60.60.
Carrier gas N2  HeHe
Substrate      
Column diameter (mm) 0.25  0.250.25
Phase thickness (μm) 0.25  0.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specifiednot specified60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C
I 1706.1693.1691.1706.1706.
ReferenceKlika, Demirci, et al., 2004Vinogradov, 2004Vinogradov, 2004Baser, Demirci, et al., 2003Demirci, Baser, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-Innowax FSCCarbowaxHP-Innowax FSCHP-Innowax FSC
Column length (m) 60.60. 60.60.
Carrier gas HeHe HeN2
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm) 0.250.25 0.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1706.1706.1665.1706.1706.
ReferenceDemirci, Dadandi, et al., 2003Demirci, Demirci, et al., 2003Edris, Shalaby, et al., 2003Erdemoglu, Sener, et al., 2003Kaya, Demirci, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-FFAPCarbowax 20MDB-WaxHP Innowax FSP
Column length (m) 60.30.50.30.60.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.700.320.25
Phase thickness (μm) 0.25  0.50.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C(40min)60C (2min) => 5C/min => 160C (1min) => 10C/min => 230C (12min)not specified60C(2min) => 2C/min => 220C => 3C/min => 245C(20min)60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C
I 1706.1732.1661.1679.1706.
ReferenceKürkcüoglu, Demirci, et al., 2003Mockute and Judzentiene, 2003Saura, LAencina, et al., 2003Selli, Cabaroglu, et al., 2003Tasdemir, Demirci, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP Innowax FSPInnowaxHP-InnowaxHP-InnowaxInnowax FSC
Column length (m) 60.60.60.60.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C (20min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1706.1706.1706.1707.1706.
ReferenceTasdemir, Demirci, et al., 2003Tunaher, Kirimer, et al., 2003Viljoen, van Vuuren, et al., 2003Baser, Demirci, et al., 2002Baser, Demirei, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxHP-InnowaxHP-Innowax FSCSupelcowax-10HP-FFAP
Column length (m) 60.60.60.60.25.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.250.250.25 
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C40C (7min) => 4C/min => 150C => 8C/min => 240C (10min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 230C(12min)
I 1706.1706.1706.1730.1732.
ReferenceBaser, Nuriddinov, et al., 2002Demirci, Baser, et al., 2002Hüsnü Can Baser, Demirci, et al., 2002Kim and Lee, 2002Mockute and Judzentiene, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TRWAXInnowax FSCHP-InnowaxHP-InnowaxHP-Innowax FSC
Column length (m) 60.60.60.60.60.
Carrier gas He HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (10 min) 10 K/min -> 220 0C (10 min) 1K/min -> 240 0C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1728.1707.1706.1706.1706.
ReferenceTorrens, 2002Tunalier, Kirimer, et al., 2002Baser, Demirci, et al., 2001Gören, Demirci, et al., 2001Kaya, Demirci, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-Innowax FSCDB-WaxDB-WaxInnowax
Column length (m) 60.60.30.30.60.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C50C(4min) => 4C/min => 130C => 1C/min => 190C => 4C/min => 220C(20min)50C(4min) => 4C/min => 130C => 1C/min => 190C => 4C/min => 220C(20min)60C(10min) => 4C/min => 200C(10min) => 1C/min => 240C
I 1706.1706.1675.1679.1707.
ReferenceKirimer N., Tabanea N., et al., 2001Kivcak B., Mert T., et al., 2001Mayorga, Knapp, et al., 2001Mayorga, Knapp, et al., 2001Özcan, Akgül, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Innowax FSCDB-WaxInnowax FSCHP-Innowax FSC
Column length (m) 60.60.30.60.60.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.50.250.25
Program 40C(20min) => 1.5C/min => 200C(4min) => 10C/min => 250C(120min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C30C => 70C/min => 60C (3min) => 3C/min => 245C (20min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1694.1706.1698.1706.1707.
ReferenceRogerson, Castro, et al., 2001Saglam, Gozler, et al., 2001Schneider, Razungles, et al., 2001Tabanca N., Demirci F., et al., 2001Tabanca, Kirimer, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxFFAPHP-WaxInnowaxInnowax
Column length (m) 60.50.60.60.60.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.330.25 0.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(1min) => 2.5C/min => 115C => 1C/min => 210C(30min)50 0C 3 K/min -> 200 0C 8 K/min -> 280 0C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
I 1706.1686.1729.1706.1707.
ReferenceTabanca, Kirimer, et al., 2001, 2Tucker, Maciarello, et al., 2001Usubillaga, Aparicio, et al., 2001Ahmed, Choudhary, et al., 2000Baser, Özek, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxInnowax FSCFFAPSupelcowax-10HP-Innowax FSC
Column length (m) 60.60.50. 60.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.250.250.2 0.25
Phase thickness (μm) 0.250.250.33 0.25
Program 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10 min) => 4C/min => 220C(10min) => 1C/min => 240C70C(1min) => 3C/min => 142C(2min) => 25C/min => 230C(5min)not specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1707.1707.1723.1714.1707.
ReferenceBaser, Tabanca, et al., 2000Kirimer, Tabanca, et al., 2000Lopez, Lavilla, et al., 2000Zunino, Lopez, et al., 2000Bagci, Baser, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCInnowax FSCFFAPDB-WaxDB-Wax
Column length (m) 60.60.25.60.60.
Carrier gas HeHeliumH2N2N2
Substrate      
Column diameter (mm) 0.250.250.2  
Phase thickness (μm) 0.250.250.330.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C(20min)60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C40C(5min) => 4C/min => 170C => 8C/min => 240C (12min)not specifiednot specified
I 1707.1707.1691.1700.1709.
ReferenceKamariah, Lim, et al., 1999Kirimer, Tabanca, et al., 1999Reddy, Angers, et al., 1998Weyerstahl, Marschall, et al., 1998Weyerstahl, Marschall, et al., 1998, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCP-Wax 52CBSupelcowax 10Supelcowax 10Supelcowax 10
Column length (m) 60.25.60.60.60.
Carrier gas HeH2HeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.30.250.250.25
Phase thickness (μm)  1.20.250.250.25
Program 45C(4min) => 30C/min => 60C (5min) => 3C/min => 220C(40min)60C(3min) => 2C/min => 220C => 3C/min => 245C60 0C (10 min) 2 0C/min -> 80 0C 3 0C/min -> 100 0C 4 0C/min -> 220 0C (30 min)not specifiednot specified
I 1711.1697.1688.1688.1698.
ReferenceZiegleder, 1998López-Tamames, Carro-Mariño, et al., 1997Castioni and Kapetanidis, 1996Castioni and Kapetanidis, 1996Castioni and Kapetanidis, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52 CBCarbowax 20MSupelcowaxCarbowax 20MNB-351
Column length (m) 30.60.30. 25.
Carrier gas H2He He 
Substrate      
Column diameter (mm) 0.320.250.25 0.32
Phase thickness (μm)  0.25  0.2
Program 60 0C 2 0C/min -> 220 0C 3 0C/min -> 245 0Cnot specifiednot specifiednot specified40C(5min) => 4C/min => 150C => 8C/min => 240C(12min)
I 1697.1740.1684.1661.1695.
ReferenceCarro Marino, López Tamames, et al., 1995Tirado, Stashenko, et al., 1995Garneau, Bouhajib, et al., 1994Chanegriha and Baaliouamer, 1993Kerrola and Kallio, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxSupelcowax-10CP-Wax 52CBPolyethylene Glycol
Column length (m) 30.30.30.50. 
Carrier gas He    
Substrate      
Column diameter (mm) 0.250.250.530.32 
Phase thickness (μm)  0.250.25  
Program not specifiednot specified80C(5min) => 5C/min => 155C => 4C/min => 240C(30min)not specifiednot specified
I 1671.1687.1708.1680.1687.
ReferenceHatsuko, Kazuko, et al., 1992Marlatt, Ho, et al., 1992Miranda-Lopez, Libbey, et al., 1992Vernin, 1991Vernin, Metzger, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-WaxCarbowax 20MPolyethylene Glycol
Column length (m) 60.  
Carrier gas    
Substrate    
Column diameter (mm) 0.32  
Phase thickness (μm)    
Program not specifiednot specifiednot specified
I 1695.1661.1661.
ReferenceBinder and Flath, 1989Shibamoto, 1987MacLeod and Pieris, 1981
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Mancini, Arnold, et al., 2009
Mancini, E.; Arnold, N.A.; De Martino, L.; De Feo, V.; Formisano, C.; Rigano, D.; Senatore, F., Chemical composition and phytotoxic effects of essential oils of Salvia hierosolymitana Boiss. and Salvia multicaulis Vahl. var. simplicifolia Boiss. growing wild in Lebanon, Molecules, 2009, 14, 11, 4725-4736, https://doi.org/10.3390/molecules14114725 . [all data]

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Wedge, Klun, et al., 2009
Wedge, D.E.; Klun, J.A.; Tabanca, N.; Demirci, B.; Ozek, T.; Baser, K.H.C.; Liu, Z.; Zhang, S.; Cantrell, C.L.; Zhang, J., Bioactivity-guided fractionation and GC/MS fingerprinting of Amgelica sinensis and Angelica archangelica root components for antifungal and mosquito deterrent activity, J. Agric. Food Chem., 2009, 57, 2, 464-470, https://doi.org/10.1021/jf802820d . [all data]

Zellner, Amorim, et al., 2009
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Aicha, Ines, et al., 2008
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Kaack and Christensen, 2008
Kaack, K.; Christensen, L.P., Effect of packing materials and storage time on volatile compounds in tea processes from flowers of black elder (Sambucus nigra L.), Eur. Food Res. Technol., 2008, 227, 4, 1259-1273, https://doi.org/10.1007/s00217-008-0844-8 . [all data]

Li, Tao, et al., 2008
Li, H.; Tao, Y.-S.; Wang, H.; Zhang, L., Impact odorants of Chardonnay dry white wine from Changli Counti (China), Eur. Food. Res. Technol., 2008, 227, 1, 287-292, https://doi.org/10.1007/s00217-007-0722-9 . [all data]

Baser K.H.C. and Demirci B., 2007
Baser K.H.C.; Demirci B., Studies on Betula essential oils, Arkivoc, 2007, 7, 335-348. [all data]

Bosch-Fuste, Riu-Aumatell, et al., 2007
Bosch-Fuste, J.; Riu-Aumatell, M.; Guadayol, J.M.; Caixach, J.; Lopez-Tamames, E.; Buxaderas, S., Volatile profiles of sparkling wines obtained by three extraction methods and gas chromatography-mass spectrometry (GC-MS) analysis, Food Chem., 2007, 105, 1, 428-435, https://doi.org/10.1016/j.foodchem.2006.12.053 . [all data]

Formisano, Mignola, et al., 2007
Formisano, C.; Mignola, E.; Rigano, D.; Senatore, F.; Bellone, G.; Bruno, M.; Rosselli, S., Chemical composition and antimicrobial activity of the essential oil from aerial parts of Micromeria fruticulosa (Bertol.) Grande (Lamiaceae) growing wild in Southern Italy, Flavour Fragr. J., 2007, 22, 4, 289-292, https://doi.org/10.1002/ffj.1795 . [all data]

Hudaib and Aburjai, 2007
Hudaib, M.; Aburjai, T., Volatile components of Thymus vulgaris L. from wild-growing and cultivated plants in Jordan, Flavour Fragr. J., 2007, 22, 4, 322-327, https://doi.org/10.1002/ffj.1800 . [all data]

Kaya, Benirci, et al., 2007
Kaya, A.; Benirci, B.; Baser, K.H.C., Micromorphology of glandular trichomes of Nepeta congesta Fisch. Mey. var. congesta (LAmiaceae) and chemical analysis of the essential oils, South African J. Botany, 2007, 73, 1, 29-34, https://doi.org/10.1016/j.sajb.2006.05.004 . [all data]

Li, Tao, et al., 2007
Li, H.; Tao, Y.-S.; Wang, H.; Zhang, L., Impact odorants of Chardonnay dry white wine from Changli County (China), Eur. Food Res. Technol., 2007, https://doi.org/10.1007/s00217-007-0722-9 . [all data]

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Selli, 2007
Selli, S., Volatile constituents of orange obtained from moro oranges (Citrus Sinensis L. Osbeck), J. Food Quality, 2007, 30, 3, 330-341, https://doi.org/10.1111/j.1745-4557.2007.00124.x . [all data]

Tabanca, Demirci, et al., 2007
Tabanca, N.; Demirci, F.; Demirci, B.; Wedge, D.E.; Baser, K.H.C., Composition, enantiomeric distribution, and antimicrobial activity of Tanacetum argenteum subsp. ?abellifolium essential oil, J. Pharm. Biomed. Anal., 2007, 45, 5, 714-719, https://doi.org/10.1016/j.jpba.2007.08.006 . [all data]

Tabanca N., Demirci B., et al., 2007
Tabanca N.; Demirci B.; Crockett S.L.; Baser K.H.C.; Wedge D.E., Chemical composition and antifungal activity of Arnica longifolia, Aster hesperius, and Chrysothamnus nauseosus essential oils, J. Agric. Food Chem., 2007, 55, 21, 8430-8435, https://doi.org/10.1021/jf071379c . [all data]

Tian, Zhang, et al., 2007
Tian, Y.; Zhang, X.; Huang, T.; Zou, K.; Zhou, J., Research advances on the essential oils from leaves of Eucalyptus, Food Fermentation Ind. (Chinese), 2007, 33, 10, 143-147. [all data]

Wenguang, Wenlai, et al., 2007
Wenguang, J.; Wenlai, F.; Yan, X.; Guangao, Z.; Jiming, L.; Ying, Y., Analysis of free terpenoids in four Vitis vinifera varietis using solvent assisted flavour evaporation and gas chromatography-tandem mass spectrometry, Chinese J. Chromatogr., 2007, 25, 6, 881-886, https://doi.org/10.1016/S1872-2059(08)60006-1 . [all data]

Bailly, Jerkovic, et al., 2006
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Bailly, Jerkovic, et al., 2006, 2
Bailly, S.; Jerkovic, V.; Marchand-Brynaert, J.; Collin, S., Aroma Extraction Dilution Analysis of Sauternes Wines. Key Role of Polyfunctional Thiols, J. Agric. Food Chem., 2006, 54, 19, 7227-7234, https://doi.org/10.1021/jf060814k . [all data]

Baser K.H.C., Ozek G., et al., 2006
Baser K.H.C.; Ozek G.; Ozek T.; Duran A., Composition of the essential oil of Centaurea huber-morathii Wagenitz isolated from seeds by microdistillation, Flavour Fragr. J., 2006, 21, 3, 568-570, https://doi.org/10.1002/ffj.1620 . [all data]

Demirci B., Baser K.H.C., et al., 2006
Demirci B.; Baser K.H.C.; Tabanca N.; Wedge D.E., Characterization of volatile constituents of Haplopappus greenei and studies on the antifungal activity against phytopathogens, J. Agric. Food Chem., 2006, 54, 8, 3146-3150, https://doi.org/10.1021/jf053222v . [all data]

Erdurak, Coskun, et al., 2006
Erdurak, C.S.; Coskun, M.; Demirci, B.; Baser, K.H.C., Composition of the essential oil of fruits and roots of Ferulago isaurica Pesmen and F. syriaca Boiss. (Umbelliferae) from Turkey, Flavour Fragr. J., 2006, 21, 1, 118-121, https://doi.org/10.1002/ffj.1540 . [all data]

Iscan, Kirimer, et al., 2006
Iscan, G.; Kirimer, N.; Kurkcuoglu, M.; Arabaci, T.; Kupeli, E.; Baser, K.H.C., Biological Activity and Composition of the Essential Oils of Achillea schischkinii Sosn. and Achillea aleppica DC. subsp. aleppica, J. Agric. Food Chem., 2006, 54, 1, 170-173, https://doi.org/10.1021/jf051644z . [all data]

Kürkçüoglu, Hüsnü Can Baser, et al., 2006
Kürkçüoglu, M.; Hüsnü Can Baser, K.; Iscan, G.; Malyer, H.; Kaynak, G., Composition and anticandidal activity of the essential oil of Chaerophyllum byzantinum Boiss., Flavour Fragr. J., 2006, 21, 1, 115-117, https://doi.org/10.1002/ffj.1539 . [all data]

Lorenzo, Loayza, et al., 2006
Lorenzo, D.; Loayza, I.; Dellacassa, E., Composition and chiral characterization of the essential oil of Buddleja tucumanensis from Bolivia, Flavour Fragr. J., 2006, 21, 1, 95-98, https://doi.org/10.1002/ffj.1526 . [all data]

Quijano and Pino, 2006
Quijano, C.E.; Pino, J.A., Changes in volatile constituents during the ripening of cocona (Solanum sessiliflorum Dunal) fruit, Revista CENIC Ciencias Quimicas, 2006, 37, 3, 133-136. [all data]

Senatore, Apostolides Arnold, et al., 2006
Senatore, F.; Apostolides Arnold, N.; Piozzi, F.; Formisano, C., Chemical composition of the essential oil of Salvia microstegia Boiss. et Balansa growing wild in Lebanon, J. Chromatogr. A, 2006, 1108, 2, 276-278, https://doi.org/10.1016/j.chroma.2006.01.066 . [all data]

Suleimenov Y.M., Atazhanova G.A., et al., 2006
Suleimenov Y.M.; Atazhanova G.A.; Ozek T.; Demirci B.; Kulyyasov A.T.; Adekenov S.M.; Baser K.H.C., Essential oil composition of three species of Achillea from Kazakhstan, Chem. Nat. Compd. (Engl. Transl.), 2006, 37, 5, 447-450, https://doi.org/10.1023/A:1014471326724 . [all data]

Tabanca, Demirci, et al., 2006
Tabanca, N.; Demirci, B.; Ozek, T.; Kirimer, N.; Can Baser, K.H.; Bedir, E.; Khan, I.A.; Wedge, D.E., Gas chromatographic-mass spectrometric analysis of essential oils from Pimpinella species gathered from Central and Northern Turkey, J. Chromatogr. A, 2006, 1117, 2, 194-205, https://doi.org/10.1016/j.chroma.2006.03.075 . [all data]

Tabanca, Demirci, et al., 2006, 2
Tabanca, N.; Demirci, B.; Can Baser, K.H.; Aytac, Z.; Ekici, M.; Khan, S.I.; Jacob, M.R.; Wedge, D.E., Chemical Composition and Antifungal Activity of Salvia macrochlamys and Salvia recognita Essential Oils, J. Agric. Food Chem., 2006, 54, 18, 6593-6597, https://doi.org/10.1021/jf0608773 . [all data]

Berlinet, Ducruet, et al., 2005
Berlinet, C.; Ducruet, V.; Brillouet, J.-M.; Reynes, M.; Brat, P., Evolution of aroma compounds from orange juice stored in polyethylene terephthalate (PET), Food Addit. Contam., 2005, 22, 2, 185-195, https://doi.org/10.1080/02652030500037860 . [all data]

Demirci, Demirci, et al., 2005
Demirci, B.; Demirci, F.; Baser, K.H.C., Headspace-SPME and hydrodistillation of two fragrant Artemisia sp., Flavour Fragr. J., 2005, 20, 4, 395-398, https://doi.org/10.1002/ffj.1426 . [all data]

Demirci, Demirci, et al., 2005, 2
Demirci, B.; Demirci, F.; Dönmez, A.A.; Franz, G.; Paper, D.H.; Baser, K.H.C., Effects of Salvia essential oils on the chorioallantoic membrane (CAM) assay, Pharm. Biol., 2005, 43, 8, 666-671, https://doi.org/10.1080/13880200500383397 . [all data]

Duman, Kartal, et al., 2005
Duman, H.; Kartal, M.; Altun, L.; Demirci, B.; Baser, K.H.C., The essential oil of Stachys laetivirens Kotschy Boiss. ex Rech. fil., endemic in Turkey, Flavour Fragr. J., 2005, 20, 1, 48-50, https://doi.org/10.1002/ffj.1362 . [all data]

Editorial paper, 2005
Editorial paper, Solid Phase Microextraction (SPME) Application Guide, The Reporter Europe (Supelco), 2005, 16, 5, 12-12. [all data]

Giuseppe, Manuela, et al., 2005
Giuseppe, Z.; Manuela, G.; Marta, B.; Vincenzo, G., Application of artificial neural network on mono- and sesquiterpenes compounds determined by headspace solid-phase microextraction-gas chromatography-mass spectrometry for the Piedmont ricotta cheese traceability, J. Chromatogr. A, 2005, 1071, 1-2, 247-253, https://doi.org/10.1016/j.chroma.2004.11.083 . [all data]

Kosar, Özek, et al., 2005
Kosar, M.; Özek, T.; Göger, F.; Kürkcüoglu, M.; Hüsnü Can Baser, K., Comparison of Microwave-Assisted Hydrodistillation and Hydrodistillation Methods for the Analysis of Volatile Secondary Metabolites, Pharm. Biol., 2005, 43, 6, 491-495, https://doi.org/10.1080/13880200500220136 . [all data]

Pala-Paul, Perez-Alonso, et al., 2005
Pala-Paul, J.; Perez-Alonso, M.J.; Velasco-Negueruela, A.; Vadare, J.; Villa, A.M.; Sanz, J.; Brophy, J.J., Essential oil composition of the different parts of Eryngium bourgatii Gouan from Spain, J. Chromatogr. A, 2005, 1074, 1-2, 235-239, https://doi.org/10.1016/j.chroma.2005.03.036 . [all data]

Sezik E., Kocakulak E., et al., 2005
Sezik E.; Kocakulak E.; Baser K.H.C.; Ozek T., Composition of the essential oils of Juniperus oxycedrus subsp macrocarpa from Turkey, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 3, 352-354, https://doi.org/10.1007/s10600-005-0149-0 . [all data]

Viljoen, Subramoney, et al., 2005
Viljoen, A.M.; Subramoney, S.; van Vuuren, S.F.; Baser, K.H.C.; Demirci, B., The composition, geographical variation and antimicrobial activity of Lippia javanica (Verbenaceae) leaf essential oils, J. Ethnopharmacol., 2005, 96, 1-2, 271-277, https://doi.org/10.1016/j.jep.2004.09.017 . [all data]

Baser, Özek, et al., 2004
Baser, K.H.C.; Özek, T.; Kirimer, N.; Deliorman, D.; Ergun, F., Composition of the essential oils of Galium aparine L. and Galium odoratum (L.) Scop. from Turkey, J. Essent. Oil Res., 2004, 16, 4, 305-307, https://doi.org/10.1080/10412905.2004.9698728 . [all data]

Demirci, Paper, et al., 2004
Demirci, F.; Paper, D.H.; Franz, G.; Hüsnü Can Baser, K., Investigation of the origanum onites L. essential oil using the Chorioallantoic Membrane (CAM) assay, J. Agric. Food Chem., 2004, 52, 2, 251-254, https://doi.org/10.1021/jf034850k . [all data]

Kivcak, Akay, et al., 2004
Kivcak, B.; Akay, S.; Demirci, B.; Baser, K.H.C., Chemical composition of essential oils from leaves and twigs of Pistacia lentiscus, Pistacia lentiscus var. chia, and Pistacia terebinthus from Turkey, Pharm. Biol, 2004, 42, 4-5, 360-366, https://doi.org/10.1080/13880200490519677 . [all data]

Klika, Demirci, et al., 2004
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Notes

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