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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Polydimethyl siloxaneSE-54HP-1DB-5 MS
Column length (m) 30. 30.50.60.
Carrier gas Hydrogen HeliumHeliumHelium
Column diameter (mm) 0.32 0.320.200.32
Phase thickness (mum) 0.50 0.250.331.0
Program 40 0C (5 min) 4 0C/min -> 100 0C 6 0C/min -> 220 0C (20 min)40 0C 20 0C/min -> 60 0C (5 min) 4 0C/min -> 250 0C35 0C (2 min) 10 0C/min -> 50 0C (2 min) 6 0C/min -> 250 0Cnot specified40 0C (2 min) 6 0C/min -> 100 0C 4 0C/min -> 180 0C 8 0C/min -> 250 0C (12 min)
I 907.913.911.878.912.
ReferenceSan-Juan, Petka, et al., 2010Xu, He, et al., 2010Christlbauer and Schieberle, 2009Breme, Langle, et al., 2008Liu, Xu, et al., 2007
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1SE-30DB-5DB-5
Column length (m) 50.12. 30.30.
Carrier gas He   Helium
Column diameter (mm) 0.320.32 0.530.25
Phase thickness (mum) 0.520.52 1.50.25
Program 40C => 2C/min => 130C => 4C/min => 250C (25min)35C(3min) => 6C/min => 190C => 30C/min => 225Cnot specified-5C(1min) => 4C/min => 50C => 6C/min => 120C => 8C/min => 250C(2min)35 0C (2 min) 40 0C/min -> 50 0C (1 min) 6 0C/min -> 180 0C 10 0C/min -> 240 0C (10 min)
I 890.892.890.906.911.
ReferenceSenger-Emonnot, Rochard, et al., 2006Carpino, Mallia, et al., 2004Vinogradov, 2004Bücking and Steinhart, 2002Lin, Fay, et al., 2000
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5Methyl SiliconeSE-54DB-1
Column length (m) 30.30.  60.
Carrier gas He   He
Column diameter (mm) 0.320.32  0.32
Phase thickness (mum) 0.25   1.0
Program 35C(1min) => 40C/min => 60C (1min) => 6C/min => 230Cnot specifiednot specified0C (2min) => 6C/min => 50C (2min) => 6C/min => 230 C (10min)35 0C (5 min), 2 0C/min to 150 0C, 3 0C/min to 260 0C (30 min)
I 910.912.880.912.883.
ReferenceMatsui, Guth, et al., 1998Schieberle, 1996Misharina, 1995Guth and Grosch, 1994Ruther and Baltes, 1994
Column type CapillaryCapillaryPacked
Active phase SE-54SE-54Apiezon M
Column length (m)   5.6
Carrier gas   N2
Substrate   Chromosorb W AW/DMCS
Column diameter (mm)    
Phase thickness (mum)    
Program not specifiednot specified60C(7min), 100C(7min), 150C isothermal
I 912.913.910.
ReferenceGuth and Grosch, 1993Blank, Sen, et al., 1992Golovnya, Misharina, et al., 1983


Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

San-Juan, Petka, et al., 2010
San-Juan, F.; Petka, J.; Cacho, J.; Ferreira, V.; Escudero, A., Producing headspace extracts for the gas chromatography - olphactometric evaluation of wine aroma, Food Chemistry, 2010, 123, 1, 188-195, https://doi.org/10.1016/j.foodchem.2010.03.129 . [all data]

Xu, He, et al., 2010
Xu, H.; He, W.; Liu, X.; Gao, Y., Effect of pressure on the Maillard reaction between ribose and cysteine in supercritical carbon dioxide, Czech J. Food Sci., 2010, 28, 3, 192-201. [all data]

Christlbauer and Schieberle, 2009
Christlbauer, M.; Schieberle, P., Characterization of the key aroma compounds in beef and pork vegetable gravies a la chef by application of the aroma extract dilution analysis, J. Agric. Food Chem., 2009, 57, 19, 9114-9112, https://doi.org/10.1021/jf9023189 . [all data]

Breme, Langle, et al., 2008
Breme, K.; Langle, S.; Fernandez, X.; Meierhenrich, U.J.; Brevard, H.; Joulain, D., Character impact odorants from Brassicaceae by aroma extracts dilution analysis (AEDA): Brassica cretica and Brassica insularis, Flavour Fragr. J., 2008, 24, 2, 88-93, https://doi.org/10.1002/ffj.1912 . [all data]

Liu, Xu, et al., 2007
Liu, Y.; Xu, X.-L.; Zhou, G.-H., Comparative study of volatile compounds in traditional Chinese Nanjing marinated duck by different extraction techniques, Int. J. Food Sci. Technol., 2007, 42, 5, 543-550, https://doi.org/10.1111/j.1365-2621.2006.01264.x . [all data]

Senger-Emonnot, Rochard, et al., 2006
Senger-Emonnot, P.; Rochard, S.; Pellegrin, F.; George, G.; Fernandez, X.; Lizzani-Cuvelier, L., Odour active aroma compounds of sea fig (Microcosmus sulcatus), Food Chem., 2006, 97, 3, 465-471, https://doi.org/10.1016/j.foodchem.2005.05.026 . [all data]

Carpino, Mallia, et al., 2004
Carpino, S.; Mallia, S.; Licitra, G.; van Soest, P.J.; Acree, T.E., Aroma compounds of some Hyblean pasture species, Flavour Fragr. J., 2004, 19, 4, 293-297, https://doi.org/10.1002/ffj.1346 . [all data]

Vinogradov, 2004
Vinogradov, B.A., Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]

Bücking and Steinhart, 2002
Bücking, M.; Steinhart, H., Headspace GC and sensory analysis characterization of the influence of different milk additives on the flavor release of coffee beverages, J. Agric. Food Chem., 2002, 50, 6, 1529-1534, https://doi.org/10.1021/jf011117p . [all data]

Lin, Fay, et al., 2000
Lin, J.; Fay, L.B.; Blank, I., Aroma impact compounds formed in meat-like model systems containing cysteine, ribose, and phospholipids in Frontiers of Flavour Science, Scheberle, P.; Engel, K.-H., ed(s)., Deutsche Forschungsanstalt fur Lebensmittelchemie, Garching, 2000, 498-502. [all data]

Matsui, Guth, et al., 1998
Matsui, T.; Guth, H.; Grosch, W., A comparative study of potent odorants in peanut, hazelnut, and pumpkin seed oils on the basis of aroma extract dilution analysis (AEDA) and gas chromatography-olfactometry of headspace samples (GCOH), Lipid - Fett, 1998, 100, 2, 51-56, https://doi.org/10.1002/(SICI)1521-4133(199802)100:2<51::AID-LIPI51>3.0.CO;2-W . [all data]

Schieberle, 1996
Schieberle, P., Odour-active compounds in moderately roasted sesame, Food Chem., 1996, 55, 2, 145-152, https://doi.org/10.1016/0308-8146(95)00095-X . [all data]

Misharina, 1995
Misharina, T.A., Sorption regularities of sulfur- and oxygen-containing compounds in chromatography and their application in identification of volatile organic compounds, Diss. degree of Dr. Sci. (Chemistry), 1995, 52. [all data]

Guth and Grosch, 1994
Guth, H.; Grosch, W., Identification of the character impact odorants of stewed beef juice by instrumental analyses and sensory studies, J. Agric. Food Chem., 1994, 42, 12, 2862-2866, https://doi.org/10.1021/jf00048a039 . [all data]

Ruther and Baltes, 1994
Ruther, J.; Baltes, W., Sulfur-containing furans in commercial meat flavorings, J. Agric. Food Chem., 1994, 42, 10, 2254-2259, https://doi.org/10.1021/jf00046a032 . [all data]

Guth and Grosch, 1993
Guth, H.; Grosch, W., 12-Methyltridecanal, a species-specific odorant of stewed beef, Lebensm. Wiss. Technol., 1993, 26, 2, 171-177, https://doi.org/10.1006/fstl.1993.1035 . [all data]

Blank, Sen, et al., 1992
Blank, I.; Sen, A.; Grosch, W., Potent odorants of the roasted powder and brew of Arabica coffee, Z. Lebensm. Unters Forsch., 1992, 195, 3, 239-245, https://doi.org/10.1007/BF01202802 . [all data]

Golovnya, Misharina, et al., 1983
Golovnya, R.V.; Misharina, T.A.; Garbuzov, V.G.; Medvedyev, F.A., Volatile sulfur containing compounds in simulated meat flavour and their comparison with the constituents of natural aroma, Nahrung, 1983, 27, 3, 237-249, https://doi.org/10.1002/food.19830270314 . [all data]


Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References