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Van Den Dool and Kratz RI, polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxHP-InnowaxDB-WaxDB-Wax
Column length (m) 30.30.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.50.50.250.250.25
Tstart (C) 40.40.50.40.40.
Tend (C) 250.250.220.200.265.
Heat rate (K/min) 4.4.4.4.7.
Initial hold (min) 5.5.4.1. 
Final hold (min) 15.15.10.10.5.
I 1460.1464.1439.1465.1480.
ReferencePozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007Quijano, Linares, et al., 2007Cho, Choi, et al., 2006Gurbuz O., Rouseff J.M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxZB-WaxInnowaxDB-WaxCP-Wax 52CB
Column length (m) 30.30.60.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (mum) 0.50.150.250.5 
Tstart (C) 40.35.40.40.60.
Tend (C) 265.220.230.240.220.
Heat rate (K/min) 7.5.4.5.4.
Initial hold (min)  5.4. 5.
Final hold (min) 5.10.20.10.30.
I 1476.1462.1458.1469.1456.
ReferenceGurbuz O., Rouseff J.M., et al., 2006Ledauphin, Basset, et al., 2006Lee, Lee, et al., 2006Lopez-Galilea I., Fournier N., et al., 2006Mahadevan and Farmer, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBCP-Wax 52CBDB-WaxDB-WaxOV-351
Column length (m) 50.50.60.30.50.
Carrier gas   H2HeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (mum)   0.250.250.2
Tstart (C) 60.60.30.40.60.
Tend (C) 220.220.230.250.220.
Heat rate (K/min) 4.4.3.3.5.
Initial hold (min) 5.5.2.  
Final hold (min) 30.30.4.20. 
I 1458.1468.1462.1432.1445.
ReferenceMahadevan and Farmer, 2006Mahadevan and Farmer, 2006Schwambach and Peterson, 2006Berlinet, Ducruet, et al., 2005Bonvehí, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPStabilwaxInnowaxInnowaxSupelcowax-10
Column length (m) 30.30.50.30.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.251.0.250.250.25
Tstart (C) 40.40.50.40.60.
Tend (C) 230.230.220.200.240.
Heat rate (K/min) 5.4.2.5.3.
Initial hold (min) 2.2.3.5.5.
Final hold (min) 6.10.20.2.10.
I 1455.1474.1471.1471.1454.
ReferenceColahan-Sederstrom and Peterson, 2005Fang and Qian, 2005Lee, Lee, et al., 2005Pena, Barciela, et al., 2005Riu-Aumatell, Lopez-Tamames, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MZB-WaxDB-WaxOV-351AT-Wax
Column length (m) 60.30.30.50.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.150.250.20.25
Tstart (C) 45.35.40.60.65.
Tend (C) 250.220.240.220.250.
Heat rate (K/min) 2.1.86.5.2.
Initial hold (min) 0.1710.10. 10.
Final hold (min)  10.25. 60.
I 1447.1462.1439.1438.1451.
ReferenceVerzera, Campisi, et al., 2005Ledauphin, Saint-Clair, et al., 2004Varming, Andersen, et al., 2004Bonvehi and Coll, 2003Pino, Almora, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10AT-WaxSupelcowax-10CP-Wax 52CB
Column length (m) 60.30.60.60.50.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 35.50.65.35.50.
Tend (C) 195.230.250.195.200.
Heat rate (K/min) 2.3.2.2.2.
Initial hold (min) 5. 10.5. 
Final hold (min) 90.30.60.90. 
I 1471.1456.1448.1471.1449.
ReferenceChung, Yung, et al., 2002Moreira, Trugo, et al., 2002Pino, Marbot, et al., 2002Chung, Yung, et al., 2001Liu, Yang, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-WaxAT-WaxCP-Wax 52CBDB-FFAPSupelcowax-10
Column length (m) 60.60.60.30.60.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.320.320.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 65.65.45.40.35.
Tend (C) 250.250.250.240.195.
Heat rate (K/min) 2.2.2.5.2.
Initial hold (min) 10.10.0.172. 
Final hold (min) 60.60.  90.
I 1452.1448.1447.1460.1472.
ReferencePino and Marbot, 2001Pino, Marbot, et al., 2001Verzera, Campisi, et al., 2001Charles, Martin, et al., 2000Chung, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBCP-Wax 52CBCP-Wax 52CBSupelcowax-10Supelcowax-10
Column length (m) 50.50.50.60.60.
Carrier gas    HeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum)    0.250.25
Tstart (C) 60.60.40.35.35.
Tend (C) 220.220.220.195.195.
Heat rate (K/min) 4.4.4.2.2.
Initial hold (min) 5.5.5.5.5.
Final hold (min) 30.30.30.90.90.
I 1460.1455.1462.1473.1472.
ReferenceChevance and Farmer, 1999Chevance and Farmer, 1999, 2Chevance and Farmer, 1999, 2Chung, 1999Chung, 1999, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxFFAPPEG-20MDB-WaxDB-Wax
Column length (m) 60.30.60.60.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.20.50.50.50.
Tend (C) 200.200.230.230.230.
Heat rate (K/min) 3.4.2.2.3.
Initial hold (min) 5.1.   
Final hold (min) 60.1.60.60. 
I 1458.1495.1456.1456.1467.
ReferenceCha, Kim, et al., 1998Ott, Fay, et al., 1997Shimoda, Nakada, et al., 1997Shimoda, Shiratsuchi, et al., 1996Shimoda, Wu, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.60.60.60.30.
Carrier gas  HeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25 0.25 
Tstart (C) 50.50.40.50.40.
Tend (C) 230.230.200.230.200.
Heat rate (K/min) 2.2.3.2.2.
Initial hold (min)   5.4.10.
Final hold (min)  60. 30. 
I 1447.1465.1466.1457.1451.
ReferenceShimoda, Shigematsu, et al., 1995Shiratsuchi, Shimoda, et al., 1994Sumitani, Suekane, et al., 1994Shiratsuchi, Shimoda, et al., 1993Umano, Hagi, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10CP-WAX 57CBCP-WAX 57CBCP-WAX 57CB
Column length (m) 60.60.50.50.50.
Carrier gas   He He
Substrate      
Column diameter (mm) 0.250.250.240.320.32
Phase thickness (mum) 0.250.25   
Tstart (C) 40.40.50.60.60.
Tend (C) 175.175.210.200.200.
Heat rate (K/min) 2.2.2.4.4.
Initial hold (min) 5.5.5.5.5.
Final hold (min) 20.20.  10.
I 1469.1471.1445.1455.1454.
ReferenceTanchotikul and Hsieh, 1989Tanchotikul and Hsieh, 1989Baltes and Mevissen, 1988Salter L.J., Mottram D.S., et al., 1988Whitfield, Mottram, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase CP-WAX 57CBCarbowax 20MCarbowax 20M
Column length (m) 50.50.50.
Carrier gas HeHeH2
Substrate    
Column diameter (mm) 0.320.320.2
Phase thickness (mum)    
Tstart (C) 60.50.50.
Tend (C) 200.200.200.
Heat rate (K/min) 4.2.2.
Initial hold (min) 5.5. 
Final hold (min) 10.40.55.
I 1455.1460.1429.
ReferenceWhitfield, Mottram, et al., 1988Chen, Kuo, et al., 1986Wu and Liou, 1986
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Sumitani, Suekane, et al., 1994
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Umano, Hagi, et al., 1992
Umano, K.; Hagi, Y.; Nakahara, K.; Shoji, A.; Shibamoto, T., Volatile constituents of green and ripened pineapple (Aanas comosus [L.] Merr.), J. Agric. Food Chem., 1992, 40, 4, 599-603, https://doi.org/10.1021/jf00016a014 . [all data]

Tanchotikul and Hsieh, 1989
Tanchotikul, U.; Hsieh, T.C.-Y., Volatile Flavor Components in Crayfish Waste, J. Food Sci., 1989, 54, 6, 1515-1520, https://doi.org/10.1111/j.1365-2621.1989.tb05149.x . [all data]

Baltes and Mevissen, 1988
Baltes, W.; Mevissen, L., Model reactions on roast aroma formation. VI. Volatile reaction products from the reaction of phenylalanine with glucose during cooking and roasting, Z. Lebensm. Unters. Forsch., 1988, 187, 3, 209-214, https://doi.org/10.1007/BF01043341 . [all data]

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Wu and Liou, 1986
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Notes

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