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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5SPB-5CP Sil 8 CBDB-5MS
Column length (m) 60.30.60.50.60.
Carrier gas  HeHe H2
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (mum) 1.0.251. 0.25
Tstart (C) 40.50.40.60.30.
Tend (C) 260.250.230.220.250.
Heat rate (K/min) 4.4.3.4.2.
Initial hold (min) 2.4.5.5.2.
Final hold (min) 10.10.5.30.2.
I 835.836.834.826.831.
ReferenceMethven L., Tsoukka M., et al., 2007Quijano, Salamanca, et al., 2007Deport, Ratel, et al., 2006Mahadevan and Farmer, 2006Schwambach and Peterson, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.251.0.250.25
Tstart (C) 60.40.40.60.60.
Tend (C) 250.230.230.220.250.
Heat rate (K/min) 10.5.4.5.4.
Initial hold (min) 2.2.2.10.2.
Final hold (min) 10.6.10. 20.
I 834.833.840.833.830.
ReferenceZhao J.Y., Liu J.M., et al., 2006Colahan-Sederstrom and Peterson, 2005Fang and Qian, 2005Flamini, Luigi Cioni, et al., 2005Pino, Mesa, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5ZB-5ZB-5CP-Sil 8CB-MSSPB-5
Column length (m) 25.30.0.60.30.
Carrier gas HeHelium  He
Substrate      
Column diameter (mm) 0.20.320.320.250.25
Phase thickness (mum) 1.0.500.50.250.25
Tstart (C) 40.40.40.40.60.
Tend (C) 280.265.265.280.250.
Heat rate (K/min) 5.7.7.4.4.
Initial hold (min)    2.2.
Final hold (min) 5.5.5.5.20.
I 841.850.832.839.830.
ReferenceSolina, Baumgartner, et al., 2005Bell, 2004Gocmen, Gurbuz, et al., 2004Hierro, de la Hoz, et al., 2004Píno, Marbot, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5SPB-5HP-5HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.251.0.10.25
Tstart (C) 60.60.-30.-30.50.
Tend (C) 250.250.250.250.200.
Heat rate (K/min) 4.4.10.10.6.
Initial hold (min) 2.2.1.1.1.5
Final hold (min) 20.20. 5.5.
I 830.817.829.830.839.
ReferencePino, Marbot, et al., 2004Pino, Marbot, et al., 2004, 2Siegmund, Derler, et al., 2004Siegmund and Murkovic, 2004Weissbecker, Holighaus, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSCP Sil 5 CBSPB-5CP Sil 8 CB
Column length (m) 30.60.60.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.40.
Tend (C) 240.310.280.250.250.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)  1.10.2.8.
Final hold (min)  20.60.20.10.
I 831.832.794.830.847.
ReferenceFlamini, Cioni, et al., 2003Lalel, Singh, et al., 2003Pino, Almora, et al., 2003Pino, Marbot, et al., 2003Duckham, Dodson, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5CP Sil 8 CBSPB-5CP Sil 5 CB
Column length (m) 60.30.60.30.30.
Carrier gas He HeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.40.60.60.
Tend (C) 250.280.250.250.280.
Heat rate (K/min) 4.3.4.4.2.
Initial hold (min) 8.5.8.2.10.
Final hold (min) 10. 10.20.40.
I 848.830.835.807.795.
ReferenceDuckham, Dodson, et al., 2002Fokialakis, Magiatis, et al., 2002Oruna-Concha, Ames, et al., 2002Pino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5BPX-5BPX-5BPX-5
Column length (m) 50.30.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 0.40.250.50.50.25
Tstart (C) 60.40.60.60.60.
Tend (C) 280.260.250.250.250.
Heat rate (K/min) 3.5.4.4.4.
Initial hold (min) 10.4.5.5.5.
Final hold (min) 60. 10.10.10.
I 795.830.838.838.848.
ReferencePino, Marbot, et al., 2002, 3Venskutonis, Vasiliauskaite, et al., 2002Ames, Guy, et al., 2001Ames, Guy, et al., 2001Ames, Guy, et al., 2001, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-SulfurBPX-5BPX-5BPX-5BPX-5
Column length (m) 30.50.50.50.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 4.0.250.250.250.25
Tstart (C) 40.35.35.35.35.
Tend (C) 200.250.250.250.250.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min) 12.53.3.3.3.
Final hold (min)  10.10.10.10.
I 800.4846.848.846.848.
Referencede Lacy Costello, Evans, et al., 2001Oruna-Concha, Duckham, et al., 2001Oruna-Concha, Duckham, et al., 2001Oruna-Concha, Duckham, et al., 2001Oruna-Concha, Duckham, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBSE-54SE-54CP Sil 8 CB
Column length (m) 50.50.25.25.60.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.320.320.310.310.25
Phase thickness (mum) 0.40.4  0.25
Tstart (C) 60.60.35.35.40.
Tend (C) 280.280.230.230.280.
Heat rate (K/min) 3.3.4.4.4.
Initial hold (min) 10.10.3.3.2.
Final hold (min) 60.60.10.10. 
I 795.795.833.84835.20837.
ReferencePino and Marbot, 2001Pino, Marbot, et al., 2001Yin, Xiu, et al., 2001Yin, Xiu, et al., 2001Elmore, Mottram, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5DB-1CP Sil 8 CBCP Sil 8 CBDB-5
Column length (m) 50.60.25.50.30.
Carrier gas HeN2  H2
Substrate      
Column diameter (mm) 0.320.250.20.320.25
Phase thickness (mum) 1.1.0.25 0.25
Tstart (C) 40.30.40.60.50.
Tend (C) 190.200.200.220.290.
Heat rate (K/min) 2.5.2.4.4.
Initial hold (min) 5. 8.5. 
Final hold (min)  30. 30. 
I 846.804.805.826.850.
ReferenceEscudero, Cacho, et al., 2000Wu, Wang, et al., 2000Yassaa, Meklati, et al., 2000Chevance and Farmer, 1999da Silva, Borba, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeSPB-1DB-5BP-1BPX-5
Column length (m) 50.60.30.25.50.
Carrier gas N2N2 HeHe
Substrate      
Column diameter (mm) 0.250.320.320.320.325
Phase thickness (mum) 0.170.251. 0.5
Tstart (C) 80.40.60.5.50.
Tend (C) 200.200.250.250.250.
Heat rate (K/min) 2.4.4.5.4.
Initial hold (min)   5.5.2.
Final hold (min)  20.20.30.10.
I 816.799.829.802.842.
ReferenceSumathykutty, Rao, et al., 1999Chen, Huang, et al., 1998Madruga and Mottram, 1998Sinyinda and Gramshaw, 1998Ames, Defaye, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SE-30OV-101HP-1HP-1
Column length (m) 60.50.50.50.50.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 0.250.250.51.051.5
Tstart (C) 50.50.50.40.40.
Tend (C) 200.250.200.260.220.
Heat rate (K/min) 8.8.4.2.2.
Initial hold (min)      
Final hold (min)    40.30.
I 800.804.806.815.803.
ReferenceMisharina, Beletsky, et al., 1994Misharina, Golovnya, et al., 1994Misharina, Golovnya, et al., 1993Oh, Shu, et al., 1992Zhang, Dorjpalam, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101HP-1DB-1DB-1
Column length (m) 50.50.50.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 1.050.501.050.250.25
Tstart (C) 40.50.40.40.40.
Tend (C) 260.250.260.220.220.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)      
Final hold (min) 40. 10.10.10.
I 802.810.808.804.802.
ReferenceIzzo and Ho, 1991Misharina, Aerove, et al., 1991Oh, Shu, et al., 1991Zhang and Ho, 1991Zhang and Ho, 1991, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-1OV-1
Column length (m) 50.183.
Carrier gas H2N2
Substrate   
Column diameter (mm) 0.2 
Phase thickness (mum)   
Tstart (C) 50.0.
Tend (C) 200.230.
Heat rate (K/min) 2.1.
Initial hold (min)   
Final hold (min) 55. 
I 799.804.
ReferenceWu and Liou, 1986Schreyen, Dirinck, et al., 1976
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Pino, Marbot, et al., 2001
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Escudero, Cacho, et al., 2000
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References