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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5VF-5 MSDB-5HP-5 MSVF-5 MS
Column length (m) 30.60.25.30.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.200.250.32
Phase thickness (mum) 0.250.250.330.250.25
Tstart (C) 60.40.50.50.30.
Tend (C) 246.250.240.180.260.
Heat rate (K/min) 3.4.20.2.2.
Initial hold (min) 1.2.1.  
Final hold (min)     28.
I 824.832.825.829.831.
ReferenceAl-Qudah, Muhaidat, et al., 2012Srisajjalerwaja, Apichartsrangkoon, et al., 2012Cais-Sokolinska, Majcher, et al., 2011Hammami, Kamoun, et al., 2011Leffingwell and Alford, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5 MSVF-5 MSHP-5OV-1HP-5 MS
Column length (m) 60.30.60.50.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (mum) 0.250.250.250.500.25
Tstart (C) 30.40.35.40.70.
Tend (C) 260.250.220.270.290.
Heat rate (K/min) 2.5.10.2.5.
Initial hold (min)  3.1.  
Final hold (min) 28.3.15.10. 
I 836.837.835.800.828.
ReferenceLeffingwell and Alford, 2011Liu, Lu, et al., 2011Piyachaiseth, Jirapakkul, et al., 2011Da Costa, Yang, et al., 2010Lazarevic, Radulovic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-5 MSHP-5HP-5 MSDB-5
Column length (m) 25.30.30.30.30.
Carrier gas HeliumHeliumHydrogenHeliumHelium
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (mum) 0.330.250.250.250.25
Tstart (C) 40.70.70.70.50.
Tend (C) 250.290.290.290.220.
Heat rate (K/min) 10.5.5.5.4.
Initial hold (min) 1.    
Final hold (min)  10. 10. 
I 842.828.834.829.826.
ReferenceMajcher, Lawrowski, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2Shedid, 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSZB-5HP-5 MSHP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.35.70.50.
Tend (C) 230.280.195.290.280.
Heat rate (K/min) 6.6.2.5.4.
Initial hold (min) 2.1.5.  
Final hold (min) 20.9.30.10. 
I 829.832.829.828.832.
ReferenceChen, Song, et al., 2009Harrison and Priest, 2009Kim and Chung, 2009Radulovic, Blagojevic, et al., 2009Zhao, Zeng, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101HP-1SLB-5MSDB-5RTX-5
Column length (m) 25.50.10.60.10.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.200.200.180.320.18
Phase thickness (mum) 0.250.330.181.00.2
Tstart (C) 70.60.40.35.40.
Tend (C) 200.250.295.240.275.
Heat rate (K/min) 3.2.10.15.50.
Initial hold (min) 2. 1.57.0.5
Final hold (min)  20. 10.0.5
I 839.802.845.829.845.
ReferenceBlazevic and Mastelic, 2008Breme, Langle, et al., 2008Risticevic, Carasek, et al., 2008Gogus, Ozel, et al., 2007Setkova, Risticevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-5MSHP-1HP-1DB-5DB-5
Column length (m) 30.50.50.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.20.20.320.32
Phase thickness (mum) 0.50.50.33  
Tstart (C) 40.60.60.60.50.
Tend (C) 280.250.250.250.250.
Heat rate (K/min) 4.2.2.4.4.
Initial hold (min) 5. 4.5.5.
Final hold (min) 10.120.30.  
I 829.800.800.850.850.
ReferenceTava, Pecetti, et al., 2007Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Fadel, Mageed, et al., 2006Fadel, Mageed, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSHP-101HP-5
Column length (m) 30.30.30.25.30.
Carrier gas HeN2HeHeHelium
Substrate      
Column diameter (mm) 0.320.320.250.20.32
Phase thickness (mum) 1.1.0.250.20.25
Tstart (C) 40.40.50.70.40.
Tend (C) 250.230.280.200.240.
Heat rate (K/min) 4.6.5.3.4.
Initial hold (min) 2.2.4.2. 
Final hold (min) 15.15.10.15.5.
I 831.829.829.830.860.
ReferenceFan and Qian, 2006Fan and Qian, 2006, 2Kim, Abd El-Aty, et al., 2006Mastelic, Jerkovic, et al., 2006Miyazawa and Kawata, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5 MSDB-5HP-5 MSHP-1
Column length (m) 30.30.30.30.50.
Carrier gas Helium HeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.5
Tstart (C) 60.40.40.60.60.
Tend (C) 250.200.250.250.250.
Heat rate (K/min) 4.8.4.2.2.
Initial hold (min) 2.3.2.8. 
Final hold (min) 20.20.10.15.40.
I 830.821.833.831.808.
ReferencePino, Marquez, et al., 2006Schirack, Drake, et al., 2006Shen X., Gao Y., et al., 2006Tigrine-Kordiani, Meklati, et al., 2006Valette, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MDN-5SPB-5HP-5OV-101
Column length (m) 60.60.30.30.25.
Carrier gas HeHeHeHeliumN2/He
Substrate      
Column diameter (mm) 0.320.250.250.320.20
Phase thickness (mum) 0.250.250.250.250.10
Tstart (C) 30.40.60.40.50.
Tend (C) 260.270.250.250.250.
Heat rate (K/min) 2.4.4.5.6.
Initial hold (min) 2.4.2.2. 
Final hold (min) 28.5.20.5. 
I 838.2832.807.830.810.
ReferenceLeffingwell and Alford, 2005van Loon, Linssen, et al., 2005Pino, Marbot, et al., 2005N/AZenkevich, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-1DB-1
Column length (m) 30.50.60.60.60.
Carrier gas HeliumHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (mum)   0.250.250.25
Tstart (C) 60.60.35.35.35.
Tend (C) 240.240.230.230.230.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)   4.4.4.
Final hold (min) 999.999.25.25.25.
I 830.830.794.797.798.
ReferenceMiyazawa, Fuhita, et al., 2004Miyazawa, Fujita, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5CP Sil 8 CBDB-5SPB-5
Column length (m) 60.30.30.60.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.250.320.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.60.50.35.40.
Tend (C) 230.240.200.280.220.
Heat rate (K/min) 2.3.5.5.5.
Initial hold (min) 4. 5.2.1.
Final hold (min) 25.  4.20.
I 800.830.835.831.837.
ReferencePark, Lee, et al., 2004Tellez, Khan, et al., 2004Wang, Guo, et al., 2004Dhanda, Pegg, et al., 2003Ledauphin, Guichard, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1HP-5HP-5RSL-200
Column length (m) 30.50.25.30.30.
Carrier gas H2HeH2 H2
Substrate      
Column diameter (mm) 0.250.20.320.250.25
Phase thickness (mum) 0.250.50.53 0.25
Tstart (C) 60.60.40.50.40.
Tend (C) 280.220.280.200.280.
Heat rate (K/min) 4.2.4.3.6.
Initial hold (min) 10.   2.
Final hold (min) 40.40.  10.
I 829.796.836.832.837.
ReferencePino, Marbot, et al., 2003Valette, Fernandez, et al., 2003Velickovic, Randjelovic, et al., 2003Isidorov and Jdanova, 2002Jirovetz, Smith, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-5DB-5SPB-5OV-101
Column length (m) 30.30.30.60.50.
Carrier gas HeHeliumHeHeNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.251. 
Tstart (C) 60.60.60.40.40.
Tend (C) 240.250.240.200.200.
Heat rate (K/min) 3.4.3.3.2.
Initial hold (min)  2.  10.
Final hold (min)  20.   
I 831.829.830.833.809.
ReferenceKobaisy, Tellez, et al., 2002Pino, Marbot, et al., 2002Tellez, Khan, et al., 2002Poligné, Collignan, et al., 2001Tamura, Boonbumrung, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeDB-1BP-5DB-5DB-1
Column length (m) 60.60.50.30.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.32
Phase thickness (mum) 0.251.1.0.251.0
Tstart (C) 40.40.40.60.40.
Tend (C) 220.260.190.240.260.
Heat rate (K/min) 5.2.2.3.2.
Initial hold (min) 10. 5.  
Final hold (min)      
I 801.05817.853.833.820.
ReferenceBaraldi, Rapparini, et al., 1999Chen and Ho, 1999Lopez, Ferreira, et al., 1999Tellez, Canel, et al., 1999Chen and Ho, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-1DB-1DB-1
Column length (m) 60.60.25.60.60.
Carrier gas HeHe He 
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (mum) 1.01. 1.0 
Tstart (C) 40.40.35.40.30.
Tend (C) 260.260.250.280.200.
Heat rate (K/min) 3.3.4.2.4.
Initial hold (min)     25.
Final hold (min)     20.
I 808.808.798.803.800.
ReferenceChen and Ho, 1998, 2Chen, Wang, et al., 1998Ong, Acree, et al., 1998Tai and Ho, 1998Buttery, Ling, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5DB-1DB-1DB-1DB-1
Column length (m) 50.60.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.320.250.250.32
Phase thickness (mum) 0.251. 1. 
Tstart (C) 50.40.30.40.30.
Tend (C) 250.280.200.260.200.
Heat rate (K/min) 3.2.4.2.4.
Initial hold (min) 1.2.25.5.25.
Final hold (min) 10.40.20.60.20.
I 848.783.800.829.800.
ReferenceD'Arcy, Rintoul, et al., 1997Lu, Yu, et al., 1997Buttery and Ling, 1995Yu and Ho, 1995Buttery, Stern, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-101DB-1DB-1
Column length (m) 60.60.50.30.30.
Carrier gas  He HeHe
Substrate      
Column diameter (mm) 0.320.250.220.250.25
Phase thickness (mum) 0.501.0 0.250.25
Tstart (C) 50.40.80.50.50.
Tend (C) 225.260.200.240.240.
Heat rate (K/min) 2.2.2.3.3.
Initial hold (min)  5. 5.5.
Final hold (min)  60.   
I 810.804.815.800.805.
ReferenceSagrero-Nieves, Bartley, et al., 1994Yu, Wu, et al., 1994Egolf and Jurs, 1993Shiota, 1993Shiota, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HG-5DB-5DB-1
Column length (m) 30.30.50.60.60.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.520.25 
Tstart (C) 50.50.35.40.30.
Tend (C) 240.240.250.250.200.
Heat rate (K/min) 5.5.3.2.4.
Initial hold (min) 3.3.15.5.25.
Final hold (min)   45. 5.
I 801.805.843.836.800.
ReferenceShiota, 1993Shiota, 1993Drumm and Spanier, 1991Lee, Macku, et al., 1991Buttery, Teranishi, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-1DB-1SE-54
Column length (m) 50.50.60.60.25.
Carrier gas H2H2  N2
Substrate      
Column diameter (mm) 0.30.30.320.320.25
Phase thickness (mum)   0.250.25 
Tstart (C) 80.80.50.50.60.
Tend (C) 250.250.250.250.260.
Heat rate (K/min) 16.16.4.4.6.
Initial hold (min)     2.
Final hold (min)      
I 815.841.799.804.828.
ReferenceSpadone, Takeoka, et al., 1990Spadone, Takeoka, et al., 1990Flath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989Bestmann, Classen, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5OV-1DB-1OV-101
Column length (m) 60.30.50.50.50.
Carrier gas HeHydrogenHydrogen He
Substrate      
Column diameter (mm) 0.3150.350.200.320.31
Phase thickness (mum) 0.251.0   
Tstart (C) 50.45.50.0.0.
Tend (C) 250.220.200.250.225.
Heat rate (K/min) 4.2.1.3.3.
Initial hold (min)     1.
Final hold (min)   35.  
I 800.848.814.799.810.
ReferenceEngel, Flath, et al., 1988Georgilopoulos and Gallois, 1988Wu, Liou, et al., 1987Habu, Flath, et al., 1985del Rosario, de Lumen, et al., 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SE-30SE-30OV-1
Column length (m) 50.50.183.
Carrier gas  HeN2
Substrate    
Column diameter (mm) 0.50.50.762
Phase thickness (mum)    
Tstart (C) 40.40.0.
Tend (C) 170.170.230.
Heat rate (K/min) 3.3.1.
Initial hold (min) 3.3. 
Final hold (min)    
I 813.814.801.
ReferenceHeydanek and McGorrin, 1981Heydanek and McGorrin, 1981, 2Schreyen, Dirinck, et al., 1979
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Al-Qudah, Muhaidat, et al., 2012
Al-Qudah, M.A.; Muhaidat, R.; Trawenh, I.N.; Jaber, H.I.; Abu Zarga, M.H.; Abu Orabi, S.T., Volatile constituents of leaves and bulbs of Gynandriris Sisyrinchicum and their antimicrobial activities, Jordan J. Chem., 2012, 7, 3, 287-295. [all data]

Srisajjalerwaja, Apichartsrangkoon, et al., 2012
Srisajjalerwaja, S.; Apichartsrangkoon, A.; Chaikham, P.; Chakrabandhu, Y.; Pathomrungsiyounggul, P.; Leksawasdi, N.; Supraditareporn, W.; Hirun, S., Color, capsaicin and volatile components of baked thai green chili (Capsicum anmuum Linn. var. Jak Ka Pat), J. Agricultural Sci., 2012, 4, 12, 75-84. [all data]

Cais-Sokolinska, Majcher, et al., 2011
Cais-Sokolinska, D.; Majcher, M.; Pikul, J.; Bielinska, S.; Czauderma, M.; Wojtowski, J., The effect of Camelia sativa cake diet supplementation on sensory and volatile profiles of ewe's milk, African J. Biotechnol., 2011, 10, 37, 7245-7252. [all data]

Hammami, Kamoun, et al., 2011
Hammami, I.; Kamoun, N.; Rebai, A., Biocontrol of Botrytis cinerea with essential oil and methanol extract of Viola odorata flowers, Archives of Appl. Sci. Res., 2011, 3, 5, 44-51. [all data]

Leffingwell and Alford, 2011
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Liu, Lu, et al., 2011
Liu, S.; Lu, S.; Su, Y.; Guo, Y., Analysis of volatile compounds in Radix Bupleuri injection by GC-MS-MS, Chromatographia, 2011, 74, 5-6, 497-502, https://doi.org/10.1007/s10337-011-2082-7 . [all data]

Piyachaiseth, Jirapakkul, et al., 2011
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Da Costa, Yang, et al., 2010
Da Costa, N.C.; Yang, Y.; Kowalczyk, J.; Poulsen, M.L., The analysis of volatiles and non-volatiles in Yerba Mate tea (Ilex paraguariensis) in Proc. 12th Weurman Symp., Blank, I.; Wust, M.; Yeretzian, C., ed(s)., Institut fur Chemie und Biologisher Chemie, Wissenschafen, Winterthur, 2010, 494-497. [all data]

Lazarevic, Radulovic, et al., 2010
Lazarevic, J.; Radulovic, N.; Palic, R.; Zlatkovic, B., Chemical Analusis of volatile constituents of Berula erecta (Hudson) Coville subsp. erecta (Apiaceae) from Serbia, J. Essential Oil. Res., 2010, 22, 3, 153-156, https://doi.org/10.1080/10412905.2010.9700290 . [all data]

Majcher, Lawrowski, et al., 2010
Majcher, M.; Lawrowski, P.; Jelen, H., Comparison of original and adulterated oscypek cheese based on volatile and sensory profiles, Acta Sci. Pol. Technol. Aliment., 2010, 9, 3, 265-275. [all data]

Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

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Radulovic, N.S.; Dordevic, N.D.; Palic, R.M., Volatiles of Pleurospermum austriacum (L.) Hoffm. (Apiaceae), J. Serbian Chem. Soc., 2010, 75, 12, 1-11, https://doi.org/10.2298/JSC100323127R . [all data]

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Radulovic, N.; Dordevic, N.; Markovic, M.; Palic, R., Volatile constituents of Glechoma Hirsuta Waldst. Kit. and G. Hederacea L. (Lamiaceae), Bull. Chem. Soc. Ethiop., 2010, 24, 1, 67-76, https://doi.org/10.4314/bcse.v24i1.52962 . [all data]

Shedid, 2010
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Chen, Song, et al., 2009
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Harrison and Priest, 2009
Harrison, B.M.; Priest, F.G., Composition of peaks used in the preparation of malt for Scotch Whisky production - influence of geographical source and extraction depth, J. Agric. Food Chem., 2009, 57, 6, 2385-2391, https://doi.org/10.1021/jf803556y . [all data]

Kim and Chung, 2009
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Radulovic, Blagojevic, et al., 2009
Radulovic, N.S.; Blagojevic, P.D.; Palic, R.M.; Zlatkovic, B.K.; Stevanovic, B.M., Volatiles from vegetative organs of the paleoendemic resurrection plants Ramonda serbica Panc. and Ramonda nathaliae Panc. at Petrov, J. Serb. Chem. Soc., 2009, 74, 1, 35-44, https://doi.org/10.2298/JSC0901035R . [all data]

Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

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Breme, Langle, et al., 2008
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References