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Eugenol

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSHP-5 MSHP-5 MSOptima-5DB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 60.60.40.60.40.
Tend (C) 240.230.250.246.250.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)   1.1.5.
Final hold (min)   20. 20.
I 1365.1366.1332.1350.1352.
ReferencePinheiro, de Queiros, et al., 2013Pripdeevech and Saansoomchai, 2013Sardashti, Valizadeh, et al., 2013Al-Qudah, Muhaidat, et al., 2012Cao, Li, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5 MSVF-5 MSDB-1ZB-5DB-5 MS
Column length (m) 60.60.50.30.25.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.320.320.320.250.30
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 30.30.60.40.50.
Tend (C) 260.260.250.200.240.
Heat rate (K/min) 2.2.8.5.3.
Initial hold (min)    5. 
Final hold (min) 28.28. 5. 
I 1355.1357.1330.1336.1353.
ReferenceLeffingwell and Alford, 2011Leffingwell and Alford, 2011Misharina T., 2011Vazquez, Demmel, et al., 2011Chalchat, Figueredo, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSOV-1HP-5 MSDB-5 MSBP-1
Column length (m) 25.30.30.60. 
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.300.250.250.25 
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 50.50.70.40.60.
Tend (C) 240.250.290.250.220.
Heat rate (K/min) 3.5.5.5.5.
Initial hold (min)  3. 15.10.
Final hold (min)  2. 15.30.
I 1353.1358.1362.1353.1333.
ReferenceChalchat, Figueredo, et al., 2010Hu, Liang, et al., 2010Lazarevic, Radulovic, et al., 2010Mesa-Arango, Betancur-Galvis, et al., 2010Mishra, Chaudhary, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-5 MSHP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.50.100.70.
Tend (C) 240.220.240.220.290.
Heat rate (K/min) 3.5.4.2.5.
Initial hold (min) 5.10.2.  
Final hold (min)   10. 10.
I 1361.1358.1356.1355.1361.
ReferenceMonsef-Esfahani, Miri, et al., 2010Ogunwande, Flamini, et al., 2010Pino, Marquez, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Radulovic, Blagojevic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5DB-1-MSCP Sil 5 CBDB-5
Column length (m) 30.30.60.25.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.150.25
Tstart (C) 70.60.30.50.80.
Tend (C) 290.240.200.230.240.
Heat rate (K/min) 5.3.2.3.3.
Initial hold (min)   4.  
Final hold (min) 10. 35. 2.
I 1353.1359.1323.1354.1356.
ReferenceRadulovic, Dordevic, et al., 2010Scherer, Wagner, et al., 2010Takeoka, Hobbs, et al., 2010Usman, Zubair, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5VF-5MSZB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.40.40.50.
Tend (C) 220.240.220.280.250.
Heat rate (K/min) 4.3.2.6.5.
Initial hold (min) 2. 1.1.2.
Final hold (min) 2. 30.9. 
I 1326.1359.1386.1365.1359.
ReferenceXu, Tang, et al., 2010Alim, Goze, et al., 2009Fernandes, de Pinho, et al., 2009Harrison and Priest, 2009Ho, Wang, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1RTX-1BP-15 % Phenyl methyl siloxane
Column length (m) 25.60.60.50.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.200.220.220.220.25
Phase thickness (mum) 0.330.250.250.250.25
Tstart (C) 60.60.60.60.90.
Tend (C) 240.230.230.220.225.
Heat rate (K/min) 3.2.2.2.3.
Initial hold (min)      
Final hold (min) 7.30.30.20.3.
I 1358.1329.1331.1341.1358.
ReferenceMaridass, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Ottavioli, Bighelli, et al., 2009Retta, Gattuso, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1 MSHP-5MSHP-5 MSBPX-5BPX-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.50.50.100.60.
Tend (C) 250.240.280.999.999.
Heat rate (K/min) 6.5.4.3.3.
Initial hold (min) 1.    
Final hold (min) 4.    
I 1334.1356.1359.1370.1367.
ReferenceSeo, Kim, et al., 2009Wannes, Mhamdi, et al., 2009Zhao, Zeng, et al., 2009Bieri and Marriott, 2008Bieri and Marriott, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5BPX-5BPX-5BPX-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHydrogenHydrogenHydrogenNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 999.999.999.999.280.
Heat rate (K/min) 3.3.3.5.5.
Initial hold (min)     1.
Final hold (min)     1.
I 1367.1368.1374.1371.1367.
ReferenceBieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008Bousaada, Ammar, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra 2DB-5MSDB-5ZB-1Equity-5 MS
Column length (m) 50.30.25.30.30.
Carrier gas HeliumHeNitrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.200.250.220.250.25
Phase thickness (mum) 0.110.250.250.250.25
Tstart (C) 60.50.50.45.40.
Tend (C) 230.250.300.230.260.
Heat rate (K/min) 2.2.6.53.1.5
Initial hold (min) 5.5.2.  
Final hold (min) 30. 7.  
I 1357.1360.1366.1327.1357.
ReferenceByun and Shin, 2008Cheng, Liu, et al., 2008Chieng, Assim, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Mondello, Casilli, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1SLB-5MSHP-5HP-5 MSHP-5
Column length (m) 60.10.30.30.25.
Carrier gas HeHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.220.180.250.250.25
Phase thickness (mum) 0.250.180.250.250.25
Tstart (C) 60.40.50.50.60.
Tend (C) 230.295.280.240.240.
Heat rate (K/min) 2.10.5.3.4.
Initial hold (min)  1.51. 2.
Final hold (min) 35. 1.  
I 1332.1374.1364.1384.1356.
ReferencePaolini, Tomi, et al., 2008Risticevic, Carasek, et al., 2008Saidana, Mahjoub, et al., 2008Sarikurkcu, Tepe, et al., 2008Verdian-rizi, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSSE-54DB-5MSHP-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.70.35.
Tend (C) 230.260.240.200.220.
Heat rate (K/min) 3.2.3.10.3.
Initial hold (min) 10.5.   
Final hold (min) 10.20.  40.
I 1356.1361.1359.1351.1361.
ReferenceAdams, Beauchamp, et al., 2007Alma, Ertas, et al., 2007Da Silva J.K.R., Sousa P.J.C., et al., 2007Dongmo, Tatsadjieu, et al., 2007El-Ghorab A., El-Massry K.F., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DBP-5HP-101DB-5DB-5MS
Column length (m) 30.25.25.30.30.
Carrier gas HeliumHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.260.220.20.250.25
Tstart (C) 60.40.70.60.60.
Tend (C) 240.250.200.300.280.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 2.1.2.  
Final hold (min) 20.10.  30.
I 1360.1322.1364.1360.1330.
ReferenceFarsam, Amanlou, et al., 2007Heravi and Sereshti, 2007Jerkovic, Mastelic, et al., 2007Limberger, Scopel, et al., 2007Marongiu B., Piras A., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5Sil MSZB-5HP-5HP-5 MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas He HeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.40.60.50.
Tend (C) 260.220.260.220.240.
Heat rate (K/min) 5.4.4.5.4.
Initial hold (min) 2.5. 3. 
Final hold (min) 10.20. 3. 
I 1356.1361.1355.1330.1356.
ReferenceMatasyoh, Matasyoh, et al., 2007Mohottalage, Tabacchi, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Safaei-Ghomi, Bamoniri, et al., 2007Sefidkon, Abbasi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DBP-5Elite-5MSHP-5 MSDB-5HP-5
Column length (m) 25.30.30.30.60.
Carrier gas HeliumHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (mum) 0.220.50.250.250.25
Tstart (C) 40.40.60.40.60.
Tend (C) 250.280.280.250.250.
Heat rate (K/min) 3.4.3.4.3.
Initial hold (min) 1.5. 2. 
Final hold (min) 10.10. 5. 
I 1322.1352.1359.1373.1361.
ReferenceSereshti and Samadi, 2007Tava, Pecetti, et al., 2007Vagionas, Graikou, et al., 2007Xu, Fan, et al., 2007Bertrand, Comte, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1HP-1DB-5
Column length (m) 50.50.50.50.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.20.20.20.20.25
Phase thickness (mum) 0.330.330.50.330.25
Tstart (C) 60.60.60.60.70.
Tend (C) 250.250.250.250.230.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min) 4.4. 4.2.
Final hold (min) 30.30.120.30.20.
I 1326.1321.1326.1326.1351.
ReferenceCastel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006, 2Castel, Fernandez, et al., 2006, 2Choi, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-1DB-5DB-5HP-5
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.20.250.250.32
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 300.250.240.240.260.
Heat rate (K/min) 5.2.5.5.5.
Initial hold (min) 5. 2.2.2.
Final hold (min) 5.40.  13.
I 1358.1326.1354.1354.1359.
ReferenceFiguérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006Gohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Kucuk, Gulec, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1CP Sil 5 CBHP-101HP-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeN2HeHeliumHe
Substrate      
Column diameter (mm) 0.320.250.20.320.25
Phase thickness (mum) 0.250.250.20.250.25
Tstart (C) 60.50.70.40.60.
Tend (C) 300.200.200.240.220.
Heat rate (K/min) 4.5.3.4.4.
Initial hold (min)   2.  
Final hold (min)   15.5. 
I 1328.1332.1373.1351.1360.
ReferenceKula, Izydorczyk, et al., 2006Martin, Joseph, et al., 2006Mastelic, Jerkovic, et al., 2006Miyazawa and Kawata, 2006Morteza-Semnani, Akbarzadeh, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5SPB-5DB-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas N2HeHeliumHydrogenHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 50.60.60.70.60.
Tend (C) 200.280.250.280.200.
Heat rate (K/min) 4.5.4.4.2.
Initial hold (min) 3.0.52.4. 
Final hold (min)  2.20. 60.
I 1360.1364.1355.1356.1362.
ReferenceOuamba, Ouabonzi, et al., 2006Ozel, Gogus, et al., 2006Pino, Marquez, et al., 2006Pino, Marbot, et al., 2006Rout, Naik, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase FSOT-RSL-200DB-5DB-5DB-1HP-5
Column length (m) 30.30.13.530.30.
Carrier gas HydrogenHeHe He
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 40.40.35.60.60.
Tend (C) 280.260.225.230.250.
Heat rate (K/min) 6.2.6.3.10.
Initial hold (min) 5.5.3.3.2.
Final hold (min) 5.20. 10.10.
I 1357.1355.1368.1351.1371.
ReferenceSchmidt, Jirovetz, et al., 2006Senatore, Landolfi, et al., 2006de Souza, Vásquez, et al., 2006Tohar, Mohd, et al., 2006Wang, Yang, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5HP-5RSL-200
Column length (m) 50.25.25.30.30.
Carrier gas   HeHe 
Substrate      
Column diameter (mm) 0.30.250.20.250.25
Phase thickness (mum) 0.250.150.330.250.25
Tstart (C) 60.40.60.50.40.
Tend (C) 240.220.240.300.280.
Heat rate (K/min) 2.3.3.5.6.
Initial hold (min)  5. 5.2.
Final hold (min)   7.5.10.
I 1355.1352.1355.1358.1358.
ReferenceChagonda and Chalchat, 2005Chagonda and Chalchat, 2005, 2Duarte, Figueira, et al., 2005Figuérédo, Cabassu, et al., 2005Jirovetz, Buchbauer, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5SPB-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.530.250.25
Phase thickness (mum) 0.25  0.250.25
Tstart (C) 50.60.100.60.70.
Tend (C) 265.240.250.220.240.
Heat rate (K/min) 2.53.5.4.5.
Initial hold (min) 1.  5. 
Final hold (min) 20.    
I 1351.1360.1380.1359.1361.
ReferenceKhanavi, Ghasemian, et al., 2005Khayyat and Karimi, 2005Kilic, Kollmannsberger, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005Oyedeji, Yani, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5DB-5HP-5MSRTX-1
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 250.240.260.280.25.
Heat rate (K/min) 4.5.2.3.5.
Initial hold (min) 2. 5.  
Final hold (min) 20. 20. 10.
I 1356.1356.1355.1362.1332.
ReferencePino, Marbot, et al., 2005Saeidnia, Gohari, et al., 2005Senatore, Apostolides Arnold, et al., 2005Slavkovska, Couladis, et al., 2005Sonboli, Salehi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 8 CBHP-5MSHP-5SPB-1
Column length (m) 30.30.30.30.50.
Carrier gas N2HeHeHeliumHe
Substrate      
Column diameter (mm) 0.320.250.250.320.2
Phase thickness (mum) 0.25 0.250.250.33
Tstart (C) 60.60.60.40.50.
Tend (C) 220.290.285.300.220.
Heat rate (K/min) 5.3.4.34.4.
Initial hold (min)  5.  3.
Final hold (min) 15.  5.30.
I 1340.1353.1356.1344.1333.
ReferenceSrivastava, Srivastava, et al., 2005Suárez, Vásquez, et al., 2005Tesevic, Nikicevic, et al., 2005Utsunomia, Kawata, et al., 2005Wong, Lee, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-1DB-5SE-54SE-54
Column length (m) 50.25.25.30.30.
Carrier gas He NitrogenHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.053
Phase thickness (mum) 0.330.250.250.251.5
Tstart (C) 50.60.60.60.100.
Tend (C) 220.180.240.260.250.
Heat rate (K/min) 4.3.3.2.5.
Initial hold (min) 3.10. 5. 
Final hold (min) 30.10.   
I 1333.1357.1357.1354.1378.
ReferenceWong and Tan, 2005bin Jantan, Ayop, et al., 2004JAvidnia, Mojab, et al., 2004Kilic, Hafizoglu, et al., 2004Kilic, Hafizoglu, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSBP-1DB-5MSDB-5DB-5
Column length (m) 30.25.30.30.50.
Carrier gas HeN2HeHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.25  
Tstart (C) 60.60.60.60.60.
Tend (C) 240.220.280.240.240.
Heat rate (K/min) 3.5.3.2.2.
Initial hold (min)      
Final hold (min)   30.999.999.
I 1357.1330.1329.1353.1353.
Referencepaz Lima, Silva, et al., 2004Mallavarapu, Kulkarni, et al., 2004Marongiu, Porcedda, et al., 2004Miyazawa, Fuhita, et al., 2004Miyazawa, Fujita, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30NB-30DB-1DB-1DB-1
Column length (m) 50.50.50.60.60.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.20.20.250.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.95.35.35.
Tend (C) 250.250.240.230.230.
Heat rate (K/min) 2.2.4.2.2.
Initial hold (min)    4.4.
Final hold (min)    25.25.
I 1336.1336.1345.1322.1323.
ReferenceOrav, Stulova, et al., 2004Orav, Stulova, et al., 2004Palá-Paúl, Velasco-Negueruela, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5MSDB-5HP-5
Column length (m) 60.60.30.30.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.320.320.250.250.2
Phase thickness (mum) 0.250.250.250.250.5
Tstart (C) 35.35.60.40.30.
Tend (C) 230.230.280.250.280.
Heat rate (K/min) 2.2.4.2.3.
Initial hold (min) 4.4. 5. 
Final hold (min) 25.25. 20. 
I 1324.1327.1353.1353.1367.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Sadeghpour, Asghari, et al., 2004Senatore, Rigano, et al., 2004Shafi, Nambiar, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5CP Sil 8 CBHP-5MSRTX-5Sil
Column length (m) 25.30.30.30.30.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (mum) 0.520.250.250.250.25
Tstart (C) 40.60.50.60.70.
Tend (C) 240.240.200.275.200.
Heat rate (K/min) 4.3.5.4.4.
Initial hold (min)   5.  
Final hold (min)     10.
I 1356.1353.1359.1356.1357.
ReferenceSimic, Sokovic, et al., 2004Tellez, Khan, et al., 2004Wang, Guo, et al., 2004Afsharypuor and Jahromy, 2003Dudai, Larkov, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSHP-1RSL-200
Column length (m) 60.60.30.50.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.320.320.250.20.32
Phase thickness (mum)   0.250.50.25
Tstart (C) 50.50.60.60.40.
Tend (C) 220.200.220.220.280.
Heat rate (K/min) 3.3.5.2.6.
Initial hold (min)   20. 5.
Final hold (min)   20.45.5.
I 1375.1362.1360.1331.1336.
ReferenceEdris and Farrag, 2003Edris, Shalaby, et al., 2003Feizbaksh, Saber Tehrani, et al., 2003Fernandez, Lizzani-Cuvelier, et al., 2003Jirovetz, Buchbauer, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200DB-5SPB-5DB-1
Column length (m) 30.30.50.30.30.
Carrier gas H2H2HeHeN2
Substrate      
Column diameter (mm) 0.250.320.20.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.50.40.80.
Tend (C) 280.280.220.220.250.
Heat rate (K/min) 6.6.3.5.4.
Initial hold (min) 2.5.2.1. 
Final hold (min) 10.5.10.20. 
I 1358.1335.1356.1359.1324.
ReferenceJirovetz, Buchbauer, et al., 2003, 2Jirovetz, Buchbauer, et al., 2003, 3Juteau, Jerkovic, et al., 2003Ledauphin, Guichard, et al., 2003Mahalwal and Ali, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBZB-1DB-1HP-5
Column length (m) 50.25.30.50.30.
Carrier gas He N2N2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.250.390.250.250.25
Tstart (C) 50.60.45.95.60.
Tend (C) 220.220.230.240.280.
Heat rate (K/min) 3.5.3.4.3.
Initial hold (min) 2.    
Final hold (min)      
I 1360.1333.1327.1340.1342.
ReferenceMasotti, Juteau, et al., 2003Mazloomifar, Saber-Tehrani, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pitarokili, Tzakou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-1HP-5HP-5DB-5
Column length (m) 30.50.25.25.30.
Carrier gas HeHeH2H2He
Substrate      
Column diameter (mm) 0.250.20.320.320.25
Phase thickness (mum) 0.250.50.530.530.25
Tstart (C) 60.60.40.40.60.
Tend (C) 240.220.280.280.280.
Heat rate (K/min) 3.2.4.4.3.
Initial hold (min)      
Final hold (min)  40.  30.
I 1355.1319.1356.1359.1350.
ReferenceTaveira, de Lima, et al., 2003Valette, Fernandez, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003Caredda, Marongiu, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RSL-200RSL-200DB-5DB-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeH2H2HeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.50.60.60.
Tend (C) 200.280.280.240.240.
Heat rate (K/min) 3.6.6.3.3.
Initial hold (min) 6.5.5.  
Final hold (min)  5.5.  
I 1350.1348.1351.1355.1354.
ReferenceCimanga, Apers, et al., 2002Jirovetz, Buchbauer, et al., 2002Jirovetz, Ngassoum, et al., 2002Kobaisy, Tellez, et al., 2002Maia, Zoghbi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-1RTX-1SPB-1CBP-1PTE-5
Column length (m) 25.30.30.25.60.
Carrier gas HeN2N2NitrogenH2
Substrate      
Column diameter (mm) 0.200.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.3
Tstart (C) 50.60.70.50.60.
Tend (C) 250.300.180.210.285.
Heat rate (K/min) 3.4.2.3.4.3
Initial hold (min) 3. 2.2. 
Final hold (min)   1.  
I 1337.1337.1394.1328.1356.
ReferenceBrun, Bessière, et al., 2001Kalemba, Marschall, et al., 2001Kamath, Asha, et al., 2001Ly, Yamauchi, et al., 2001Stojanovic, Palic, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5DB-5Methyl SiliconeSE-30
Column length (m) 60.30.30.50.25.
Carrier gas HeH2HeH2He
Substrate      
Column diameter (mm) 0.250.320.250.250.2
Phase thickness (mum) 0.250.50.250.5 
Tstart (C) 70.60.60.40.60.
Tend (C) 240.245.240.260.230.
Heat rate (K/min) 5.3.3.4.3.
Initial hold (min) 8.3. 0.5 
Final hold (min) 20.20.   
I 1369.1355.1355.1327.1329.
ReferenceKim, Kim, et al., 2000Kotseridis and Baumes, 2000Maia, Zoghbi, et al., 2000Vendramini and Trugo, 2000Ali N.A.M. and Jantan, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1RTX-1BP-5SE-30OV-1
Column length (m) 50.30.50.25.25.
Carrier gas  N2HeHeH2
Substrate      
Column diameter (mm) 0.20.250.320.20.25
Phase thickness (mum) 0.330.251. 0.25
Tstart (C) 60.60.40.60.40.
Tend (C) 260.300.190.230.220.
Heat rate (K/min) 4.4.2.3.3.
Initial hold (min)   5.10.5.
Final hold (min)     5.
I 1329.1336.1369.1329.1320.
ReferenceChoo, Wong, et al., 1999Kalemba, 1999Lopez, Ferreira, et al., 1999Mohd and Jantan, 1999Oberhofer, Nikiforov, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PONADB-5CP Sil 5 CBBP-5Optima 1
Column length (m) 50.30.25.50.25.
Carrier gas HeHeN2HeHelium
Substrate      
Column diameter (mm) 0.20.25 0.320.20
Phase thickness (mum) 0.50.250.391.0.25
Tstart (C) 40.60.60.40.50.
Tend (C) 250.240.220.190.200.
Heat rate (K/min) 6.3.5.2.3.
Initial hold (min) 5.  5. 
Final hold (min)      
I 1340.1356.1336.1369.1355.
ReferenceRamalho, de Freitas, et al., 1999Tellez, Canel, et al., 1999Weyerstahl, Marschall, et al., 1999Ferreira, Ardanuy, et al., 1998Fons, Rapior, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-1CBP-1HP-101OV-101
Column length (m) 25.30.30.25.25.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.20.250.250.20.32
Phase thickness (mum)  0.25 0.2 
Tstart (C) 60.50.60.70.50.
Tend (C) 180.200.240.200.200.
Heat rate (K/min) 3.5.4.3.5.
Initial hold (min) 10.  2. 
Final hold (min)    10. 
I 1334.1321.1358.1371.1338.
ReferenceJantan, Ahmad, et al., 1998Kjällstrand, Ramnäs, et al., 1998Lamarque, Maestri, et al., 1998Milso, Mastelic, et al., 1998Zollo, Biyiti, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-1OV-101DB-1DB-1
Column length (m) 60.25.50.30.30.
Carrier gas HeHelium HeHe
Substrate      
Column diameter (mm) 0.320.320.220.250.25
Phase thickness (mum) 0.500.25 0.250.25
Tstart (C) 50.60.80.50.50.
Tend (C) 250.220.200.240.240.
Heat rate (K/min) 8.4.2.3.3.
Initial hold (min) 1.2. 5.5.
Final hold (min) 6.20.   
I 1399.1327.1351.1333.1338.
ReferenceSagrero-Nieves and Bartley, 1996Thanh, Dung, et al., 1996Egolf and Jurs, 1993Shiota, 1993Shiota, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-101OV-101DB-1
Column length (m) 30.30.50.50.60.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25   
Tstart (C) 50.50.80.80.30.
Tend (C) 240.240.200.200.200.
Heat rate (K/min) 5.5.2.2.4.
Initial hold (min) 3.3.  25.
Final hold (min)     5.
I 1338.1343.1330.1333.1326.
ReferenceShiota, 1993Shiota, 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993Buttery, Teranishi, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBOV-101OV-101HP-1HP-1
Column length (m) 25.50.50.12.12.
Carrier gas  N2N2  
Substrate      
Column diameter (mm) 0.200.250.250.20.2
Phase thickness (mum)    0.330.33
Tstart (C) 60.80.80.40.40.
Tend (C) 230.200.200.  
Heat rate (K/min) 3.2.2.16.4.
Initial hold (min) 10.  0.3950.4
Final hold (min)      
I 1358.1330.1330.1327.01319.7
ReferenceJantan and Goh, 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Yin and Sun, 1990Yin and Sun, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1OV-101DB5-30W
Column length (m) 12.25.50.50.30.
Carrier gas    N2He
Substrate      
Column diameter (mm) 0.20.320.20.250.25
Phase thickness (mum) 0.330.520.11 0.25
Tstart (C) 40.40.40.80.60.
Tend (C)    200.300.
Heat rate (K/min) 8.8.6.2.5.
Initial hold (min) 0.8010.83.194  
Final hold (min)      
I 1327.51327.71332.81330.1365.
ReferenceYin and Sun, 1990Yin and Sun, 1990Yin and Sun, 1990Sugisawa, Yamamoto, et al., 1989Schwab and Schreier, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-1DB-1
Column length (m) 50.50.50.60.
Carrier gas     
Substrate     
Column diameter (mm) 0.300.320.320.32
Phase thickness (mum)     
Tstart (C) 40.0.50.50.
Tend (C) 230.250.250.250.
Heat rate (K/min) 3.53.3.4.
Initial hold (min) 5.  0.1
Final hold (min)    5.
I 1324.1325.1325.1324.
ReferenceNykanen, 1986Habu, Flath, et al., 1985Habu, Flath, et al., 1985Flath, Mon, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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