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Phenol, 2-methyl-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBRTX-5CP-Sil 8CB-MSHP-5MSDB-1
Column length (m) 50.30.60.30.30.
Carrier gas  N2 HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 60.40.40.60.40.
Tend (C) 220.300.280.280.325.
Heat rate (K/min) 4.5.4.3.3.
Initial hold (min) 5.2.2.  
Final hold (min) 30.10.5.  
I 1052.1042.71071.1073.1031.1
ReferenceMahadevan and Farmer, 2006Ádámová, Orinák, et al., 2005Hierro, de la Hoz, et al., 2004Mimica-Dukic, Kujundzic, et al., 2003Sun and Stremple, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CB5 % Phenyl methyl siloxaneOV-1DB-1
Column length (m) 50.50.25. 30.
Carrier gas   He N2
Substrate      
Column diameter (mm) 0.320.32  0.32
Phase thickness (mum)     0.25
Tstart (C) 60.60.80.35.150.
Tend (C) 220.220.300.300.280.
Heat rate (K/min) 4.4.20.8.3.
Initial hold (min) 5.5.3.  
Final hold (min) 30.30.0.  
I 1054.1080.1042.1029.71032.
ReferenceChevance and Farmer, 1999Chevance and Farmer, 1999Climent and Miranda, 1996Gautzsch and Zinn, 1996Coen, Engel, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-5
Column length (m) 30.30.60.30.
Carrier gas N2N2 He
Substrate     
Column diameter (mm) 0.2350.2350.320.26
Phase thickness (mum) 0.250.251.0.25
Tstart (C) 50.50.-50.50.
Tend (C)   180.300.
Heat rate (K/min) 10.5.6.6.
Initial hold (min) 0.0.4.4.
Final hold (min)    20.
I 1042.1044.1029.1055.
ReferenceGerbino and Castello, 1995Gerbino and Castello, 1995Kaiser and Siegl, 1994Rostad and Pereira, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Mahadevan and Farmer, 2006
Mahadevan, K.; Farmer, L., Key Odor Impact Compounds in Three Yeast Extract Pastes, J. Agric. Food Chem., 2006, 54, 19, 7242-7250, https://doi.org/10.1021/jf061102x . [all data]

Ádámová, Orinák, et al., 2005
Ádámová, M.; Orinák, A.; Halás, L., Retention indices as identification tool in pyrolysis-capillary gas chromatography, J. Chromatogr. A, 2005, 1087, 1-2, 131-141, https://doi.org/10.1016/j.chroma.2005.01.003 . [all data]

Hierro, de la Hoz, et al., 2004
Hierro, E.; de la Hoz, L.; Ordóñez, J.A., Headspace volatile compounds from salted and occasionally smoked dried meats (cecinas) as affected by animal species, Food Chem., 2004, 85, 4, 649-657, https://doi.org/10.1016/j.foodchem.2003.07.001 . [all data]

Mimica-Dukic, Kujundzic, et al., 2003
Mimica-Dukic, N.; Kujundzic, S.; Sokovic, M.; Couladis, M., Essential oil composition and antifungal activity of Foeniculum vulgare Mill. obtained by different distillation conditions, Phytother. Res., 2003, 17, 4, 368-371, https://doi.org/10.1002/ptr.1159 . [all data]

Sun and Stremple, 2003
Sun, G.; Stremple, P., Retention index characterization of flavor, fragrance, and many other compounds on DB-1 and DB-XLB, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/pdf/b-0279.pdf. [all data]

Chevance and Farmer, 1999
Chevance, F.F.V.; Farmer, L.J., Identification of major volatile odor compounds in frankfurters, J. Agric. Food Chem., 1999, 47, 12, 5151-5160, https://doi.org/10.1021/jf990515d . [all data]

Climent and Miranda, 1996
Climent, M.J.; Miranda, M.A., Gas chromatographic - mass spectrometric study of photodegradation of carbamate pesticides, J. Chromatogr. A, 1996, 738, 2, 225-231, https://doi.org/10.1016/0021-9673(96)00084-2 . [all data]

Gautzsch and Zinn, 1996
Gautzsch, R.; Zinn, P., Use of incremental models to estimate the retention indexes of aromatic compounds, Chromatographia, 1996, 43, 3/4, 163-176, https://doi.org/10.1007/BF02292946 . [all data]

Coen, Engel, et al., 1995
Coen, M.; Engel, R.; Nahrstedt, A., Chavicol «beta»-D-glucoside, a phenylpropanoid heteroside, benzyl-«beta»-D-glucoside and glycosidically bound volatiles from subspecies of Cedronella canariensis, Phytochemistry, 1995, 40, 1, 149-155, https://doi.org/10.1016/0031-9422(95)00241-X . [all data]

Gerbino and Castello, 1995
Gerbino, T.C.; Castello, G., Prediction of programmed temperature retention indices on capillary columns of different polarities, J. Chromatogr. A, 1995, 699, 1-2, 161-171, https://doi.org/10.1016/0021-9673(95)00024-H . [all data]

Kaiser and Siegl, 1994
Kaiser, E.W.; Siegl, W.O., High resolution gas chromatographic determination of the atmospheric reactivity of engine-out hydrocarbon emissions from a spark-ignited engine, J. Hi. Res. Chromatogr., 1994, 17, 4, 264-270, https://doi.org/10.1002/jhrc.1240170414 . [all data]

Rostad and Pereira, 1986
Rostad, C.E.; Pereira, W.E., Kovats and Lee retention indices determined by gas chromatography/mass spectrometry for organic compounds of environmental interest, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 6, 328-334, https://doi.org/10.1002/jhrc.1240090603 . [all data]


Notes

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