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o-Xylene

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Kovats' RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-20Supelcowax-10DB-WaxDB-WaxBP-20
Column length (m) 25.60.60.60.25.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.20.250.250.250.20
Phase thickness (mum) 0.25 0.250.25 
Tstart (C) 50.35.40.40.65.
Tend (C) 200.200.200.200.180.
Heat rate (K/min) 4.3.3.3.12.
Initial hold (min) 5.5.5.5.3.
Final hold (min)  20.   
I 1184.1181.1185.1185.1191.
ReferenceShimadzu, 2003Wong and Teng, 1994Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990MacLeod and Pieris, 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase Carbowax 20MCarbowax 20M
Column length (m) 70.70.
Carrier gas N2N2
Substrate   
Column diameter (mm) 0.280.28
Phase thickness (mum)   
Tstart (C) 80.80.
Tend (C) 200.200.
Heat rate (K/min) 2.2.
Initial hold (min)   
Final hold (min)   
I 1178.1183.
ReferenceYamaguchi and Shibamoto, 1981Yamaguchi and Shibamoto, 1981
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Shimadzu, 2003
Shimadzu, Gas chromatography analysis of organic solvents using capillary columns (No. 2), 2003, retrieved from http://www.shimadzu.com/apps/form.cfm. [all data]

Wong and Teng, 1994
Wong, K.C.; Teng, Y.E., Volatile Components of Mimusops elengi L. Flowers, J. Essent. Oil Res., 1994, 6, 5, 453-458, https://doi.org/10.1080/10412905.1994.9698425 . [all data]

Tatsuka, Suekane, et al., 1990
Tatsuka, K.; Suekane, S.; Sakai, Y.; Sumitani, H., Volatile constituents of kiwi fruit flowers: simultaneous distillation and extraction versus headspace sampling, J. Agric. Food Chem., 1990, 38, 12, 2176-2180, https://doi.org/10.1021/jf00102a015 . [all data]

MacLeod and Pieris, 1983
MacLeod, A.J.; Pieris, N.M., Volatile components of papaya (Carica papaya L.) with particular reference to glucosinolate products, J. Agric. Food Chem., 1983, 31, 5, 1005-1008, https://doi.org/10.1021/jf00119a021 . [all data]

Yamaguchi and Shibamoto, 1981
Yamaguchi, K.; Shibamoto, T., Volatile constituents of green tea, Gyokuro (Camellia sinensis L. var Yabukita), J. Agric. Food Chem., 1981, 29, 2, 366-370, https://doi.org/10.1021/jf00104a035 . [all data]


Notes

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