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Benzene, 1,2-dimethoxy-4-(1-propenyl)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51495.Zeller and Rychlik, 200630. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 6. K/min; Tend: 230. C
CapillaryDB-51508.Zhang, Xu, et al., 200530. m/0.25 mm/0.25 «mu»m, N2, 45. C @ 10. min, 2.5 K/min, 180. C @ 20. min
CapillaryBPX-51520.Zabaras and Wyllie, 200150. m/0.22 mm/0.25 «mu»m, H2, 60. C @ 5. min, 4. K/min, 180. C @ 5. min
CapillaryHP-51455.Lazari, Skaltsa, et al., 200030. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryOV-11461.Bicchi, Fresia, et al., 199725. m/0.25 mm/0.3 «mu»m, H2, 50. C @ 1. min, 3. K/min, 200. C @ 20. min

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-51480.García, Alvarez, et al., 200250. m/0.2 mm/0.33 «mu»m, He; Program: 50C(2min) => 5C/min => 150C => 10C/min => 250C(30min)
CapillaryHP-51480.García, Alvarez, et al., 200250. m/0.2 mm/0.33 «mu»m, He; Program: 50C(2min) => 5C/min => 150C => 10C/min => 250C(30min)

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-FFAP2189.Zeller and Rychlik, 200630. m/0.32 mm/0.25 «mu»m, He, 40. C @ 1. min, 6. K/min; Tend: 230. C
CapillaryCarbowax 20M2196.Bicchi, Fresia, et al., 199725. m/0.25 mm/0.3 «mu»m, 50. C @ 1. min, 3. K/min, 200. C @ 20. min

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51492.Andrade, Cardoso, et al., 201130. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51492.Ho, Wang, et al., 200930. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryDB-51492.Rahimi-Nasrabadi, Gholivand, et al., 200930. m/0.25 mm/0.25 «mu»m, Nitrogen, 40. C @ 1. min, 3. K/min, 250. C @ 10. min
CapillaryCP Sil 8 CB1504.Suárez, Vásquez, et al., 2005He, 60. C @ 5. min, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 290. C
CapillaryDB-51491.Caredda, Marongiu, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 280. C @ 30. min; Tstart: 60. C
CapillaryOV-1011468.Menon, Chacko, et al., 1999N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C
CapillaryOV-1011468.Sugisawa, Yamamoto, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51492.Andrade, Cardoso, et al., 201130. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryDB-11466.Delort and Jaquier, 200960. m/0.25 mm/0.25 «mu»m, Helium; Program: 50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)
CapillaryHP-5MS1462.Deng, Li, et al., 200430. m/0.25 mm/0.25 «mu»m, He; Program: 60C => 10C/min => 160C => 12C/min => 300C (5min)

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryCarbowax2126.Singh, Kumar, et al., 200760. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 40. C; Tend: 180. C
CapillaryInnowax2185.Joichi, Yomogida, et al., 200560. m/0.25 mm/0.25 «mu»m, He, 5. K/min, 240. C @ 30. min; Tstart: 60. C
CapillaryTC-Wax2176.Miyazawa, Yamafuji, et al., 20033. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 240. C
CapillarySupelcowax-102194.Choo, Wong, et al., 199930. m/0.25 mm/0.25 «mu»m, 4. K/min; Tstart: 60. C; Tend: 220. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zeller and Rychlik, 2006
Zeller, A.; Rychlik, M., Character impact odorants of fennel fruits and fennel tea, J. Agric. Food Chem., 2006, 54, 10, 3686-3692, https://doi.org/10.1021/jf052944j . [all data]

Zhang, Xu, et al., 2005
Zhang, F.; Xu, Q.; Fu, S.; Ma, X.; Xiao, H.; Liang, X., Chemical constituents of the essential oil of Asarum forbesii Maxim (Aristolochiaceae), Flavour Fragr. J., 2005, 20, 3, 318-320, https://doi.org/10.1002/ffj.1423 . [all data]

Zabaras and Wyllie, 2001
Zabaras, D.; Wyllie, S.G., Quantitative analysis of terpenoids in the gas phase using headspace solid-phase microextraction (HS-SPME), Flavour Fragr. J., 2001, 16, 6, 411-416, https://doi.org/10.1002/ffj.1025 . [all data]

Lazari, Skaltsa, et al., 2000
Lazari, D.M.; Skaltsa, H.D.; Constantinidis, T., Volatile constituents of Cerastium candidissimum, a Greek endemic species, Flavour Fragr. J., 2000, 15, 3, 174-176, https://doi.org/10.1002/1099-1026(200005/06)15:3<174::AID-FFJ886>3.0.CO;2-Y . [all data]

Bicchi, Fresia, et al., 1997
Bicchi, C.; Fresia, M.; Rubiolo, P.; Monti, D.; Franz, C.; Goehler, I., Constituents of Tagetes lucida Cav. ssp. lucida essential oil, Flavour Fragr. J., 1997, 12, 1, 47-52, https://doi.org/10.1002/(SICI)1099-1026(199701)12:1<47::AID-FFJ610>3.0.CO;2-7 . [all data]

García, Alvarez, et al., 2002
García, D.; Alvarez, A.; Tornos, P.; Fernandez, A.; Sáenz, T., Gas chromatographic-mass spectrometry study of the essential oils of Pimenta racemosa var. terebinthina and P. racemosa var. grisea, Z. Naturforsch., 2002, 57c, 449-451. [all data]

Andrade, Cardoso, et al., 2011
Andrade, M.A.; Cardoso, M.G.; Batista, L.R.; Freire, J.M.; Nelson, D.L., Antimicrobial activity and chemical composition of essential oil of Pelargonium odoratissimum, Braz. J. Pharmacognosy, 2011, 21, 1, 47-52. [all data]

Ho, Wang, et al., 2009
Ho, C.-L.; Wang, E.I.-C.; Su, Y.-C., Essential oil compositions and bioactivities of the various parts of Cinnamomum camphora Sieb. var. linallolifera Fujuta, Journal title only in Chinese, 2009, 31, 2, 77-96. [all data]

Rahimi-Nasrabadi, Gholivand, et al., 2009
Rahimi-Nasrabadi, M.; Gholivand, M.B.; Batooli, H.; Vatanara, A., Chemical composition of the essential oil from leaves and flowering aerial parts of Psammogeton canscens (DC). Vake from Iran, J. Medicinal Plants, 2009, 8, 31, 82-86. [all data]

Suárez, Vásquez, et al., 2005
Suárez, A.I.; Vásquez, L.J.; Manzano, M.A.; Compagnone, R.S., Essential oil composition of Croton cuneatus and Croton malambo growing in Venezuela, Flavour Fragr. J., 2005, 20, 6, 611-614, https://doi.org/10.1002/ffj.1498 . [all data]

Caredda, Marongiu, et al., 2002
Caredda, A.; Marongiu, B.; Porcedda, S.; Soro, C., Supercritical carbon dioxide extraction and characterization of Laurus nobilis essential oil, J. Agric. Food Chem., 2002, 50, 6, 1492-1496, https://doi.org/10.1021/jf0108563 . [all data]

Menon, Chacko, et al., 1999
Menon, A.N.; Chacko, S.; Narayanan, C.S., Free and glycosidically bound volatiles of cardamom (Eletteria cardamomum Maton var. miniscula Burkill), Flavour Fragr. J., 1999, 14, 1, 65-68, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<65::AID-FFJ789>3.0.CO;2-A . [all data]

Sugisawa, Yamamoto, et al., 1989
Sugisawa, H.; Yamamoto, M.; Tamura, H.; Takagi, N., The comparison of volatile components in peel oil from four species of navel orange, Nippon Shokuhin Kogio Gakkaishi, 1989, 36, 6, 455-462, https://doi.org/10.3136/nskkk1962.36.6_455 . [all data]

Delort and Jaquier, 2009
Delort, E.; Jaquier, A., Novel terpenyl esters from Australian finger lime (Citrus australasica) peel extract, Flav. Fragr. J., 2009, 24, 3, 123-132, https://doi.org/10.1002/ffj.1922 . [all data]

Deng, Li, et al., 2004
Deng, C.; Li, N.; Zhang, X., Rapid determination of essential oil in Acorus tatarinowii Schott. by pressurized hot water extraction followed by solid-phase microextraction and gas chromatography-mass spectrometry, J. Chromatogr. A, 2004, 1059, 1-2, 149-155, https://doi.org/10.1016/j.chroma.2004.10.005 . [all data]

Singh, Kumar, et al., 2007
Singh, B.; Kumar, R.; Bhandari, S.; Pathania, S.; Lal, B., Volatile constituents of natural Boswellia serrata oleo-gum-resin and commercial samples, Flavour Fragr. J., 2007, 22, 2, 145-147, https://doi.org/10.1002/ffj.1772 . [all data]

Joichi, Yomogida, et al., 2005
Joichi, A.; Yomogida, K.; Awano, K.; Ueda, Y., Volatile components of tea-scented modern roses and ancient Chinese roses, Flavour Fragr. J., 2005, 20, 2, 152-157, https://doi.org/10.1002/ffj.1388 . [all data]

Miyazawa, Yamafuji, et al., 2003
Miyazawa, M.; Yamafuji, C.; Kurose, K.; Ishikawa, Y., Volatile components of the rhizomes of Cirsium japonicum DC, Flavour Fragr. J., 2003, 18, 1, 15-17, https://doi.org/10.1002/ffj.1135 . [all data]

Choo, Wong, et al., 1999
Choo, L.-C.; Wong, S.-M.; Liew, K.-Y., Essential oil of nutmeg pericarp, J. Sci. Food Agric., 1999, 79, 13, 1954-1957, https://doi.org/10.1002/(SICI)1097-0010(199910)79:13<1954::AID-JSFA460>3.0.CO;2-I . [all data]


Notes

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