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Biphenyl

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1OV-1SE-33
Column length (m) 25.25.25.25.10.
Carrier gas N2N2N2N2H2
Substrate      
Column diameter (mm) 0.20.20.20.20.20
Phase thickness (mum) 0.330.330.330.330.15
Temperature (C) 150.150.150.160.120.
I 1369.1369.1370.1378.1353.
ReferenceZhang, Chen, et al., 1997Zhang, Chen, et al., 1997Zhang, Chen, et al., 1997Zhang, Chen, et al., 1997Juvancz, Cserháti, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1SE-54Methyl SiliconeMethyl Silicone
Column length (m) 25.25.10.  
Carrier gas N2N2He  
Substrate      
Column diameter (mm) 0.200.200.200.320.32
Phase thickness (mum)   0.150.250.25
Temperature (C) 100.100.120.125.125.
I 1340.1340.1382.1351.1351.
ReferenceZhang, Li, et al., 1992Zhang, Li, et al., 1992Juvancz, Pulsipher, et al., 1989Bemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Temperature (C) 125.125.125.125.125.
I 1351.1352.1352.1352.1352.
ReferenceBemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeSE-30
Column length (m)     25.
Carrier gas     N2
Substrate      
Column diameter (mm) 0.320.320.320.320.33
Phase thickness (mum) 0.250.250.250.25 
Temperature (C) 125.125.125.125.180.
I 1352.1352.1352.1354.1387.
ReferenceBemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987Bemgård, Blomberg, et al., 1987Korhonen and Lind, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedPacked
Active phase SE-30OV-101OV-101OV-101SE-30
Column length (m) 100.50.50.3. 
Carrier gas  N2N2  
Substrate    Chromosorb W HP (80-100 mesh) 
Column diameter (mm) 0.50.30.3  
Phase thickness (mum)      
Temperature (C) 130.140.160.200.150.
I 1359.1366.31377.91396.1373.
ReferenceBredael, 1982Gerasimenko, Kirilenko, et al., 1981Gerasimenko, Kirilenko, et al., 1981Albro, Haseman, et al., 1977Shlyakhov, Anvaer, et al., 1975
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SE-30Polymethylsiloxane, (PMS-20000)SE-30SE-30SE-30
Column length (m)  2.   
Carrier gas  He   
Substrate  Chromosorb W   
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 200.50.130.170.184.
I 1405.1398.71354.1380.1399.
ReferenceShlyakhov, Anvaer, et al., 1975Ainshtein and Shulyatieva, 1972Antheaume and Guiochon, 1965Antheaume and Guiochon, 1965Antheaume and Guiochon, 1965
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase Methyl Silicone
Column length (m)  
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (mum)  
Temperature (C) 130.
I 1354.
ReferenceAntheaume and Guiochon, 1965
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zhang, Chen, et al., 1997
Zhang, M.; Chen, B.; Shen, S.; Chen, S., Compositional studies of high-temperature coal tar by g.c.-FT-i.r. analysis of middle oil fractions, Fuel, 1997, 76, 5, 415-423, https://doi.org/10.1016/S0016-2361(97)85518-4 . [all data]

Juvancz, Cserháti, et al., 1994
Juvancz, Z.; Cserháti, T.; Markides, K.E.; Bradshaw, J.S.; Lee, M.L., Characterization of some new polysiloxane stationary phases by principal component analysis, Chromatographia, 1994, 38, 3/4, 227-231, https://doi.org/10.1007/BF02290341 . [all data]

Zhang, Li, et al., 1992
Zhang, M.J.; Li, S.D.; Chen, B.J., Compositional studies of high-temperature coal tar by GC/FTIR analysis of light oil fractions, Chromatographia, 1992, 33, 3/4, 138-146, https://doi.org/10.1007/BF02275894 . [all data]

Juvancz, Pulsipher, et al., 1989
Juvancz, Z.; Pulsipher, M.A.; Tarbet, B.J.; Schirmer, M.M.; Johnson, R.S.; Markides, K.E.; Bradshaw, J.S.; Lee, M.L., New cyanophenyl-containing polysiloxane stationary phases for capillary column gas chromatography, J. Microcolumn Sep., 1989, 1, 3, 142-149, https://doi.org/10.1002/mcs.1220010307 . [all data]

Bemgård, Blomberg, et al., 1987
Bemgård, A.; Blomberg, L.; Lymann, M.; Claude, S.; Tabacchi, R., Siloxane/silarylene copolymers as stationary phases for capillary gas chromatography. Part I: Evaluation of silanol terminated dimethyl substituted polymers, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1987, 10, 5, 302-318, https://doi.org/10.1002/jhrc.1240100516 . [all data]

Korhonen and Lind, 1985
Korhonen, I.O.O.; Lind, M.A., Gas-liquid chromatographic analyses. XXXIV. Separation and retention indices with retention increments of some nitrated polynuclear aromatic hydrocarbons on a low-polarity (SE-30) capillary column, J. Chromatogr., 1985, 322, 71-81, https://doi.org/10.1016/S0021-9673(01)97660-5 . [all data]

Bredael, 1982
Bredael, P., Retention indices of hydrocarbons on SE-30, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1982, 5, 6, 325-328, https://doi.org/10.1002/jhrc.1240050610 . [all data]

Gerasimenko, Kirilenko, et al., 1981
Gerasimenko, V.A.; Kirilenko, A.V.; Nabivach, V.M., Capillary gas chromatography of aromatic compounds found in coal tar fractions, J. Chromatogr., 1981, 208, 1, 9-16, https://doi.org/10.1016/S0021-9673(00)87953-4 . [all data]

Albro, Haseman, et al., 1977
Albro, P.W.; Haseman, J.K.; Clemmer, T.A.; Corbett, B.J., Identification of the Individual Polychlorinated Biphenyls in a Mixture by Gas-Liquid Chromatography, J. Chromatogr., 1977, 136, 1, 147-153, https://doi.org/10.1016/S0021-9673(00)83003-4 . [all data]

Shlyakhov, Anvaer, et al., 1975
Shlyakhov, A.F.; Anvaer, B.I.; Zolotareva, O.V.; Romina, N.N.; Novikova, N.V.; Koreshkova, R.I., On the possibility of group indentification of hydrocarbons by gas chromatography from temperature coefficients of retention indices, Zh. Anal. Khim., 1975, 30, 788-792. [all data]

Ainshtein and Shulyatieva, 1972
Ainshtein, A.A.; Shulyatieva, T.I., Retention indices of alkyl- and arylchlorosilanes, Zh. Anal. Khim., 1972, 27, 816-821. [all data]

Antheaume and Guiochon, 1965
Antheaume, J.; Guiochon, G., Application de la chromatographie en phase gazeuse à l'étude de la composition des fractions moyennes d'un brut pétrolier, Bull. Soc. Chim. Fr., 1965, 2, 298-307. [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References