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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-1HP-5HP-5ZB-5SE-30
Column length (m) 50.50.60.30. 
Carrier gas HeliumHeliumHeHe 
Substrate      
Column diameter (mm) 0.200.200.320.25 
Phase thickness (mum) 0.330.330.250.25 
Tstart (C) 50.50.30.40.82.
Tend (C) 280.280.260.200.177.
Heat rate (K/min) 2.10.2.10.1.7
Initial hold (min)   2.  
Final hold (min) 20.8.528.2. 
I 1200.1242.1240.31224.1221.6
ReferenceDu, Clery, et al., 2008Du, Clery, et al., 2008Leffingwell and Alford, 2005Kluchinsky, Sheely, et al., 2002Bur'yan and Nabivach, 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-1DB-1Ultra-1DB-1
Column length (m)  60.60.25.60.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm)  0.250.250.320.32
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 82.50.50.80.50.
Tend (C) 177.240.240.260.250.
Heat rate (K/min) 1.73.3.3.4.
Initial hold (min)  5.5.  
Final hold (min)      
I 1221.61201.1206.1199.1199.
ReferenceBur'yan and Nabivach, 1992Ishihara, Tsuneya, et al., 1992Ishihara, Tsuneya, et al., 1992Okumura, 1991Flath, Matsumoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase DB-1SE-30
Column length (m) 60.60.
Carrier gas  N2
Substrate   
Column diameter (mm) 0.320.32
Phase thickness (mum) 0.25 
Tstart (C) 50.50.
Tend (C) 250.275.
Heat rate (K/min) 4.5.
Initial hold (min)  8.
Final hold (min)  10.
I 1200.1203.
ReferenceFlath, Matsumoto, et al., 1989Ibrahim and Suffet, 1988
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Du, Clery, et al., 2008
Du, Z.; Clery, R.; Hammond, C.J., Volatile organic nitrogen-containing constituents in ambrette seed Abelmoschus moschatus Medik (Malvaceae), J. Agric. Food Chem., 2008, 56, 16, 7388-7392, https://doi.org/10.1021/jf800958d . [all data]

Leffingwell and Alford, 2005
Leffingwell, J.C.; Alford, E.D., Volatile constituents of Perique tobacco, Electron. J. Environ. Agric. Food Chem., 2005, 4, 2, 899-915. [all data]

Kluchinsky, Sheely, et al., 2002
Kluchinsky, T.A., Jr.; Sheely, M.V.; Savage, P.B.; Smith, P.A., Formation of 2-chlorobenzylidenemalononitrile (CS riot control agent) thermal degradation products at elevated temperatures, J. Chromatogr. A, 2002, 952, 1-2, 205-213, https://doi.org/10.1016/S0021-9673(02)00096-1 . [all data]

Bur'yan and Nabivach, 1992
Bur'yan, P.; Nabivach, V.M., Investigation of composition of higher heterocnitrogen bases of brown coal tar, Coke Chem. (Engl. Transl.), 1992, 5, 29-33. [all data]

Ishihara, Tsuneya, et al., 1992
Ishihara, M.; Tsuneya, T.; Shiga, M.; Kawashima, S.; Yamagishi, K.; Yoshida, F.; Sato, H.; Uneyama, K., New pyridine derivatives and basic components in spearmint oil (Mentha gentilis f. cardiaca) and peppermint oil (Mentha piperita), J. Agric. Food Chem., 1992, 40, 9, 1647-1655, https://doi.org/10.1021/jf00021a034 . [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]

Flath, Matsumoto, et al., 1989
Flath, R.A.; Matsumoto, K.E.; Binder, R.G.; Cunningham, R.T.; Mon, T.R., Effect of pH on the volatiles of hydrolyzed protein insect baits, J. Agric. Food Chem., 1989, 37, 3, 814-819, https://doi.org/10.1021/jf00087a053 . [all data]

Ibrahim and Suffet, 1988
Ibrahim, E.A.; Suffet, I.H., Freon FC-113, an Alternative to Methylene Chloride for Liquid-Liquid Extraction of Trace Organics from Chlorinated Drinking Water, J. Chromatogr., 1988, 454, 217-232, https://doi.org/10.1016/S0021-9673(00)88615-X . [all data]


Notes

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