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Naphthalene, 1-methyl-

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SqualaneOV-1OV-1OV-1
Column length (m) 30.50.25.25.25.
Carrier gas He N2N2N2
Substrate      
Column diameter (mm) 0.53 0.20.20.2
Phase thickness (mum) 3. 0.330.330.33
Temperature (C) 170.120.150.150.150.
I 1330.121293.71318.1318.1318.
ReferenceKuhn, 2001Gerasimenko and Nabivach, 1997Zhang, Chen, et al., 1997Zhang, Chen, et al., 1997Zhang, Chen, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedCapillary
Active phase OV-1HP-1HP-1OV-1OV-101
Column length (m) 25.25.25.2.550.
Carrier gas N2N2N2 He
Substrate    Chromosorb W HP 
Column diameter (mm) 0.20.200.20 0.25
Phase thickness (mum) 0.33    
Temperature (C) 160.100.100.150.145.
I 1326.1277.1278.1306.1327.
ReferenceZhang, Chen, et al., 1997Zhang, Li, et al., 1992Zhang, Li, et al., 1992Antal, 1984Grinberg, Tokarev, et al., 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SE-30SE-30SE-30SE-30
Column length (m) 100.100.100.100.100.
Carrier gas He    
Substrate      
Column diameter (mm) 0.250.50.50.50.5
Phase thickness (mum)      
Temperature (C) 145.100.130.150.80.
I 1326.1281.1303.1318.1268.
ReferenceGrinberg, Tokarev, et al., 1984Bredael, 1982Bredael, 1982Bredael, 1982Bredael, 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneOV-101OV-1Squalane
Column length (m) 50.50.50.50. 
Carrier gas N2N2N2  
Substrate      
Column diameter (mm) 0.250.250.30.23 
Phase thickness (mum)      
Temperature (C) 86.96.140.130.130.
I 1264.71267.91309.01302.1279.
ReferenceMacák, Nabivach, et al., 1982Macák, Nabivach, et al., 1982Gerasimenko, Kirilenko, et al., 1981Engewald, Wennrich, et al., 1979Bogoslovsky, Anvaer, et al., 1978
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualane
Column length (m)  50.50.
Carrier gas    
Substrate    
Column diameter (mm)  0.250.25
Phase thickness (mum)    
Temperature (C) 130.86.96.
I 1294.1264.71267.9
ReferenceBogoslovsky, Anvaer, et al., 1978Nabivach, Bur'yan, et al., 1978Nabivach, Bur'yan, et al., 1978
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kuhn, 2001
Kuhn, E.R., Selectivity vs. polarity: the fundamentals of chromatographic separation, J. Sep. Sci., 2001, 24, 6, 473-476, https://doi.org/10.1002/1615-9314(20010601)24:6<473::AID-JSSC473>3.0.CO;2-Y . [all data]

Gerasimenko and Nabivach, 1997
Gerasimenko, V.A.; Nabivach, V.M., Sorption-structure correlations in the series of alkyl derivatives of naphthalene, J. Anal. Chem. USSR (Engl. Transl.), 1997, 52, 1, 21-27. [all data]

Zhang, Chen, et al., 1997
Zhang, M.; Chen, B.; Shen, S.; Chen, S., Compositional studies of high-temperature coal tar by g.c.-FT-i.r. analysis of middle oil fractions, Fuel, 1997, 76, 5, 415-423, https://doi.org/10.1016/S0016-2361(97)85518-4 . [all data]

Zhang, Li, et al., 1992
Zhang, M.J.; Li, S.D.; Chen, B.J., Compositional studies of high-temperature coal tar by GC/FTIR analysis of light oil fractions, Chromatographia, 1992, 33, 3/4, 138-146, https://doi.org/10.1007/BF02275894 . [all data]

Antal, 1984
Antal, J., Adatok az alkil-naftalinok gáz-folyadék kromatográfiájához, I., Magy. Kem. Foly., 1984, 90, 121-125. [all data]

Grinberg, Tokarev, et al., 1984
Grinberg, A.A.; Tokarev, M.I.; Bigdash, T.V.; Kogan, L.O.; Leont'eva, S.A., Special features of using Kovats retention indices in chromatomass spectrometric analysis, Zh. Anal. Khim., 1984, 39, 6, 909-911. [all data]

Bredael, 1982
Bredael, P., Retention indices of hydrocarbons on SE-30, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1982, 5, 6, 325-328, https://doi.org/10.1002/jhrc.1240050610 . [all data]

Macák, Nabivach, et al., 1982
Macák, J.; Nabivach, V.; Buryan, P.; Sindler, S., Dependence of retention indices of alkylbenzenes on their molecular structure, J. Chromatogr., 1982, 234, 2, 285-302, https://doi.org/10.1016/S0021-9673(00)81867-1 . [all data]

Gerasimenko, Kirilenko, et al., 1981
Gerasimenko, V.A.; Kirilenko, A.V.; Nabivach, V.M., Capillary gas chromatography of aromatic compounds found in coal tar fractions, J. Chromatogr., 1981, 208, 1, 9-16, https://doi.org/10.1016/S0021-9673(00)87953-4 . [all data]

Engewald, Wennrich, et al., 1979
Engewald, W.; Wennrich, L.; Ritter, E., Molekülstruktur und Retentionsverhalten. XII. Zur Retention von Alkylnaphthalinen Bei der Gasverteilungs- und Gas-Adsorptions-Chromatographie, J. Chromatogr., 1979, 174, 2, 315-323, https://doi.org/10.1016/S0021-9673(00)86005-7 . [all data]

Bogoslovsky, Anvaer, et al., 1978
Bogoslovsky, Yu.N.; Anvaer, B.I.; Vigdergauz, M.S., Chromatographic constants in gas chromatography (in Russian), Standards Publ. House, Moscow, 1978, 192. [all data]

Nabivach, Bur'yan, et al., 1978
Nabivach, V.M.; Bur'yan, P.; Matsak, I., Retention indices of aromatic hydrocarbons on a squalane capillary column, Zh. Anal. Khim., 1978, 33, 7, 1108-1113. [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References