Phenol, 2-methoxy-
- Formula: C7H8O2
- Molecular weight: 124.1372
- IUPAC Standard InChIKey: LHGVFZTZFXWLCP-UHFFFAOYSA-N
- CAS Registry Number: 90-05-1
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: Phenol, o-methoxy-; o-Guaiacol; o-Hydroxyanisole; o-Methoxyphenol; Anastil; Guaiacol; Guaiastil; Guaicolina; Guajol; Guasol; O-Methyl catechol; Pyrocatechol monomethyl ether; Pyroguaiac acid; 1-Hydroxy-2-methoxybenzene; 2-Hydroxyanisole; 2-Methoxyphenol; Guaicol; Guajakol; Methylcatechol; Methylcatachol; Catechol monomethyl ether; o-Guiacol; ortho-Guaiacol; NSC 3815; 2-methoxyphenol (guaiacol); 2-Methoxy phenol (guiacol); guiacol; guaiacol (2-methoxyphenol)
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Van Den Dool and Kratz RI, polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | Innowax | DB-FFAP | DB-FFAP | FFAP |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | H2 | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.5 | 0.5 | 0.25 |
Tstart (C) | 50. | 45. | 35. | 35. | 35. |
Tend (C) | 180. | 210. | 225. | 225. | 225. |
Heat rate (K/min) | 3.5 | 3.5 | 4. | 4. | 10. |
Initial hold (min) | 2. | 5. | 5. | 5. | 5. |
Final hold (min) | 25. | 20. | 30. | 30. | 25. |
I | 1862. | 1875. | 1867. | 1871. | 1862. |
Reference | Botelho, Caldeira, et al., 2007 | Botelho, Caldeira, et al., 2007 | Jarunrattanasri, Theerakulkait, et al., 2007 | Jarunrattanasri, Theerakulkait, et al., 2007 | Lozano P.R., Drake M., et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | FFAP | DB-Wax | DB-Wax | FFAP | BP-20 |
Column length (m) | 30. | 30. | 30. | 30. | 50. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.32 | 0.22 |
Phase thickness (μm) | 0.25 | 0.5 | 0.5 | 0.25 | 0.25 |
Tstart (C) | 35. | 40. | 40. | 40. | 60. |
Tend (C) | 225. | 250. | 240. | 240. | 220. |
Heat rate (K/min) | 10. | 4. | 7. | 6. | 2. |
Initial hold (min) | 5. | 5. | 2. | ||
Final hold (min) | 25. | 15. | 5. | 10. | 20. |
I | 1841. | 1860. | 1871. | 1846. | 1855. |
Reference | Lozano P.R., Drake M., et al., 2007 | Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007 | Ruiz Perez-Cacho, Mahattanatawee, et al., 2007 | Steinhaus and Schieberle, 2007 | Duquesnoy, Dinh, et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | DB-Wax | DB-Wax | DB-Wax | CP-Wax 52CB |
Column length (m) | 60. | 30. | 30. | 30. | 50. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.5 | 0.5 | 0.5 | |
Tstart (C) | 40. | 40. | 40. | 40. | 60. |
Tend (C) | 265. | 265. | 240. | 240. | 220. |
Heat rate (K/min) | 7. | 7. | 5. | 5. | 4. |
Initial hold (min) | 5. | ||||
Final hold (min) | 5. | 5. | 10. | 10. | 30. |
I | 1889. | 1865. | 1864. | 1864. | 1861. |
Reference | Gurbuz O., Rouseff J.M., et al., 2006 | Gurbuz O., Rouseff J.M., et al., 2006 | Lopez-Galilea I., Fournier N., et al., 2006 | Lopez-Galilea I., Fournier N., et al., 2006 | Mahadevan and Farmer, 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP-Wax 52CB | CP-Wax 52CB | DB-Wax | DB-FFAP | OV-351 |
Column length (m) | 50. | 50. | 30. | 30. | 50. |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.2 | ||
Tstart (C) | 60. | 60. | 50. | 40. | 60. |
Tend (C) | 220. | 220. | 220. | 230. | 220. |
Heat rate (K/min) | 4. | 4. | 4. | 6. | 5. |
Initial hold (min) | 5. | 5. | 4. | 1. | |
Final hold (min) | 30. | 30. | 20. | ||
I | 1861. | 1849. | 1823. | 1875. | 1815. |
Reference | Mahadevan and Farmer, 2006 | Mahadevan and Farmer, 2006 | Osorio, Alarcon, et al., 2006 | Zeller and Rychlik, 2006 | Bonvehí, 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Supelcowax-10 | Stabilwax | DB-Wax | DB-Wax | Innowax |
Column length (m) | 60. | 30. | 30. | 30. | 50. |
Carrier gas | N2 | He | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 1. | 0.5 | 0.5 | 0.25 |
Tstart (C) | 35. | 40. | 40. | 40. | 50. |
Tend (C) | 195. | 230. | 240. | 240. | 220. |
Heat rate (K/min) | 6. | 4. | 7. | 7. | 2. |
Initial hold (min) | 5. | 2. | 3. | ||
Final hold (min) | 60. | 10. | 5. | 5. | 20. |
I | 1823. | 1872. | 1868. | 1868. | 1871. |
Reference | Chung, Fung, et al., 2005 | Fang and Qian, 2005 | Gocmen, Elston, et al., 2005 | Gocmen, Elston, et al., 2005 | Lee, Lee, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | ZB-Wax | DB-Wax | DB-FFAP | Supelcowax-10 | Supelcowax-10 |
Column length (m) | 30. | 30. | 30. | 60. | 30. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.15 | 0.5 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 35. | 40. | 35. | 35. | 50. |
Tend (C) | 220. | 240. | 200. | 195. | 230. |
Heat rate (K/min) | 5. | 7. | 10. | 2. | 3. |
Initial hold (min) | 5. | 5. | 5. | ||
Final hold (min) | 10. | 5. | 30. | 90. | 30. |
I | 1855. | 1872. | 1840. | 1867. | 1849. |
Reference | Ledauphin, Saint-Clair, et al., 2004 | Högnadóttir and Rouseff, 2003 | Karagül-Yüceer, Vlahovich, et al., 2003 | Chung, Yung, et al., 2002 | Moreira, Trugo, et al., 2002 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | Supelcowax-10 | DB-Wax | DB-Wax | DB-Wax |
Column length (m) | 30. | 60. | 60. | 60. | 30. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 1. | 0.25 | 0.25 | 0.25 | 0.5 |
Tstart (C) | 40. | 35. | 40. | 40. | 60. |
Tend (C) | 200. | 195. | 200. | 200. | 245. |
Heat rate (K/min) | 10. | 2. | 2. | 2. | 3. |
Initial hold (min) | 5. | 5. | 5. | 3. | |
Final hold (min) | 30. | 90. | 30. | 20. | |
I | 1873. | 1867. | 1859. | 1872. | 1840. |
Reference | Wu and Cadwallader, 2002 | Chung, Yung, et al., 2001 | Kim, 2001 | Lee, Suriyaphan, et al., 2001 | Wirth, Guo, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | Supelcowax-10 | CP-Wax 52CB | CP-Wax 52CB | CP-Wax 52CB |
Column length (m) | 30. | 60. | 50. | 50. | 50. |
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | 0.32 | 0.32 |
Phase thickness (μm) | 0.5 | 0.25 | |||
Tstart (C) | 60. | 35. | 60. | 60. | 40. |
Tend (C) | 245. | 195. | 220. | 220. | 220. |
Heat rate (K/min) | 3. | 2. | 4. | 4. | 4. |
Initial hold (min) | 3. | 5. | 5. | 5. | |
Final hold (min) | 20. | 90. | 30. | 30. | 30. |
I | 1850. | 1868. | 1856. | 1849. | 1852. |
Reference | Bureau, Baumes, et al., 2000 | Chung, 2000 | Chevance and Farmer, 1999 | Chevance and Farmer, 1999 | Chevance and Farmer, 1999, 2 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP-Wax 52CB | CP-Wax 52CB | Supelcowax-10 | DB-Wax | DB-Wax |
Column length (m) | 50. | 50. | 60. | 60. | 60. |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.53 | 0.53 |
Phase thickness (μm) | 0.25 | 1. | 1. | ||
Tstart (C) | 60. | 40. | 35. | 20. | 20. |
Tend (C) | 220. | 220. | 195. | 200. | 200. |
Heat rate (K/min) | 4. | 4. | 2. | 4. | 4. |
Initial hold (min) | 5. | 5. | 5. | 5. | 5. |
Final hold (min) | 30. | 30. | 90. | 10. | 10. |
I | 1850. | 1851. | 1867. | 1894. | 1896. |
Reference | Chevance and Farmer, 1999, 2 | Chevance and Farmer, 1999, 2 | Chung, 1999 | Ott, Fay, et al., 1997 | Ott, Fay, et al., 1997 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | DB-Wax | PEG-20M | DB-Wax | DB-Wax |
Column length (m) | 60. | 60. | 60. | 60. | 60. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.53 | 0.53 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 1. | 1. | 0.25 | 0.25 | 0.25 |
Tstart (C) | 20. | 20. | 50. | 50. | 50. |
Tend (C) | 200. | 200. | 230. | 230. | 230. |
Heat rate (K/min) | 4. | 4. | 2. | 2. | 2. |
Initial hold (min) | 5. | 5. | 4. | ||
Final hold (min) | 10. | 10. | 60. | 60. | 30. |
I | 1896. | 1897.5 | 1846. | 1846. | 1859. |
Reference | Ott, Fay, et al., 1997 | Ott, Fay, et al., 1997 | Shimoda, Nakada, et al., 1997 | Shimoda, Shiratsuchi, et al., 1996 | Shiratsuchi, Shimoda, et al., 1993 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary |
---|---|---|---|
Active phase | DB-Wax | DB-Wax | DB-Wax |
Column length (m) | 30. | 30. | 30. |
Carrier gas | He | He | He |
Substrate | |||
Column diameter (mm) | 0.25 | 0.259 | 0.259 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 |
Tstart (C) | 50. | 50. | 50. |
Tend (C) | 220. | 240. | 240. |
Heat rate (K/min) | 4. | 4. | 4. |
Initial hold (min) | 3. | 3. | 3. |
Final hold (min) | 20. | ||
I | 1836. | 1829. | 1840. |
Reference | Humpf and Schreier, 1991 | Suárez, Duque, et al., 1991 | Suárez, Duque, et al., 1991 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Botelho, Caldeira, et al., 2007
Botelho, G.; Caldeira, I.; Mendes-Faia, A.; Clímaco, M.C.,
Evaluation of two quantitative gas chromatography-olfactometry methods for clonal red wines differentiation,
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Jarunrattanasri, A.; Theerakulkait, C.; Cadwallader, K.R.,
Aroma Components of Acid-Hydrolyzed Vegetable Protein Made by Partial Hydrolysis of Rice Bran Protein,
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Lozano P.R., Drake M., et al., 2007
Lozano P.R.; Drake M.; Benitez D.; Cadwallader K.R.,
Instrumental and sensory characterization of heat-induced odorants in aseptically packaged soy milk,
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Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007
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Influence of eggs on the aroma composition of a sponge cake and on the aroma release in model studies on flavored sponge cakes,
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Identification of Sulfur Volatiles in Canned Orange Juices Lacking Orange Flavor,
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Changes in headspace volatile concentrations of coffee brews caused by the roasting process and the brewing procedure,
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Key Odor Impact Compounds in Three Yeast Extract Pastes,
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Characterization of Odor-Active Volatiles in Champa ( Campomanesia lineatifolia R. P.),
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Aroma impact components in commercial plain sufu,
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Identification of aroma active compounds in organce essence oil using gas chromatography-olfactometry and gas chromatography-mass spectrometry,
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Chung, Yung, et al., 2002
Chung, H.-Y.; Yung, I.K.S.; Ma, W.C.J.; Kim, J.-S.,
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Wu and Cadwallader, 2002
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Characterization of the aroma of a meatlike process flavoring from soybean-based enzyme-hydrolyzed vegetable protein,
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Chung, Yung, et al., 2001
Chung, H.Y.; Yung, I.K.S.; Kim, J.-S.,
Comparison of volatile components in dried scallops (Chlamys farreri and Patinopecten yessoensis) prepared by boiling and steaming methods,
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Kim, 2001
Kim, J.S.,
Einfluss der Temperatur beim Rösten von Sesam auf Aroma und antioxidative Eigenschaften des Öls, PhD Thesis, Technischen Universität Berlin zur Erlangung des akademischen Grades, Berlin, 2001, 151. [all data]
Lee, Suriyaphan, et al., 2001
Lee, G.-H.; Suriyaphan, O.; Cadwallader, K.R.,
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Wirth, Guo, et al., 2001
Wirth, J.; Guo, W.; Baumes, R.; Günata, Z.,
Volatile compounds released by enzymatic hydrolysis of glycoconjugates of leaves and grape berries from Vitis vinifera muscat of Alexandria and Shiraz cultivars,
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Bureau, Baumes, et al., 2000
Bureau, S.M.; Baumes, R.L.; Razungles, A.J.,
Effects of vine or bunch shading on the glycosylated flavor precursors in grapes of Vitis vinifera L. Cv. Syrah,
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Chung, 2000
Chung, H.Y.,
Volatile flavor components in red fermented soybean (Glycine max) curds,
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Chevance and Farmer, 1999
Chevance, F.F.V.; Farmer, L.J.,
Identification of major volatile odor compounds in frankfurters,
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Chevance and Farmer, 1999, 2
Chevance, F.F.V.; Farmer, L.J.,
Release of volatile odor compounds from full-fat and reduced-fat frankfurters,
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Chung, 1999
Chung, H.Y.,
Volatile components in fermented soybean (Glycine max) curds,
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Ott, Fay, et al., 1997
Ott, A.; Fay, L.B.; Chaintreau, A.,
Determination and origin of the aroma impact compounds of yogurt flavor,
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Shimoda, Nakada, et al., 1997
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Notes
Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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