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Phenol, 2-methoxy-

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Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSVF-5 MSVF-5 MSVF-5 MSVF-5 MS
Column length (m) 30.30.60.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.30.30.40.
Tend (C) 250.280.260.260.250.
Heat rate (K/min) 5.6.2.2.5.
Initial hold (min) 0.51.  3.
Final hold (min) 0.53.28.28.3.
I 1088.1093.1087.1088.1090.
ReferenceFanaro, Duarte, et al., 2012Souza, Re-Poppi, et al., 2012Leffingwell and Alford, 2011Leffingwell and Alford, 2011Liu, Lu, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSZB-5HP-5 MSSE-54RTX-5 MS
Column length (m) 25.30.30.30.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.200.250.250.320.25
Phase thickness (mum) 0.330.250.250.250.50
Tstart (C) 40.40.35.0.35.
Tend (C) 250.280.195.200.225.
Heat rate (K/min) 10.6.2.6.6.
Initial hold (min) 1.1.5.2.5.
Final hold (min)  9.30. 10.
I 1110.1096.1086.1089.1090.
ReferenceMajcher, Lawrowski, et al., 2010Harrison and Priest, 2009Kim and Chung, 2009Laselan, Buettner, et al., 2009Watcharananun, Cadwallader, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSSLB-5MSElite-5MSHP-1
Column length (m) 30.30.10.30.50.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.180.320.2
Phase thickness (mum) 0.250.250.180.50.33
Tstart (C) 50.50.40.40.60.
Tend (C) 280.230.295.280.250.
Heat rate (K/min) 4.4.10.4.2.
Initial hold (min)  4.1.55.4.
Final hold (min)  10. 10.30.
I 1089.1089.1102.1084.1053.
ReferenceZhao, Zeng, et al., 2009Forero, Quijano, et al., 2008Risticevic, Carasek, et al., 2008Tava, Pecetti, et al., 2007Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1DB-5DB-5HP-5MS
Column length (m) 50.50.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.20.320.320.25
Phase thickness (mum) 0.330.33  0.25
Tstart (C) 60.60.60.50.50.
Tend (C) 250.250.250.250.280.
Heat rate (K/min) 2.2.4.4.5.
Initial hold (min) 4.4.5.5.4.
Final hold (min) 30.30.  10.
I 1058.1058.1092.1091.1090.
ReferenceCastel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006, 2Fadel, Mageed, et al., 2006Fadel, Mageed, et al., 2006, 2Kim, Abd El-Aty, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-5CP Sil 5 CBZB-5ZB-5
Column length (m) 30.13.525.60.60.
Carrier gas  HeH2HeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.25  0.250.25
Tstart (C) 40.35.50.40.40.
Tend (C) 200.225.230.250.250.
Heat rate (K/min) 8.6.3.6.6.
Initial hold (min) 3.3. 7.7.
Final hold (min) 20.  1.1.
I 1089.1088.1083.1102.1102.
ReferenceSchirack, Drake, et al., 2006de Souza, Vásquez, et al., 2006Tesso, König, et al., 2006Dötterl and Jürgens, 2005Dötterl, Wolfe, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1ZB-5DB-1DB-1
Column length (m) 60.60.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.35.40.35.35.
Tend (C) 230.230.260.230.230.
Heat rate (K/min) 2.2.6.2.2.
Initial hold (min) 4.4.4.64.4.
Final hold (min) 25.25.1.25.25.
I 1057.1058.1100.1053.1055.
ReferenceLee, Lee, et al., 2005Lee, Lee, et al., 2005Jürgens and Dötterl, 2004Park, Lee, et al., 2004Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5DB-5DB-5
Column length (m) 60.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.35.40.40.60.
Tend (C) 230.230.230.230.240.
Heat rate (K/min) 2.2.6.6.3.
Initial hold (min) 4.4.2.2. 
Final hold (min) 25.25.5.5. 
I 1056.1058.1074.1092.1088.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Sanz, Czerny, et al., 2002Sanz, Czerny, et al., 2002Tellez, Khan, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSSPB-5DB-5MSDB-5
Column length (m) 30.60.60.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.530.250.320.320.32
Phase thickness (mum) 1.50.251.0.250.5
Tstart (C) 40.40.40.40.60.
Tend (C) 225.200.200.195.245.
Heat rate (K/min) 6.2.3.5.3.
Initial hold (min) 5.5. 5.3.
Final hold (min) 30.30. 40.20.
I 1097.1089.1095.1089.1090.
ReferenceCadwallader and Heo, 2001Lee, Suriyaphan, et al., 2001Poligné, Collignan, et al., 2001Suriyaphan, Drake, et al., 2001Kotseridis and Baumes, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-5HP-1DB-5OV-101
Column length (m) 30.50.25.30.10.
Carrier gas H2He HeHelium
Substrate      
Column diameter (mm) 0.320.320.200.250.25
Phase thickness (mum) 0.51. 0.250.52
Tstart (C) 60.40.35.60.35.
Tend (C) 245.190.250.240.225.
Heat rate (K/min) 3.2.4.3.6.
Initial hold (min) 3.5.  3.
Final hold (min) 20.    
I 1090.1103.1056.1088.1066.
ReferenceKotseridis and Baumes, 2000Lopez, Ferreira, et al., 1999Ong and Acree, 1999Tellez, Canel, et al., 1999Deibler, Acree, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-5DB-1HP-1HP-1DB-1
Column length (m) 50.30.25.25.60.
Carrier gas HeHe   
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (mum) 1.0.25   
Tstart (C) 40.50.35.35.30.
Tend (C) 190.200.250.250.200.
Heat rate (K/min) 2.5.4.4.4.
Initial hold (min) 5.   25.
Final hold (min)     20.
I 1103.1057.1056.1056.1058.
ReferenceFerreira, Ardanuy, et al., 1998Kjällstrand, Ramnäs, et al., 1998Ong and Acree, 1998Ong, Acree, et al., 1998Buttery, Ling, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedCapillaryCapillary
Active phase DB-1OV-101SE-54DB-1DB-1
Column length (m) 60.50.3.60.60.
Carrier gas He    
Substrate   Chromosorb G AW DMCS (100-120 mesh)  
Column diameter (mm) 0.250.22 0.320.32
Phase thickness (mum) 0.25  0.250.25
Tstart (C) 50.80.50.50.50.
Tend (C) 250.200.230.250.250.
Heat rate (K/min) 3.52.6.4.4.
Initial hold (min) 5. 2.  
Final hold (min)   10.  
I 1058.1071.1091.1057.1057.
ReferenceStashenko, Torres, et al., 1995Egolf and Jurs, 1993Schieberle, 1991Flath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1
Column length (m) 60.60.50.50.
Carrier gas     
Substrate     
Column diameter (mm) 0.320.320.320.32
Phase thickness (mum) 0.250.25  
Tstart (C) 50.50.0.50.
Tend (C) 250.250.250.250.
Heat rate (K/min) 4.4.3.3.
Initial hold (min)     
Final hold (min)     
I 1058.1059.1059.1057.
ReferenceFlath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989Habu, Flath, et al., 1985Habu, Flath, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Fanaro, Duarte, et al., 2012
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Zhao, Zeng, et al., 2009
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Kjällstrand, Ramnäs, et al., 1998
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Ong, Acree, et al., 1998
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Buttery, Ling, et al., 1997
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Stashenko, Torres, et al., 1995
Stashenko, E.E.; Torres, W.; Morales, J.R.M., A study of the compositional variation of the essential oil of ylang-ylang (Cananga odorata Hook Fil. et Thomson, forma genuina) during flower development, J. Hi. Res. Chromatogr., 1995, 18, 2, 101-104, https://doi.org/10.1002/jhrc.1240180206 . [all data]

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Egolf, L.M.; Jurs, P.C., Quantitative structure-retention and structure-odor intensity relationships for a diverse group of odor-active compounds, Anal. Chem., 1993, 65, 21, 3119-3126, https://doi.org/10.1021/ac00069a027 . [all data]

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Flath, Matsumoto, et al., 1989
Flath, R.A.; Matsumoto, K.E.; Binder, R.G.; Cunningham, R.T.; Mon, T.R., Effect of pH on the volatiles of hydrolyzed protein insect baits, J. Agric. Food Chem., 1989, 37, 3, 814-819, https://doi.org/10.1021/jf00087a053 . [all data]

Habu, Flath, et al., 1985
Habu, T.; Flath, R.A.; Mon, T.R.; Morton, J.F., Volatile components of Rooibos tea (Aspalathus linearis), J. Agric. Food Chem., 1985, 33, 2, 249-254, https://doi.org/10.1021/jf00062a024 . [all data]


Notes

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