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(1aR,4S,4aR,7R,7aS,7bS)-1,1,4,7-Tetramethyldecahydro-1H-cyclopropa[e]azulen-4-ol


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneRTX-5RTX-5HP-5 MSDB-5
Column length (m) 30.30.30.30. 
Carrier gas HeliumNitrogenNitrogenHelium 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.250.250.250.25 
Program 50 0C (2 min) 10 0C/min -> 150 0C 15 0C/min -> 300 0C (10 min)60 0C 95 min) 110 0C 3 0C/min -> 200 0C 5 0C/min -> 220 0C 95 min)not specified40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)not specified
I 1557.1596.1588.1629.1576.
ReferenceHuang, Qin, et al., 2009Leela, Vipin, et al., 2009Leela, Vipin, et al., 2009Mancini, Arnold, et al., 2009Ferreira, Costantin, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB-1
Column length (m) 60.
Carrier gas  
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum)  
Program not specified
I 1548.
ReferenceBinder and Flath, 1989
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Huang, Qin, et al., 2009
Huang, B.; Qin, L.; Chu, Q.; Zhang, Q.; Gao, L.; Zheng, H., Comparison of headspace SPME with hydrodistillation and SFE for analysis of the volatile components of the roots of Valeriana officinalis var. latifolia, Chromatographia, 2009, 69, 5/6, 489-496, https://doi.org/10.1365/s10337-008-0921-y . [all data]

Leela, Vipin, et al., 2009
Leela, N.K.; Vipin, T.M.; Shafeekh, K.M.; Priyanka, V.; Rema, J., Chemical composition of essential oils from aerial parts of Cinnamomum malabatrum (Burman f.) Bercht Presl., Flavor Fragr. J., 2009, 24, 1, 13-16, https://doi.org/10.1002/ffj.1910 . [all data]

Mancini, Arnold, et al., 2009
Mancini, E.; Arnold, N.A.; De Martino, L.; De Feo, V.; Formisano, C.; Rigano, D.; Senatore, F., Chemical composition and phytotoxic effects of essential oils of Salvia hierosolymitana Boiss. and Salvia multicaulis Vahl. var. simplicifolia Boiss. growing wild in Lebanon, Molecules, 2009, 14, 11, 4725-4736, https://doi.org/10.3390/molecules14114725 . [all data]

Ferreira, Costantin, et al., 2001
Ferreira, M.J.P.; Costantin, M.B.; Sartorelli, P.; Rodrigues, G.V.; Limberger, R.; Henriques, A.T.; Kato, M.J.; Emerenciano, V.P., Computer-aided method for identification of components in essential oils by 13C NMR spectroscopy, Anal. Chim. Acta., 2001, 447, 1-2, 125-134, https://doi.org/10.1016/S0003-2670(01)01204-1 . [all data]

Binder and Flath, 1989
Binder, R.G.; Flath, R.A., Volatile components of pineapple guava, J. Agric. Food Chem., 1989, 37, 3, 734-736, https://doi.org/10.1021/jf00087a034 . [all data]


Notes

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