Home Symbol which looks like a small house Up Solid circle with an upward pointer in it

(1aR,4S,4aR,7R,7aS,7bS)-1,1,4,7-Tetramethyldecahydro-1H-cyclopropa[e]azulen-4-ol


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.260.260.250.25
Phase thickness (mum) 0.320.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 250.240.290.300.300.
Heat rate (K/min) 5.3.3.3.3.
Initial hold (min) 30.    
Final hold (min)      
I 1585.1580.1580.1585.1564.
ReferenceYassa and Akhani, 2008Bos, Woerdenbag, et al., 2007Elfami, Bos, et al., 2007Limberger, Scopel, et al., 2007Moreno, Lima, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5DB-5DB-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas HeliumHeHe Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.26
Phase thickness (mum) 0.250.320.250.250.25
Tstart (C) 100.60.60.60.60.
Tend (C) 280.250.300.300.290.
Heat rate (K/min) 4.5.3.3.3.
Initial hold (min) 3.30.   
Final hold (min) 5.    
I 1564.1585.1582.1588.1580.
ReferencePhutdhawong, Kawaree, et al., 2007Yassa and Akhani, 2007Apel, Sobral, et al., 2006Apel, Sobral, et al., 2006, 2Elfami, Komar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-1DB-5DB-5
Column length (m) 30.30.50.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.50.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 300.250.250.300.230.
Heat rate (K/min) 5.10.2.3.3.
Initial hold (min) 5.5. 3. 
Final hold (min) 5. 60.  
I 1597.1582.1578.1587.1580.
ReferenceFiguérédo, Cabassu, et al., 2006Robinson, 2006Bendimerad and Bendiab, 2005Ferraz, Limberger, et al., 2005Limberger, Sobral, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 260.300.300.300.300.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 5.    
Final hold (min) 20.    
I 1608.1587.1588.1589.1588.
ReferenceSenatore, Apostolides Arnold, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Limberger, Sobral, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-1
Column length (m) 30.30.30.60.
Carrier gas  HeHe 
Substrate     
Column diameter (mm) 0.250.250.250.32
Phase thickness (mum) 0.250.250.25 
Tstart (C) 60.60.60.50.
Tend (C) 300.250.250.250.
Heat rate (K/min) 3.3.3.4.
Initial hold (min)    0.1
Final hold (min)    5.
I 1581.1587.1580.1548.
ReferenceSuyenaga, Apel, et al., 2004Limberger, Simões-Pires, et al., 2003Limberger, Simões-Pires, et al., 2002Binder and Flath, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Yassa and Akhani, 2008
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2008, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Bos, Woerdenbag, et al., 2007
Bos, R.; Woerdenbag, H.J.; Kayser, O.; Quax, W.J.; Ruslan, K.; Elfami, Essential oil constituents of Piper cubeba L. fils. from Indonesia, J. Essent. Oil Res., 2007, 19, 1, 14-17, https://doi.org/10.1080/10412905.2007.9699217 . [all data]

Elfami, Bos, et al., 2007
Elfami; Bos, R.; Ruslan, K.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential Oil Constituents of Piper cubeba from Indonesia, 2007, 53-60. [all data]

Limberger, Scopel, et al., 2007
Limberger, R.P.; Scopel, M.; Sobral, M.; Henriques, A.T., Comparative analysis of volatiles from Drimys brasiliensis Miers and D. angustifolia Miers (Winteraceae) from Southern Brazil, Biochem. Syst. Ecol., 2007, 35, 3, 130-137, https://doi.org/10.1016/j.bse.2006.09.007 . [all data]

Moreno, Lima, et al., 2007
Moreno, P.R.H.; Lima, M.E.L.; Sobral, M.; Young, M.C.M.; Cordeiro, I.; Apel, M.A.A.; Limberger, R.P.; Henriques, A.T., Essential oil composition of fruit colour varieties of Eugenia brasiliensis Lam., Sci. Agr.; (Piracicaba Praz.), 2007, 64, 4, 428-432. [all data]

Phutdhawong, Kawaree, et al., 2007
Phutdhawong, W.; Kawaree, R.; Sanjaia, S.; Sengpracha, W.; Buddhasukh, D., Microwave-Assisted Isolation of Essential Oil of Cinnamomum iners Reinw. es Bl.: Comparison with Conventional Hydrodistillation, Molecules, 2007, 12, 4, 868-877, https://doi.org/10.3390/12040868 . [all data]

Yassa and Akhani, 2007
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Apel, Sobral, et al., 2006
Apel, M.A.; Sobral, M.; Zuanazzi, J.A.S.; Henriques, A.T., Essential oil composition of four Plinia species (Myrtaceae), Flavour Fragr. J., 2006, 21, 3, 565-567, https://doi.org/10.1002/ffj.1638 . [all data]

Apel, Sobral, et al., 2006, 2
Apel, M.A.; Sobral, M.; Zuanazzi, J.A.S.; Henriques, A.T., Essential oil composition of Calycorectes australis and Calycorectes psidiiflorus (Myrtaceae), Flavour Fragr. J., 2006, 21, 4, 656-658, https://doi.org/10.1002/ffj.1640 . [all data]

Elfami, Komar, et al., 2006
Elfami, R.B.; Komar, R.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential oil constituents of Piper cubeba from Indonesia, 2006, retrieved from http://dissertations.ub.rug.nl/FILES/facultiew/science/2006/elfahmi/05c5.pdf. [all data]

Figuérédo, Cabassu, et al., 2006
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations. VIII. Chemical composition of essential oils of oreganos of various origins, Flavour Fragr. J., 2006, 21, 1, 134-139, https://doi.org/10.1002/ffj.1543 . [all data]

Robinson, 2006
Robinson, C.J., A new essential oil - Agonis fragrans, A report for the Rural Industries Research and Development Corporation, RIRDC Publication No. 06/090, Rural Industries Research and Development Corporation, Barton, ACT, 2006, 12. [all data]

Bendimerad and Bendiab, 2005
Bendimerad, N.; Bendiab, S.A.T., Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria, J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u . [all data]

Ferraz, Limberger, et al., 2005
Ferraz, A.B.F.; Limberger, R.P.; Bordignon, S.A.L.; von Poser, G.L.; Henriques, A.T., Essential oil composition of six Hypericum species from southern Brazil, Flavour Fragr. J., 2005, 20, 3, 335-339, https://doi.org/10.1002/ffj.1435 . [all data]

Limberger, Sobral, et al., 2005
Limberger, R.P.; Sobral, M.; Henriques, A.T., Intraspecific volatile oil variation in Myrceugenia cucullata (Myrtaceae), Biochem. Syst. Ecol., 2005, 33, 3, 287-293, https://doi.org/10.1016/j.bse.2004.10.002 . [all data]

Senatore, Apostolides Arnold, et al., 2005
Senatore, F.; Apostolides Arnold, N.; Bruno, M., Volatile components of Centaurea eryngioides Lam. and Centaurea liberica Trev. var. hermonis Boiss. Lam., two Asteraceae growing wild in Lebanon, Nat. Prod. Res., 2005, 19, 8, 749-754, https://doi.org/10.1080/14786410412331302136 . [all data]

Simoes-Pires C.A., Debenedetti S., et al., 2005
Simoes-Pires C.A.; Debenedetti S.; Spegazzini E.; Mentz L.A.; Matzenbacher N.I.; Limberger R.P.; Henriques A.T., Investigation of the essential oil from eight species of Baccharis belonging to sect. Caulopterae (Asteraceae, Astereae): a taxonomic approach, Plant Systematics and Evolution, 2005, 253, 1-4, 23-32, https://doi.org/10.1007/s00606-005-0296-6 . [all data]

Limberger, Sobral, et al., 2004
Limberger, R.P.; Sobral, M.; Henriques, A.T.; Menut, C.; Bessière, J.-M., Óleos voláteis de espécies de Myrcia nativas do rio grande do sul, Quim. Nova, 2004, 27, 6, 916-919, https://doi.org/10.1590/S0100-40422004000600015 . [all data]

Suyenaga, Apel, et al., 2004
Suyenaga, E.S.; Apel, M.A.; Chaves, C.G.; Zuanazzi, J.A.; Henriques, A.T., Essential oil composition of Heterothalamus psiadioides Less, Biochem. Syst. Ecol., 2004, 32, 1, 83-86, https://doi.org/10.1016/S0305-1978(03)00190-X . [all data]

Limberger, Simões-Pires, et al., 2003
Limberger, R.P.; Simões-Pires, C.A.; Sobral, M.; Menut, C.; Bessiere, J.-M.; Henriques, A.T., Essential oils of six Gomidesia spp. from southern Brazil, Flavour Fragr. J., 2003, 18, 2, 144-147, https://doi.org/10.1002/ffj.1122 . [all data]

Limberger, Simões-Pires, et al., 2002
Limberger, R.P.; Simões-Pires, C.; Sobral, M.; Menu, C.; Bessiere, J.-M.; Henriques, A.T., Essential oils from some Myrceugenia species (Myrtaceae), Flavour Fragr. J., 2002, 17, 5, 341-344, https://doi.org/10.1002/ffj.1113 . [all data]

Binder and Flath, 1989
Binder, R.G.; Flath, R.A., Volatile components of pineapple guava, J. Agric. Food Chem., 1989, 37, 3, 734-736, https://doi.org/10.1021/jf00087a034 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References