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2,6-Xylidine

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySPB-1100.1135.52Berezkin, Korolev, et al., 200030. m/0.25 mm/0.25 «mu»m, He
CapillaryDB-1100.1136.26Berezkin, Korolev, et al., 200030. m/0.25 mm/0.25 «mu»m, He
CapillaryZB-1100.1137.15Berezkin, Korolev, et al., 200030. m/0.25 mm/0.25 «mu»m, He
CapillaryBP-1100.1136.34Berezkin, Korolev, et al., 200030. m/0.25 mm/0.25 «mu»m, He
CapillarySE-30100.1137.93Malyukova, Berezkin, et al., 199730. m/0.25 mm/0.25 «mu»m, He
CapillarySE-30100.1143.41Malyukova, Berezkin, et al., 199730. m/0.25 mm/0.25 «mu»m, SF6
CapillarySE-33120.1179.Juvancz, Cserháti, et al., 199410. m/0.20 mm/0.15 «mu»m, H2
CapillaryOV-101110.1140.7Farkas, Sojak, et al., 198914. m/0.325 mm/0.305 «mu»m, H2

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryCarbowax 20M130.1940.Hedin, Thopson, et al., 1972N2; Column length: 15.24 m; Column diameter: 0.5 mm

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-11136.2Gautzsch and Zinn, 19968. K/min; Tstart: 35. C; Tend: 300. C
CapillaryDB-51167.Rostad and Pereira, 198630. m/0.26 mm/0.25 «mu»m, He, 50. C @ 4. min, 6. K/min, 300. C @ 20. min

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30120.1149.Berezkin, Korolev, et al., 199875. m/0.14 mm/0.30 «mu»m, He
CapillarySE-3090.1134.Berezkin and Korolev, 1985Helium; Column length: 25. m; Column diameter: 0.32 mm
CapillarySE-3090.1143.Berezkin and Korolev, 1985Helium; Column length: 25. m; Column diameter: 0.32 mm
CapillarySE-3090.1143.Berezkin and Korolev, 1985Helium; Column length: 25. m; Column diameter: 0.32 mm
CapillarySE-3090.1146.Berezkin and Korolev, 1985Helium; Column length: 25. m; Column diameter: 0.32 mm
CapillarySE-3090.1157.Berezkin and Korolev, 1985Helium; Column length: 25. m; Column diameter: 0.32 mm
CapillarySE-3090.1173.Berezkin and Korolev, 1985Helium; Column length: 25. m; Column diameter: 0.32 mm

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51168.19Kim, Kim, et al., 199330. m/0.25 mm/0.241 «mu»m, 60. C @ 2. min, 4. K/min; Tend: 160. C
CapillaryUltra-11131.Okumura, 199125. m/0.32 mm/0.25 «mu»m, He, 3. K/min; Tstart: 80. C; Tend: 260. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-11130.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified

Lee's RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5196.15Rostad and Pereira, 198630. m/0.26 mm/0.25 «mu»m, He, 50. C @ 4. min, 6. K/min, 300. C @ 20. min

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Berezkin, Korolev, et al., 2000
Berezkin, V.G.; Korolev, A.A.; Malyukova, I.V., A comparative analysis of retention values obtained on fused silica capillary columns from various manufacturers, Analusis, 2000, 28, 2, 132-135, https://doi.org/10.1051/analusis:2000105 . [all data]

Malyukova, Berezkin, et al., 1997
Malyukova, I.V.; Berezkin, V.G.; Kramers, K.; Jansen, H.G., Capillary chromatrography of hydrocarbons and their derivatives. Use of sulphur hexafluoride as the carrier gas, Pet. Chem. USSR (Engl. Transl.), 1997, 37, 3, 265-272. [all data]

Juvancz, Cserháti, et al., 1994
Juvancz, Z.; Cserháti, T.; Markides, K.E.; Bradshaw, J.S.; Lee, M.L., Characterization of some new polysiloxane stationary phases by principal component analysis, Chromatographia, 1994, 38, 3/4, 227-231, https://doi.org/10.1007/BF02290341 . [all data]

Farkas, Sojak, et al., 1989
Farkas, P.; Sojak, L.; Kovac, M.; Janak, J., Interface Adsorption and Reproducibility of Retention Indices in Glass Capillary Columns with Dimethylpolysiloxane Stationary Phases Cross-Linked by «gamma»-Irradiation, J. Chromatogr., 1989, 471, 251-261, https://doi.org/10.1016/S0021-9673(00)94173-6 . [all data]

Hedin, Thopson, et al., 1972
Hedin, P.A.; Thopson, A.C.; Gueldner, R.C.; Minyard, J.P., Volatile constituents of the boll weevil, J. Insect. Physiol., 1972, 18, 1, 79-86, https://doi.org/10.1016/0022-1910(72)90066-2 . [all data]

Gautzsch and Zinn, 1996
Gautzsch, R.; Zinn, P., Use of incremental models to estimate the retention indexes of aromatic compounds, Chromatographia, 1996, 43, 3/4, 163-176, https://doi.org/10.1007/BF02292946 . [all data]

Rostad and Pereira, 1986
Rostad, C.E.; Pereira, W.E., Kovats and Lee retention indices determined by gas chromatography/mass spectrometry for organic compounds of environmental interest, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 6, 328-334, https://doi.org/10.1002/jhrc.1240090603 . [all data]

Berezkin, Korolev, et al., 1998
Berezkin, V.G.; Korolev, A.A.; Malyukova, I.V., Dependence of the relative retention of compounds on the average pressure of helium as a carrier gas in capillary GLC, Russ. Chem. Bull. (Engl. Transl.), 1998, 47, 2, 307-309, https://doi.org/10.1007/BF02498955 . [all data]

Berezkin and Korolev, 1985
Berezkin, V.G.; Korolev, A.A., Investigation of the role of adsorption at the stationary phase interface in capillary columns with cross-linked phases, Chromatographia, 1985, 20, 8, 482-486, https://doi.org/10.1007/BF02344790 . [all data]

Kim, Kim, et al., 1993
Kim, K.-R.; Kim, J.-H.; Park, H.-K.; Oh, C.-H., Dual capillary column system for the qualitative gas chromatography: 2. Comparison between splitless and on-column injection modes, Bull. Korean Chem. Soc., 1993, 14, 2, 250-255. [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]


Notes

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