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Nonane, 2-methyl-

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase SqualaneOV-101OV-101OV-101Squalane
Column length (m)     10.
Carrier gas     He
Substrate     Chromosorb P.A.W.D.M.C.S.
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 100.40.60.80.100.
I 964.962.962.962.976.
ReferenceHeinzen, Soares, et al., 1999Laub and Purnell, 1988Laub and Purnell, 1988Laub and Purnell, 1988Chelghoum, Haddad, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 10.10.10.10.10.
Carrier gas HeHeHeHeHe
Substrate Chromosorb P.A.W.D.M.C.S.Chromosorb P.A.W.D.M.C.S.Chromosorb P.A.W.D.M.C.S.Chromosorb P.A.W.D.M.C.S.Chromosorb P.A.W.D.M.C.S.
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 110.120.130.140.150.
I 966.964.964.972.972.
ReferenceChelghoum, Haddad, et al., 1985Chelghoum, Haddad, et al., 1985Chelghoum, Haddad, et al., 1985Chelghoum, Haddad, et al., 1985Chelghoum, Haddad, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-1SqualaneVacuum Grease Oil (VM-4)
Column length (m) 60.60.150. 150.
Carrier gas   He N2
Substrate      
Column diameter (mm) 0.2640.2590.50 0.25
Phase thickness (mum)  1.   
Temperature (C) 60.60.60.60.95.
I 965.2965.1962.963.9964.7
ReferenceLubeck and Sutton, 1983Lubeck and Sutton, 1983Nijs and Jacobs, 1981Chretien and Dubois, 1976Sultanov and Arustamova, 1975
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedCapillary
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m) 6.16.16.16.16.1
Carrier gas N2N2N2N2H2
Substrate Chrom WChrom WChrom WChrom W 
Column diameter (mm)     3.18
Phase thickness (mum)      
Temperature (C) 110.120.130.140.130.
I 965.964.966.968.964.
ReferenceMitra, Mohan, et al., 1974Mitra, Mohan, et al., 1974Mitra, Mohan, et al., 1974Mitra, Mohan, et al., 1974Mitra, Mohan, et al., 1974, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30SE-30SE-30Squalane
Column length (m) 6.16.16.16.150.
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm) 3.183.183.183.180.2
Phase thickness (mum)      
Temperature (C) 140.150.160.170.100.
I 966.965.967.968.963.
ReferenceMitra, Mohan, et al., 1974, 2Mitra, Mohan, et al., 1974, 2Mitra, Mohan, et al., 1974, 2Mitra, Mohan, et al., 1974, 2Mitra, Mohan, et al., 1974, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 100.100.3.91.4100.
Carrier gas   N2N2Ar
Substrate   Chromosorb W  
Column diameter (mm) 0.250.25 0.25 
Phase thickness (mum)      
Temperature (C) 80.80.50.60.80.
I 964.43964.43963.8964.964.
ReferenceSchomburg and Dielmann, 1973Schomburg and Dielmann, 1973, 2Takács, Szita, et al., 1971Matukuma, 1969Schomburg, 1967
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Heinzen, Soares, et al., 1999
Heinzen, V.E.F.; Soares, M.F.; Yunes, R.A., Semi-empirical topological method for the prediction of the chromatographic retention of cis- and trans-alkene isomers and alkanes, J. Chromatogr. A, 1999, 849, 2, 495-506, https://doi.org/10.1016/S0021-9673(99)00530-0 . [all data]

Laub and Purnell, 1988
Laub, R.J.; Purnell, J.H., Specific retention volumes, retention indices, and family-plot regressions of aliphatic, alicyclic, and aromatic hydrocarbon solutes with OV-101 poly (dimethylsiloxane) stationary phase, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1988, 11, 9, 649-660, https://doi.org/10.1002/jhrc.1240110908 . [all data]

Chelghoum, Haddad, et al., 1985
Chelghoum, C.; Haddad, Y.; Abdeddaim, K.; Guermouche, M.H., Indices de retention et structure moléculaire des iso-decanes, Rev. Roum. Chim., 1985, 30, 7, 565-569. [all data]

Lubeck and Sutton, 1983
Lubeck, A.J.; Sutton, DL., Kovats retention indices of selected hydrocarbons through C10 on bonded phase fused silica capillaries, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1983, 6, 6, 328-332, https://doi.org/10.1002/jhrc.1240060612 . [all data]

Nijs and Jacobs, 1981
Nijs, H.H.; Jacobs, P.A., On-Line Single Run Analysis of Effluents from a Fischer-Tropsch Reactor, J. Chromatogr. Sci., 1981, 19, 1, 40-45, https://doi.org/10.1093/chromsci/19.1.40 . [all data]

Chretien and Dubois, 1976
Chretien, J.R.; Dubois, J.-E., New Perspectives in the Prediction of Kovats Indices, J. Chromatogr., 1976, 126, 171-189, https://doi.org/10.1016/S0021-9673(01)84071-1 . [all data]

Sultanov and Arustamova, 1975
Sultanov, N.T.; Arustamova, L.G., Determination of the boiling points of C10 isoalkanes in an n-decane isomerizate from gas chromatographic retention indices, J. Chromatogr., 1975, 115, 2, 553-558, https://doi.org/10.1016/S0021-9673(01)98959-9 . [all data]

Mitra, Mohan, et al., 1974
Mitra, G.D.; Mohan, G.; Sinha, A., Advances in the utilization of the retention index system for characterizing hydrocarbons in complex mixtures by gas chromatography, J. Chromatogr., 1974, 99, 215-230, https://doi.org/10.1016/S0021-9673(00)90857-4 . [all data]

Mitra, Mohan, et al., 1974, 2
Mitra, G.D.; Mohan, G.; Sinha, A., Gas chromatographic analysis of complex hydrocarbon mixtures, J. Chromatogr. A, 1974, 91, 633-648, https://doi.org/10.1016/S0021-9673(01)97944-0 . [all data]

Schomburg and Dielmann, 1973
Schomburg, G.; Dielmann, G., Identification by means of retention parameters, J. Chromatogr. Sci., 1973, 11, 3, 151-159, https://doi.org/10.1093/chromsci/11.3.151 . [all data]

Schomburg and Dielmann, 1973, 2
Schomburg, G.; Dielmann, G., Use of retention increments for identification and correlation of saturated and unsaturated cyclopropane hydrocarbons by means of Kovats indices, Anal. Chem., 1973, 45, 9, 1647-1658, https://doi.org/10.1021/ac60331a021 . [all data]

Takács, Szita, et al., 1971
Takács, J.; Szita, C.; Tarján, G., Contribution to the theory of the retention index system. III. Retention index and molecular structure. Calculation of retention indices of paraffin hydrocarbons on the basis of their molecular structure, J. Chromatogr., 1971, 56, 1-12, https://doi.org/10.1016/S0021-9673(00)97771-9 . [all data]

Matukuma, 1969
Matukuma, A., Retention indices of alkanes through C10 and alkenes through C8 and relation between boiling points and retention data, Gas Chromatogr., Int. Symp. Anal. Instrum. Div Instrum Soc. Amer., 1969, 7, 55-75. [all data]

Schomburg, 1967
Schomburg, G., Struktur und Retentionsverhalten von Offenkettigen und Cyclischen Kohlenwasserstoffen und Deren Einfacher Substitutionsprodukte, Anal. Chim. Acta., 1967, 38, 45-64, https://doi.org/10.1016/S0003-2670(01)80560-2 . [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References