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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryPackedCapillaryCapillary
Active phase OV-1OV-1SE-30DB-5SE-54
Column length (m) 25.25.3.0530.25.
Carrier gas   HeHeH2
Substrate   Supelcoport and Chromosorb  
Column diameter (mm) 0.20.2 0.260.31
Phase thickness (μm) 0.330.33 0.250.17
Tstart (C) 100.100.40.50.35.
Tend (C) 180.180.250.300. 
Heat rate (K/min) 5.5.10.6.2.
Initial hold (min)   4.4. 
Final hold (min)   60.20. 
I 1801.11820.51810.1851.1806.
ReferenceZhang, Shen, et al., 2000Zhang, Shen, et al., 2000Peng, Ding, et al., 1988Rostad and Pereira, 1986Weber, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SE-54SE-52SE-52
Column length (m) 25.33.350.
Carrier gas H2HeN2
Substrate    
Column diameter (mm) 0.310.50 
Phase thickness (μm) 0.17  
Tstart (C) 35.50.100.
Tend (C)  320.300.
Heat rate (K/min) 2.6.2.5
Initial hold (min)  5. 
Final hold (min)    
I 1836.1766.1838.
ReferenceWeber, 1986Beernaert, 1979Cantuti, Cartoni, et al., 1965
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zhang, Shen, et al., 2000
Zhang, M.-J.; Shen, S.-D.; Chen, S.-Y.; Sun, Y.-H., Analysis of heavy oil fractions in high-temperature coal tar by capillary gas chromatography/fourier transform infrared spectrometry, Chin. J. Chromatogr., 2000, 18, 3, 241-246. [all data]

Peng, Ding, et al., 1988
Peng, C.T.; Ding, S.F.; Hua, R.L.; Yang, Z.C., Prediction of Retention Indexes I. Structure-Retention Index Relationship on Apolar Columns, J. Chromatogr., 1988, 436, 137-172, https://doi.org/10.1016/S0021-9673(00)94575-8 . [all data]

Rostad and Pereira, 1986
Rostad, C.E.; Pereira, W.E., Kovats and Lee retention indices determined by gas chromatography/mass spectrometry for organic compounds of environmental interest, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 6, 328-334, https://doi.org/10.1002/jhrc.1240090603 . [all data]

Weber, 1986
Weber, L., Utilization of the Sadtler standard RI system in micropollution analyses, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 8, 446-451, https://doi.org/10.1002/jhrc.1240090806 . [all data]

Beernaert, 1979
Beernaert, H., Gas Chromatographic Analysis of Polyclylic Aromatic Hydrocarbons, J. Chromatogr., 1979, 173, 1, 109-118, https://doi.org/10.1016/S0021-9673(01)80450-7 . [all data]

Cantuti, Cartoni, et al., 1965
Cantuti, V.; Cartoni, G.P.; Liberti, A.; Torri, A.G., Improved evaluation of polynuclear hydrocarbons in atmospheric dust by gas chromatography, J. Chromatogr., 1965, 17, 60-65, https://doi.org/10.1016/S0021-9673(00)99836-4 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References