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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.40.40.40.40.
Tend (C) 300.310.310.310.310.
Heat rate (K/min) 4.4.4.2.4.
Initial hold (min)   5.  
Final hold (min)      
I 1583.41579.51578.91565.21579.5
ReferenceZeng, Zhao, et al., 2007Song, Lai, et al., 2003Song, Lai, et al., 2003Song, Lai, et al., 2003Song, Lai, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-1OV-1HP-5MSDB-5
Column length (m) 30.25.25.30.30.
Carrier gas He   He
Substrate      
Column diameter (mm) 0.250.20.20.250.25
Phase thickness (mum) 0.250.330.330.250.25
Tstart (C) 40.100.100.50.40.
Tend (C) 310.180.180.300.310.
Heat rate (K/min) 6.5.5.10.2.
Initial hold (min)      
Final hold (min)      
I 1587.91590.51611.01595.1565.2
ReferenceSong, Lai, et al., 2003Zhang, Shen, et al., 2000Zhang, Shen, et al., 2000Nahir, 1999Lai and Song, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5SP-2100
Column length (m) 30.30.30.30. 
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 40.40.40.40.170.
Tend (C) 310.310.310.310. 
Heat rate (K/min) 4.6.4.4.2.
Initial hold (min)    5. 
Final hold (min)      
I 1579.51587.91579.51578.91574.59
ReferenceLai and Song, 1995Lai and Song, 1995Lai and Song, 1995Lai and Song, 1995Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SP-2100SP-2100SP-2100SP-2100SP-2100
Column length (m)      
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Tstart (C) 170.170.170.170.170.
Tend (C)      
Heat rate (K/min) 4.6.2.4.6.
Initial hold (min)      
Final hold (min)      
I 1577.831580.721593.301589.391595.90
ReferencePodmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5SE-30SE-30SE-52
Column length (m)  30.25.25.33.3
Carrier gas H2HeN2N2He
Substrate      
Column diameter (mm)  0.260.330.330.50
Phase thickness (mum)  0.25   
Tstart (C) 170.50.100.140.50.
Tend (C)  300.320.320.320.
Heat rate (K/min) 4.6.10.6.6.
Initial hold (min)  4.  5.
Final hold (min)  20.   
I 1590.561594.1583.1587.1555.
ReferencePodmaniczky, Szepesy, et al., 1986Rostad and Pereira, 1986Korhonen and Lind, 1985Korhonen and Lind, 1985Beernaert, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52
Column length (m) 12.12.65.
Carrier gas HeHeN2
Substrate    
Column diameter (mm) 0.30.280.3
Phase thickness (mum) 0.340.17 
Tstart (C) 50.50.100.
Tend (C) 250.250.300.
Heat rate (K/min) 2.2.1.8
Initial hold (min)    
Final hold (min)    
I 1555.871549.281555.
ReferenceLee, Vassilaros, et al., 1979Lee, Vassilaros, et al., 1979Carugno and Rossi, 1967
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zeng, Zhao, et al., 2007
Zeng, Y.-X.; Zhao, C.-X.; Liang, Y.-Z.; Yang, H.; Fang, H.-Z.; Yi, L.-Z.; Zeng, Z.-D., Comparative analysis of volatile components from Clematis species growing in China, Anal. Chim. Acta., 2007, 595, 1-2, 328-339, https://doi.org/10.1016/j.aca.2006.12.022 . [all data]

Song, Lai, et al., 2003
Song, C.; Lai, W.-C.; Madhusudan Reddy, K.; Wei, B., Chapter 7. Temperature-programmed retention indices for GC and GC-MS of hydrocarbon fuels and simulated distillation GC of heavy oils in Analytical advances for hydrocarbon research, Hsu,C.S., ed(s)., Kluwer Academic/Plenum Publishers, New York, 2003, 147-193. [all data]

Zhang, Shen, et al., 2000
Zhang, M.-J.; Shen, S.-D.; Chen, S.-Y.; Sun, Y.-H., Analysis of heavy oil fractions in high-temperature coal tar by capillary gas chromatography/fourier transform infrared spectrometry, Chin. J. Chromatogr., 2000, 18, 3, 241-246. [all data]

Nahir, 1999
Nahir, T.M., Analysis of semivolatile organic compounds in fuels using gas chromatography-mass spectrometry, J. Chem. Educ., 1999, 76, 12, 1695-1696, https://doi.org/10.1021/ed076p1695 . [all data]

Lai and Song, 1995
Lai, W.-C.; Song, C., Temperature-programmed retention indices for g.c. and g.c.-m.s. analysis of coal- and petroleum-derived liquid fuels, Fuel, 1995, 74, 10, 1436-1451, https://doi.org/10.1016/0016-2361(95)00108-H . [all data]

Podmaniczky, Szepesy, et al., 1986
Podmaniczky, L.; Szepesy, L.; Lakszner, K.; Schomburg, G., Determination of Retention Indices in LPTGC, Chromatographia, 1986, 21, 7, 387-391, https://doi.org/10.1007/BF02346137 . [all data]

Rostad and Pereira, 1986
Rostad, C.E.; Pereira, W.E., Kovats and Lee retention indices determined by gas chromatography/mass spectrometry for organic compounds of environmental interest, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 6, 328-334, https://doi.org/10.1002/jhrc.1240090603 . [all data]

Korhonen and Lind, 1985
Korhonen, I.O.O.; Lind, M.A., Gas-liquid chromatographic analyses. XXXIV. Separation and retention indices with retention increments of some nitrated polynuclear aromatic hydrocarbons on a low-polarity (SE-30) capillary column, J. Chromatogr., 1985, 322, 71-81, https://doi.org/10.1016/S0021-9673(01)97660-5 . [all data]

Beernaert, 1979
Beernaert, H., Gas Chromatographic Analysis of Polyclylic Aromatic Hydrocarbons, J. Chromatogr., 1979, 173, 1, 109-118, https://doi.org/10.1016/S0021-9673(01)80450-7 . [all data]

Lee, Vassilaros, et al., 1979
Lee, M.L.; Vassilaros, D.L.; White, C.M.; Novotny, M., Retention Indices for Programmed-Temperature Capillary-Column Gas Chromatography of Polycyclic Aromatic Hydrocarbons, Anal. Chem., 1979, 51, 6, 768-773, https://doi.org/10.1021/ac50042a043 . [all data]

Carugno and Rossi, 1967
Carugno, N.; Rossi, S., Evaluation of polynuclear hydrocarbons in cigarette smoke by glass capillary columns, J. Gas Chromatogr., 1967, 5, 2, 103-106, https://doi.org/10.1093/chromsci/5.2.103 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References