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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5C103H208C103H208HP-5
Column length (m) 30.30.  30.
Carrier gas Helium H2H2 
Substrate      
Column diameter (mm) 0.250.25  0.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.40.80.100.50.
Tend (C) 290.280.275.275.310.
Heat rate (K/min) 5.5.5.4.5.
Initial hold (min)     2.
Final hold (min) 10.10.   
I 1587.1598.1593.1593.1580.
ReferenceRadulovic, Blagojevic, et al., 2010Grung, Lichtenthaler, et al., 2007Dumitrescu, Buda, et al., 2000Dumitrescu, Buda, et al., 2000Miao and Wu, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas      
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.50.50.50.
Tend (C) 310.310.310.310.310.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min) 2.2.2.2.2.
Final hold (min)      
I 1581.1583.1583.1583.1584.
ReferenceMiao and Wu, 1999Miao and Wu, 1999Miao and Wu, 1999Miao and Wu, 1999Miao and Wu, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5Ultra-1DB-5Ultra-1
Column length (m) 30.30.50.30.25.
Carrier gas   H2H2He
Substrate      
Column diameter (mm) 0.320.320.20.320.32
Phase thickness (mum) 0.250.250.330.250.25
Tstart (C) 50.50.60.80.80.
Tend (C) 310.310.300.270.260.
Heat rate (K/min) 5.5.3.4.3.
Initial hold (min) 2.2. 2. 
Final hold (min)   35.5. 
I 1591.1592.1558.1559.1531.
ReferenceMiao and Wu, 1999Miao and Wu, 1999Elizalde-González, Hutfliess, et al., 1996Andersson and Weis, 1994Okumura, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-54
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum)  
Tstart (C) 50.
Tend (C) 250.
Heat rate (K/min) 8.
Initial hold (min) 2.
Final hold (min) 12.
I 1572.
ReferenceHarland, Cumming, et al., 1986
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

Grung, Lichtenthaler, et al., 2007
Grung, M.; Lichtenthaler, R.; Ahel, M.; Tollefsen, K.-E.; Langford, K.; Thomas, K.V., Effects-directed analysis of organic toxicants in wastewater effluent from Zagreb, Croatia, Chemosphere, 2007, 67, 1, 108-120, https://doi.org/10.1016/j.chemosphere.2006.09.021 . [all data]

Dumitrescu, Buda, et al., 2000
Dumitrescu, V.; Buda, W.; Medvedovici, A., Evaluation of new stationary phases for capillary gas chromatography, Rev. Roum. Chim., 2000, 45, 4, 313-318. [all data]

Miao and Wu, 1999
Miao, X.; Wu, F., Study on retention behaviors of polycyclic aromatic hydrocarbons by gas chromatography in different operation models, J. Instrumental Anal., 1999, 15, 4, 288-292. [all data]

Elizalde-González, Hutfliess, et al., 1996
Elizalde-González, M.P.; Hutfliess, M.; Hedden, K., Retention index system, adsorption characteristics, and sructure correlations of polycyclic aromatic hydrocarbons in fuels, J. Hi. Res. Chromatogr., 1996, 19, 6, 345-352, https://doi.org/10.1002/jhrc.1240190608 . [all data]

Andersson and Weis, 1994
Andersson, J.T.; Weis, U., Gas Chromatographic Determination of Polycyclic Aromatic Compounds with Fluorinated Analogues as Internal Standards, J. Chromatogr. A, 1994, 659, 1, 151-161, https://doi.org/10.1016/0021-9673(94)85017-8 . [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]

Harland, Cumming, et al., 1986
Harland, B.J.; Cumming, R.I.; Gillings, E., The Kovats indexes of some organic micropollutants on an SE54 capillary column, EUR, I Org. Micropollut. Aquat. Environ., 1986, EUR 10388, 123-127. [all data]


Notes

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