10H-Phenothiazine-10-propanamine, 2-methoxy-N,N,β-trimethyl-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryPackedPackedPackedPacked
Active phase CBP-1Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m) 12.    
Carrier gas N2    
Substrate      
Column diameter (mm) 0.53    
Phase thickness (μm)      
Tstart (C) 120.120.120.120.120.
Tend (C) 250.290.290.290.290.
Heat rate (K/min) 6.7.7.7.7.
Initial hold (min)  4.4.4.4.
Final hold (min)  10.10.10.10.
I 2512.2510.2536.2535.2535.
ReferenceOyama, Sano, et al., 1987Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Tstart (C) 120.120.120.120.120.
Tend (C) 290.290.290.290.290.
Heat rate (K/min) 7.7.7.7.7.
Initial hold (min) 4.4.4.4.4.
Final hold (min) 10.10.10.10.10.
I 2538.2539.2540.2540.2540.
ReferenceBogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Tstart (C) 120.120.120.120.120.
Tend (C) 290.290.290.290.290.
Heat rate (K/min) 7.7.7.7.7.
Initial hold (min) 4.4.4.4.4.
Final hold (min) 10.10.10.10.10.
I 2540.2542.2542.2542.2542.
ReferenceBogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Tstart (C) 120.120.120.120.120.
Tend (C) 290.290.290.290.290.
Heat rate (K/min) 7.7.7.7.7.
Initial hold (min) 4.4.4.4.4.
Final hold (min) 10.10.10.10.10.
I 2540.2540.2542.2542.2543.
ReferenceBogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Tstart (C) 120.120.120.120.120.
Tend (C) 290.290.290.290.290.
Heat rate (K/min) 7.7.7.7.7.
Initial hold (min) 4.4.4.4.4.
Final hold (min) 10.10.10.10.10.
I 2545.2545.2545.2547.2550.
ReferenceBogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Tstart (C) 120.120.120.120.120.
Tend (C) 290.290.290.290.290.
Heat rate (K/min) 7.7.7.7.7.
Initial hold (min) 4.4.4.4.4.
Final hold (min) 10.10.10.10.10.
I 2530.2530.2532.2535.2535.
ReferenceBogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Methyl SiliconeMethyl SiliconeMethyl SiliconeMethyl SiliconeMethyl Silicone
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Tstart (C) 120.120.120.120.120.
Tend (C) 290.290.290.290.290.
Heat rate (K/min) 7.7.7.7.7.
Initial hold (min) 4.4.4.4.4.
Final hold (min) 10.10.10.10.10.
I 2535.2537.2537.2537.2537.
ReferenceBogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985Bogusz, Wijsbeek, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedCapillaryCapillaryCapillaryPacked
Active phase Methyl SiliconeDB-1DB-1SE-30SE-30
Column length (m)  15.15.15.1.8
Carrier gas  HeHeHeN2
Substrate     Chromosorb W
Column diameter (mm)  0.320.250.25 
Phase thickness (μm)  0.250.250.25 
Tstart (C) 120.120.120.100.130.
Tend (C) 290.280.280.295.290.
Heat rate (K/min) 7.8.8.5.8.
Initial hold (min) 4.   2.
Final hold (min) 10.5.5. 8.
I 2540.2511.2511.2490.2515.
ReferenceBogusz, Wijsbeek, et al., 1985Perrigo, Peel, et al., 1985Perrigo, Ballantyne, et al., 1984Anderson and Stafford, 1983Perrigo and Peel, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Oyama, Sano, et al., 1987
Oyama, N.; Sano, T.; Syoyama, M.; Maeda, K., Studies on systematic analysis of poisonous compounds in forensic chemistry. II. Application of capillary column gas chromatography to substance identification by means of retention indices, Eisei Kagaku, 1987, 33, 5, 342-348, https://doi.org/10.1248/jhs1956.33.342 . [all data]

Bogusz, Wijsbeek, et al., 1985
Bogusz, M.; Wijsbeek, J.; Franke, J.P.; de Zeeuw, R.A.; Gierz, J., Impact of biological matrix, drug concentration, and method of isolation on detectability and variability of retention index values in gas chromatography, J. Anal. Toxicol., 1985, 9, 2, 49-54, https://doi.org/10.1093/jat/9.2.49 . [all data]

Perrigo, Peel, et al., 1985
Perrigo, B.J.; Peel, H.W.; Ballantyne, D.J., Use of Dual-Column Fused-Silica Capillary Gas Chromatography in Combination with Detector Response Factors for Analytical Toxicology., J. Chromatogr., 1985, 341, 81-88, https://doi.org/10.1016/S0378-4347(00)84011-6 . [all data]

Perrigo, Ballantyne, et al., 1984
Perrigo, B.J.; Ballantyne, D.J.; Peel, H.W., Condierations in developing a data base for drugs on a DBI capillary column, J. Can. Soc. Forensic Sci., 1984, 17, 2, 41-49, https://doi.org/10.1080/00085030.1984.10757360 . [all data]

Anderson and Stafford, 1983
Anderson, W.H.; Stafford, D.T., Applications of capillary gas chromatography in routine toxicological analyses, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1983, 6, 5, 247-254, https://doi.org/10.1002/jhrc.1240060506 . [all data]

Perrigo and Peel, 1981
Perrigo, B.J.; Peel, H.W., The use of retention indices and temperature-programmed gas chromatography in analytical toxicology, J. Chromatogr. Sci., 1981, 19, 5, 219-226, https://doi.org/10.1093/chromsci/19.5.219 . [all data]


Notes

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