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Diethyl Phthalate

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5DB-1DB-55 % Phenyl methyl siloxaneDB-1
Column length (m) 25.30.30.25.30.
Carrier gas He He  
Substrate      
Column diameter (mm) 0.220.20.250.310.25
Phase thickness (mum) 0.250.25 0.31 
Tstart (C) 50.50.50.50.50.
Tend (C) 300.300.250.250.300.
Heat rate (K/min) 5.5.4.5.2.
Initial hold (min) 5.2. 1. 
Final hold (min)  5. 10. 
I 1605.1543.1585.1592.1547.5
ReferenceDickschat, Wenzel, et al., 2004Johnson, Urso, et al., 1997Gómez, Ledbetter, et al., 1993Guisto, Smith, et al., 1993Chang, Sheng, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedCapillaryCapillary
Active phase DB-1SE-30SE-30SP-2100SP-2100
Column length (m) 30.2.2.  
Carrier gas    H2H2
Substrate  Chromosorb QChromosorb Q  
Column diameter (mm) 0.25    
Phase thickness (mum)      
Tstart (C) 50.100.100.170.170.
Tend (C) 300.    
Heat rate (K/min) 2.10.10.2.4.
Initial hold (min)      
Final hold (min)      
I 1550.91558.1584.1562.221563.47
ReferenceChang, Sheng, et al., 1989Helaimia and Messadi, 1989Helaimia and Messadi, 1989Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SP-2100SP-2100SP-2100SP-2100CP Sil 5 CB
Column length (m)      
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Tstart (C) 170.170.170.170.170.
Tend (C)      
Heat rate (K/min) 6.2.4.6.4.
Initial hold (min)      
Final hold (min)      
I 1561.871570.771572.651569.251563.84
ReferencePodmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPacked
Active phase CP Sil 5 CBCP Sil 5 CBSE-30
Column length (m) 26.26. 
Carrier gas   N2
Substrate   Chromosorb Q
Column diameter (mm) 0.320.32 
Phase thickness (mum) 1.251.25 
Tstart (C) 100.100.100.
Tend (C) 250.250.340.
Heat rate (K/min) 10.10.10.
Initial hold (min)    
Final hold (min)    
I 1567.1568.1558.
ReferenceHalket and Schulten, 1985Halket and Schulten, 1985Messadi and Vergnaud, 1979
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Dickschat, Wenzel, et al., 2004
Dickschat, J.S.; Wenzel, S.C.; Bode, H.B.; Muller, R.; Schulz, S., Biosynthesis of Volatiles by the Myxobacterium Myxococcus xanthus, ChemBioChem, 2004, 5, 6, 778-787, https://doi.org/10.1002/cbic.200300813 . [all data]

Johnson, Urso, et al., 1997
Johnson, C.I.; Urso, A.; Geleta, L., Broad spectrum analysis of municipal and industrial effluents discharged into the Peace, Athabasca and Slave river basins: characterization of effluent samples, 1994 - Volume 1 of 2, Northern River Basins Study Project Report No. 121, Norther River Basins Study, Edmonton, Alberta, 1997, 27. [all data]

Gómez, Ledbetter, et al., 1993
Gómez, E.; Ledbetter, C.A.; Hartsell, P.L., Volatile compounds in apricot, plum, and their interspecific hybrids, J. Agric. Food Chem., 1993, 41, 10, 1669-1676, https://doi.org/10.1021/jf00034a029 . [all data]

Guisto, Smith, et al., 1993
Guisto, R.; Smith, S.R.; Stuart, J.D., Gas chromatographic retention indices, mass, and infrared spectra of industrially important adipate esters, J. Chromatogr. Sci., 1993, 31, 6, 225-230, https://doi.org/10.1093/chromsci/31.6.225 . [all data]

Chang, Sheng, et al., 1989
Chang, L.P.; Sheng, L.S.; Yang, M.Z.; An, D.K., Retention index of essential oil in temperature-programmed capillary column gas chromatography, Acta Pharm. Sin., 1989, 24, 11, 847-852. [all data]

Helaimia and Messadi, 1989
Helaimia, F.; Messadi, D., Determination of linear programmed temperature gas chromatography retention indices for some plasticizers, C.R. Acad. Sci. Ser. 2:, 1989, 309, 37-42. [all data]

Podmaniczky, Szepesy, et al., 1986
Podmaniczky, L.; Szepesy, L.; Lakszner, K.; Schomburg, G., Determination of Retention Indices in LPTGC, Chromatographia, 1986, 21, 7, 387-391, https://doi.org/10.1007/BF02346137 . [all data]

Halket and Schulten, 1985
Halket, J.M.; Schulten, H.-R., Thick-film capillary column gas chromatography-field ionization mass spectrometry: A complementary technique for the rapid analysis of volatiles, J. Chromatogr., 1985, 322, 200-205, https://doi.org/10.1016/S0021-9673(01)97672-1 . [all data]

Messadi and Vergnaud, 1979
Messadi, D.; Vergnaud, J.-M., Quick identification and analysis of plasticizers in PVC by programmed-temperature gas chromatography using the best stationary phases, J. Appl. Polym. Sci., 1979, 24, 5, 1215-1225, https://doi.org/10.1002/app.1979.070240507 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References