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Diethyl Phthalate

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Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSVF-5MSDB-5HP-5DB-1
Column length (m) 30.30.30.60.60.
Carrier gas Helium HeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.40.60.30.35.
Tend (C) 300.250.280.260.230.
Heat rate (K/min) 3.7.5.2.2.
Initial hold (min) 5. 0.52.4.
Final hold (min) 15. 2.28.25.
I 1594.1559.1546.1602.31545.
ReferenceKotowska, Zalikowski, et al., 2012Ghiasvand, Setkova, et al., 2007Ozel, Gogus, et al., 2006Leffingwell and Alford, 2005Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedPacked
Active phase DB-1DB-1DB-1SE-30SE-30
Column length (m) 60.60.60.2.2.
Carrier gas HeHeHeNitrogenNitrogen
Substrate    Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)
Column diameter (mm) 0.320.320.32  
Phase thickness (mum) 0.250.250.25  
Tstart (C) 35.35.35.100.100.
Tend (C) 230.230.230.290.290.
Heat rate (K/min) 2.2.2.8.8.
Initial hold (min) 4.4.4.  
Final hold (min) 25.25.25.  
I 1546.1547.1550.1578.1578.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m) 2.2.2.2.2.
Carrier gas NitrogenNitrogenNitrogenNitrogenNitrogen
Substrate Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)Chromosorb Q (60-80 mesh)
Column diameter (mm)      
Phase thickness (mum)      
Tstart (C) 100.100.100.100.100.
Tend (C) 290.290.290.290.290.
Heat rate (K/min) 8.8.8.8.8.
Initial hold (min)      
Final hold (min)      
I 1578.1578.1578.1579.1582.
ReferenceLourici, Souici, et al., 1999Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999Lourici, Souici, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSUltra-1DB-1DB-1SE-54
Column length (m) 30.25.60.60.25.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (mum)  0.250.250.25 
Tstart (C) 50.80.50.50.50.
Tend (C) 250.260.240.240.250.
Heat rate (K/min) 4.3.3.3.8.
Initial hold (min)     2.
Final hold (min)     12.
I 1585.1541.1556.1563.1597.
ReferenceGomez and Ledbetter, 1994Okumura, 1991Shiota, 1991Shiota, 1991Harland, Cumming, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-1DB-1SE-30
Column length (m) 50.60.50.
Carrier gas   He
Substrate    
Column diameter (mm) 0.320.320.5
Phase thickness (mum)    
Tstart (C) 50.50.40.
Tend (C) 250.250.170.
Heat rate (K/min) 3.4.3.
Initial hold (min)  0.13.
Final hold (min)  5. 
I 1551.1547.1559.
ReferenceHabu, Flath, et al., 1985Flath, Mon, et al., 1983Heydanek and McGorrin, 1981
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kotowska, Zalikowski, et al., 2012
Kotowska, U.; Zalikowski, M.; Isidorov, V.A., HS-SPME/GC-MS analysis of volatile and semi-volatile organic compounds emitted from municipal sewage sludge, Environ. Monit. Asses., 2012, 184, 5, 2893-2907, https://doi.org/10.1007/s10661-011-2158-8 . [all data]

Ghiasvand, Setkova, et al., 2007
Ghiasvand, A.R.; Setkova, L.; Pawliszyn, J., Determination of flavour profile in Iranian fragrant rice samples using cold-fibre SPME-GC-TOF-MS, Flavour Fragr. J., 2007, 22, 5, 377-391, https://doi.org/10.1002/ffj.1809 . [all data]

Ozel, Gogus, et al., 2006
Ozel, M.Z.; Gogus, F.; Lewis, A.C., Comparison of direct thermal desorption with water distillation and superheated water extraction for the analysis of volatile components of Rosa damascena Mill. using GCxGC-TOF/MS, Anal. Chim. Acta., 2006, 566, 2, 172-177, https://doi.org/10.1016/j.aca.2006.03.014 . [all data]

Leffingwell and Alford, 2005
Leffingwell, J.C.; Alford, E.D., Volatile constituents of Perique tobacco, Electron. J. Environ. Agric. Food Chem., 2005, 4, 2, 899-915. [all data]

Park, Lee, et al., 2004
Park, B.-S.; Lee, K.-G.; Takeoka, G.R., Comparison of three sample preparation methods on the recovery of volatiles from taheebo (Tabebuia impetiginosa Martius ex DC), Flavour Fragr. J., 2004, 19, 4, 287-292, https://doi.org/10.1002/ffj.1345 . [all data]

Lourici, Souici, et al., 1999
Lourici, L.; Souici, M.-L.; Rebbani, N.; Messadi, D., Independent of local properties mathematical models for the calculation of retention indices in programmed temperature gas chromatography, Analusis, 1999, 27, 3, 249-254, https://doi.org/10.1051/analusis:1999114 . [all data]

Gomez and Ledbetter, 1994
Gomez, E.; Ledbetter, C.A., Comparative study of the aromatic profiles of two different plum species: Prunus salicina Lindl and Prunus simonii L., J. Sci. Food Agric., 1994, 65, 1, 111-115, https://doi.org/10.1002/jsfa.2740650116 . [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]

Shiota, 1991
Shiota, H., Volatile components of pawpaw fruit (Asimina triloba Dunal.), J. Agric. Food Chem., 1991, 39, 9, 1631-1635, https://doi.org/10.1021/jf00009a019 . [all data]

Harland, Cumming, et al., 1986
Harland, B.J.; Cumming, R.I.; Gillings, E., The Kovats indexes of some organic micropollutants on an SE54 capillary column, EUR, I Org. Micropollut. Aquat. Environ., 1986, EUR 10388, 123-127. [all data]

Habu, Flath, et al., 1985
Habu, T.; Flath, R.A.; Mon, T.R.; Morton, J.F., Volatile components of Rooibos tea (Aspalathus linearis), J. Agric. Food Chem., 1985, 33, 2, 249-254, https://doi.org/10.1021/jf00062a024 . [all data]

Flath, Mon, et al., 1983
Flath, R.A.; Mon, T.R.; Lorenz, G.; Whitten, C.J.; Mackley, J.W., Volatile components of Acacia sp. blossoms, J. Agric. Food Chem., 1983, 31, 6, 1167-1170, https://doi.org/10.1021/jf00120a008 . [all data]

Heydanek and McGorrin, 1981
Heydanek, M.G.; McGorrin, R.J., Gas chromatography-mass spectroscopy investigations on the flavor chemistry of oat groats, J. Agric. Food Chem., 1981, 29, 5, 950-954, https://doi.org/10.1021/jf00107a016 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References