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5«alpha»-Stigmastan-3«beta»-ol


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryOV-1265.3260.Brooks, Cole, et al., 1980Helium; Column length: 25. m; Column diameter: 0.50 mm

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5 MS3325.Radulovic and Dordevic, 201130. m/0.25 mm/0.25 «mu»m, Helium, 5. K/min, 315. C @ 10. min; Tstart: 70. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-5 MS3317.Radulovic and Dordevic, 201130. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.3290.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Brooks, Cole, et al., 1980
Brooks, C.J.W.; Cole, W.J.; McIntyre, H.B.; Smith, A.G., Selective reactions in the analysis and characterization of steroids by gas chromatography-mass spectrometry, Lipids, 1980, 15, 9, 745-755, https://doi.org/10.1007/BF02534028 . [all data]

Radulovic and Dordevic, 2011
Radulovic, N.S.; Dordevic, N.D., Sterods from poison hemlock (Conium maculatum L.): a GC-MS analysis, J. Serb. Chem. Soc., 2011, 76, 11, 1471-1483, https://doi.org/10.2298/JSC110206128R . [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]


Notes

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