2-Nonanone

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5SPB-5DB-5DB-5HP-5MS
Column length (m) 30.60.60.30.20.
Carrier gas He  He 
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.251.1.0.250.25
Tstart (C) 50.40.40.40.60.
Tend (C) 220.230.260.250.240.
Heat rate (K/min) 20.3.4.5.5.
Initial hold (min) 2.2.2.2.4.
Final hold (min) 2.10.10.5.15.
I 1092.1092.1091.1093.1096.
ReferenceBalbontin, Gaete-Eastman, et al., 2007Engel and Ratel, 2007Methven L., Tsoukka M., et al., 2007Wu, Zorn, et al., 2007Kallio, Jussila, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBRTX-1CP Sil 5 CBHP-5CP-Sil 8CB-MS
Column length (m) 50.60.25.30.0.
Carrier gas  HeHeN2He
Substrate      
Column diameter (mm) 0.320.220.250.250.25
Phase thickness (μm)  0.250.40.250.25
Tstart (C) 60.60.80.60.40.
Tend (C) 220.230.270.220.280.
Heat rate (K/min) 4.2.10.5.4.
Initial hold (min) 5.  10.2.
Final hold (min) 30.35.  5.
I 1089.1070.1074.1093.1093.
ReferenceMahadevan and Farmer, 2006Paolini J., Desjobert J.M., et al., 2006Ziegenbein, Hanssen, et al., 2006Celik, Gokturk, et al., 2005Elmore, Cooper, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP-Sil 8CB-MSSPB-5SPB-5BP-1
Column length (m) 25.60.30.30.50.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.530.22
Phase thickness (μm) 1.0.250.251.50.25
Tstart (C) 40.40.60.100.60.
Tend (C) 280.280.250.250.230.
Heat rate (K/min) 5.4.4.5.2.
Initial hold (min)  2.2.  
Final hold (min) 5.5.20. 35.
I 1093.1099.1091.1094.1070.
ReferenceSolina, Baumgartner, et al., 2005Hierro, de la Hoz, et al., 2004Pino, Marbot, et al., 2004Rodríguez-Burruezo, Kollmannsberger, et al., 2004Bianchini, Tomi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP-Sil 8CB-MSMS5DB-1DB-5
Column length (m) 30.60.25.30.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.251.
Tstart (C) 60.40.40.40.50.
Tend (C) 280.280.180.325.200.
Heat rate (K/min) 3.4.3.3.2.5
Initial hold (min)  2.   
Final hold (min)  5.   
I 1091.1098.1096.1068.41089.6
ReferenceBougatsos, Meyer, et al., 2003Bruna, Hierro, et al., 2003Shao, Marriott, et al., 2003Sun and Stremple, 2003Xu, van Stee, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5HP-1HP-5MSBP-1SPB-1
Column length (m) 50.24.30.50.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.220.32
Phase thickness (μm) 0.50.170.250.254.
Tstart (C) 60.60.50.60.45.
Tend (C) 250.250.250.230.240.
Heat rate (K/min) 4.4.5.2.5.
Initial hold (min) 5.2.2. 13.
Final hold (min) 20.20.5.35.5.
I 1103.1070.1090.1070.1075.
ReferenceBredie, Mottram, et al., 2002Nath, Sarma, et al., 2002Shang, Hu, et al., 2002Bianchini, Tomi, et al., 2001Larráyoz, Addis, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5MSCP Sil 8 CBDB-5DB-5
Column length (m) 50.30.60.30.30.
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (μm) 0.40.250.251.1.
Tstart (C) 60.60.40.40.40.
Tend (C) 280.280.280.210.210.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min) 10.5.2.  
Final hold (min) 60.    
I 1077.1091.1092.1091.1093.
ReferencePino, Marbot, et al., 2001Skaltsa, Mavrommati, et al., 2001Elmore, Mottram, et al., 2000Moio, Piombino, et al., 2000Moio, Piombino, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-1OV-1SPB-5DB-5
Column length (m) 30.20.20.60.30.
Carrier gas H2HeHeHeH2
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 1.0.30.31.1.
Tstart (C) 40.45.45.40.40.
Tend (C) 210.220.220.200.210.
Heat rate (K/min) 3.10.10.3.3.
Initial hold (min)  5.5.5. 
Final hold (min)  10.10.2. 
I 1095.1080.1078.1091.1091.
ReferenceMoio, Piombino, et al., 2000Valero, Sanz, et al., 1999Valero, Sanz, et al., 1999Verdier-Metz., Coulon, et al., 1998Moio and Addeo, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1DB-1DB-1
Column length (m) 30.25.25.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.20.20.2480.248
Phase thickness (μm) 1.0.110.110.250.25
Tstart (C) 40.50.50.50.50.
Tend (C) 210.250.250.250.250.
Heat rate (K/min) 3.5.5.5.5.
Initial hold (min)    5.5.
Final hold (min)      
I 1093.1073.1074.1069.1069.
ReferenceMoio and Addeo, 1998Warthen, Lee, et al., 1997Warthen, Lee, et al., 1997DeMilo, Lee, et al., 1996DeMilo, Lee, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-5DB-5SPB-1DB-1
Column length (m) 50.30.30.30.60.
Carrier gas  H2H2HeH2
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 0.251.1.0.250.25
Tstart (C) 50.40.40.50.50.
Tend (C) 250.220.220.250.250.
Heat rate (K/min) 4.3.3.5.2.5
Initial hold (min)    5.5.
Final hold (min)      
I 1064.1093.1093.1069.1075.
ReferenceMisharina and Golovnya, 1996Moio L., Rillo L., et al., 1996Moio L., Rillo L., et al., 1996Lee, DeMilo, et al., 1995Stashenko, Villa, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-1OV-1DB-5OV-1
Column length (m) 22.60.60.30.183.
Carrier gas N2HeHeHeN2
Substrate      
Column diameter (mm) 0.300.250.250.26 
Phase thickness (μm) 1.00.25 0.25 
Tstart (C) 60.40.50.50.0.
Tend (C) 250.220.225.300.230.
Heat rate (K/min) 2.2.1.56.1.
Initial hold (min)    4. 
Final hold (min)  10.50.20. 
I 1067.1070.1062.1090.1073.
Referencede Frutos, Sanz, et al., 1991Zhang and Ho, 1989Chen and Ho, 1987Rostad and Pereira, 1986Schreyen, Dirinck, et al., 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPacked
Active phase Apiezon MApiezon MApiezon M
Column length (m) 1.51.51.5
Carrier gas N2N2N2
Substrate Celite 545Celite 545Celite 545
Column diameter (mm)    
Phase thickness (μm)    
Tstart (C) 75.75.75.
Tend (C) 200.200.200.
Heat rate (K/min) 6.6.6.
Initial hold (min)    
Final hold (min)    
I 1051.1052.1054.
ReferenceGolovnya and Uraletz, 1971Golovnya and Uraletz, 1971Golovnya and Uraletz, 1971
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Balbontin, Gaete-Eastman, et al., 2007
Balbontin, C.; Gaete-Eastman, C.; Vergara, M.; Herrera, R.; Moya-Leon, M.A., Treatment with 1-MCP and the role of ethylene in aroma development of mountain papaya fruit, Postharvest Biol. Technol., 2007, 43, 1, 67-77, https://doi.org/10.1016/j.postharvbio.2006.08.005 . [all data]

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Methven L., Tsoukka M., et al., 2007
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Wu, Zorn, et al., 2007
Wu, S.; Zorn, H.; Krings, U.; Berger, R.G., Volatiles from submerged and surface-cultured beefsteak fungus, Fistulina hepatica, Flavour Fragr. J., 2007, 22, 1, 53-60, https://doi.org/10.1002/ffj.1758 . [all data]

Kallio, Jussila, et al., 2006
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Mahadevan and Farmer, 2006
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Paolini J., Desjobert J.M., et al., 2006
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Ziegenbein, Hanssen, et al., 2006
Ziegenbein, F.C.; Hanssen, H.-P.; König, W.A., Chemical constituents of the essential oils of three wood-rotting fungi, Flavour Fragr. J., 2006, 21, 5, 813-816, https://doi.org/10.1002/ffj.1732 . [all data]

Celik, Gokturk, et al., 2005
Celik, S.; Gokturk, R.S.; Flamini, G.; Cioni, P.L.; Morelli, I., Essential oils of Phlomis leucophracta, Phlomis chimerae and Phlomis grandiflora var. grandiflora from Turkey, Biochem. Syst. Ecol., 2005, 33, 6, 617-623, https://doi.org/10.1016/j.bse.2004.11.010 . [all data]

Elmore, Cooper, et al., 2005
Elmore, J.S.; Cooper, S.L.; Enser, M.; Mottram, D.S.; Sinclair, L.A.; Wilkinson, R.G.; Wood, J.D., Dietary manipulation of fatty acid composition in lamb meat and its effect on the volatile aroma compounds of grilled lamb, Meat Sci., 2005, 69, 2, 233-242, https://doi.org/10.1016/j.meatsci.2004.07.002 . [all data]

Solina, Baumgartner, et al., 2005
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Hierro, de la Hoz, et al., 2004
Hierro, E.; de la Hoz, L.; Ordóñez, J.A., Headspace volatile compounds from salted and occasionally smoked dried meats (cecinas) as affected by animal species, Food Chem., 2004, 85, 4, 649-657, https://doi.org/10.1016/j.foodchem.2003.07.001 . [all data]

Pino, Marbot, et al., 2004
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Rodríguez-Burruezo, A.; Kollmannsberger, H.; Prohens, J.; Nitz, S.; Nuez, F., Analysis of the volatile aroma constituents of parental and hybrid clones of pepino (Solanum muricatum), J. Agric. Food Chem., 2004, 52, 18, 5663-5669, https://doi.org/10.1021/jf040107w . [all data]

Bianchini, Tomi, et al., 2003
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Bougatsos, Meyer, et al., 2003
Bougatsos, C.; Meyer, J.J.M.; Magiatis, P.; Vagias, C.; Chinou, I.B., Composition and antimicrobial activity of the essential oils of Helichrysum kraussii Sch. Bip. and H. rugulosum Less. from south Africa, Flavour Fragr. J., 2003, 18, 1, 48-51, https://doi.org/10.1002/ffj.1152 . [all data]

Bruna, Hierro, et al., 2003
Bruna, J.M.; Hierro, E.M.; de la Hoz, L.; Mottram, D.S.; Fernández, M.; Ordóñez, J.A., Changes in selected biochemical and sensory parameters as affected by the superficial inoculation of Penicillium camemberti on dry fermented sausages, Int. J. Food Microbiol., 2003, 85, 1-2, 111-125, https://doi.org/10.1016/S0168-1605(02)00505-6 . [all data]

Shao, Marriott, et al., 2003
Shao, Y.; Marriott, P.; Shellie, R.; Hügel, H., Solid-phase micro-extraction-comprehensive two-dimensional gas chromatography of ginger (Zingiber officinale) volatiles, Flavour Fragr. J., 2003, 18, 1, 5-12, https://doi.org/10.1002/ffj.1133 . [all data]

Sun and Stremple, 2003
Sun, G.; Stremple, P., Retention index characterization of flavor, fragrance, and many other compounds on DB-1 and DB-XLB, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/pdf/b-0279.pdf. [all data]

Xu, van Stee, et al., 2003
Xu, X.; van Stee, L.L.P.; Williams, J.; Beens, J.; Adahchour, M.; Vreuls, R.J.J.; Brinkman, U.A.Th.; Lelieveld, J., Comprehensive two-dimensional gas chromatography (GC×GC) measurements of volatile organic compounds in the atmosphere, Atmos. Chem. Phys., 2003, 3, 3, 665-682, https://doi.org/10.5194/acp-3-665-2003 . [all data]

Bredie, Mottram, et al., 2002
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Nath, Sarma, et al., 2002
Nath, S.C.; Sarma, K.K.; Vajezikova, I.; Leclercq, P.A., Comparison of volatile inflorescence oils and taxonomy of certain Cymbopogon taxa described as Cymbopogon flexuosus (Nees ex Steud.) Wats., Biochem. Syst. Ecol., 2002, 30, 2, 151-162, https://doi.org/10.1016/S0305-1978(01)00066-7 . [all data]

Shang, Hu, et al., 2002
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Bianchini, Tomi, et al., 2001
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Larráyoz, Addis, et al., 2001
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Pino, Marbot, et al., 2001
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Elmore, Mottram, et al., 2000
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Moio, Piombino, et al., 2000
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DeMilo, Lee, et al., 1996
DeMilo, A.B.; Lee, C.-J.; Moreno, D.S.; Martinez, A.J., Identification of volatiles derived from Citrobacter freundii fermentation of a trypticase soy broth, J. Agric. Food Chem., 1996, 44, 2, 607-612, https://doi.org/10.1021/jf950525o . [all data]

Misharina and Golovnya, 1996
Misharina, T.A.; Golovnya, R.V., Study of the composition of volatiles in raw and processed sardine by gas chromatography and gas chromatography-mass spectrometry, Zh. Anal. Khim., 1996, 51, 7, 791-795. [all data]

Moio L., Rillo L., et al., 1996
Moio L.; Rillo L.; Ledda A.; Addeo F., Odorous constituents of ovine milk in relationship to diet, J. Dairy Sci., 1996, 79, 8, 1322-1331, https://doi.org/10.3168/jds.S0022-0302(96)76488-3 . [all data]

Lee, DeMilo, et al., 1995
Lee, C.-J.; DeMilo, A.B.; Moreno, D.S.; Martinez, A.J., Analysis of the volatile components of a bacterial fermentation that is attractive to the Mexican fruit fly, Anastrepha ludens, J. Agric. Food Chem., 1995, 43, 5, 1348-1351, https://doi.org/10.1021/jf00053a041 . [all data]

Stashenko, Villa, et al., 1995
Stashenko, E.E.; Villa, H.S.; Combariza, M.Y., Comparative study of Colombian rue oils by high resolution gas chromatography using different detection systems, J. Microcolumn Sep., 1995, 7, 2, 117-122, https://doi.org/10.1002/mcs.1220070204 . [all data]

de Frutos, Sanz, et al., 1991
de Frutos, M.; Sanz, J.; Martinez-Castro, I., Characterization of artisanal cheeses by GC and GC/MS analysis of their medium volatility (SDE) fraction, J. Agric. Food Chem., 1991, 39, 3, 524-530, https://doi.org/10.1021/jf00003a019 . [all data]

Zhang and Ho, 1989
Zhang, Y.; Ho, C.-T., Volatile compounds formed from thermnal interaction of 2,4-decadienal with cysteine and glutathione, J. Agric. Food Chem., 1989, 37, 4, 1016-1020, https://doi.org/10.1021/jf00088a044 . [all data]

Chen and Ho, 1987
Chen, C.-C.; Ho, C.-T., Gas chromatographic analysis of thermal degradation products of gingerol compounds in steam-distilled oil from ginger (Zingiber officinale Roscoe), J. Chromatogr., 1987, 387, 499-504, https://doi.org/10.1016/S0021-9673(01)94559-5 . [all data]

Rostad and Pereira, 1986
Rostad, C.E.; Pereira, W.E., Kovats and Lee retention indices determined by gas chromatography/mass spectrometry for organic compounds of environmental interest, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 6, 328-334, https://doi.org/10.1002/jhrc.1240090603 . [all data]

Schreyen, Dirinck, et al., 1976
Schreyen, L.; Dirinck, P.; van Wassenhove, F.; Schamp, N., Volatile flavor components of leek, J. Agric. Food Chem., 1976, 24, 2, 336-341, https://doi.org/10.1021/jf60204a056 . [all data]

Golovnya and Uraletz, 1971
Golovnya, V.; Uraletz, V.P., Gas chromatographic analysis of flavour components with correlation isothermal retention indices, J. Chromatogr., 1971, 61, 65-71, https://doi.org/10.1016/S0021-9673(00)92384-7 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References