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Methyl methacrylate

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5RTX-5RTX-5RTX-5OV-101
Column length (m) 30.30.30.30.19.
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.28
Phase thickness (mum) 0.250.250.250.25 
Temperature (C) 100.120.60.80.120.
I 714.3717.33716.28713.44696.
ReferenceÁdámová, Orinák, et al., 2005Ádámová, Orinák, et al., 2005Ádámová, Orinák, et al., 2005Ádámová, Orinák, et al., 2005Horna, Táborský, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedPackedPacked
Active phase OV-101SE-30Apiezon LApiezon LSE-30
Column length (m) 19.2.  3.7
Carrier gas N2   He
Substrate  Gaschrom QCelite 545Celite 545Celatom silanized (62-72 mesh)
Column diameter (mm) 0.28    
Phase thickness (mum)      
Temperature (C) 80.100.120.160.150.
I 700.694.666.670.699.
ReferenceHorna, Táborský, et al., 1985Winskowski, 1983Bogoslovsky, Anvaer, et al., 1978Bogoslovsky, Anvaer, et al., 1978Ashes and Haken, 1975
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPacked
Active phase OV-1SE-30SE-30
Column length (m)  3.73.7
Carrier gas    
Substrate  Celite 560 silanizedCelite 560
Column diameter (mm)    
Phase thickness (mum)    
Temperature (C) 150.150.150.
I 677.677.677.
ReferenceAshes and Haken, 1971Allen and Haken, 1970Germaine and Haken, 1969
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ádámová, Orinák, et al., 2005
Ádámová, M.; Orinák, A.; Halás, L., Retention indices as identification tool in pyrolysis-capillary gas chromatography, J. Chromatogr. A, 2005, 1087, 1-2, 131-141, https://doi.org/10.1016/j.chroma.2005.01.003 . [all data]

Horna, Táborský, et al., 1985
Horna, A.; Táborský, J.; Dufka, O.; Matousek, P.; Churácek, J., Chromatography of monomers. II. Glass capillary gas chromatography of C1-C18 alkyl esters of acrylic and methacrylic acids, J. Chromatogr., 1985, 325, 367-378, https://doi.org/10.1016/S0021-9673(00)96047-3 . [all data]

Winskowski, 1983
Winskowski, J., Gaschromatographische Identifizierung von Stoffen anhand von Indexziffem und unterschiedlichen Detektoren, Chromatographia, 1983, 17, 3, 160-165, https://doi.org/10.1007/BF02271041 . [all data]

Bogoslovsky, Anvaer, et al., 1978
Bogoslovsky, Yu.N.; Anvaer, B.I.; Vigdergauz, M.S., Chromatographic constants in gas chromatography (in Russian), Standards Publ. House, Moscow, 1978, 192. [all data]

Ashes and Haken, 1975
Ashes, J.R.; Haken, J.K., Gas chromatography of homologous esters. IX. Structure-retention increments of unsaturated esters, J. Chromatogr., 1975, 111, 1, 171-187, https://doi.org/10.1016/S0021-9673(01)80159-X . [all data]

Ashes and Haken, 1971
Ashes, J.R.; Haken, J.K., Gas chromatography of homologous esters. Part V. Retention of aliphatic esters on non-polar, donar and acceptor stationary phases, J. Chromatogr., 1971, 60, 33-44, https://doi.org/10.1016/S0021-9673(00)95527-4 . [all data]

Allen and Haken, 1970
Allen, I.D.; Haken, J.K., Gas chromatography of homologous esters. Part IV. Influence of stationary phase polarity on retention of unsaturated esters, J. Chromatogr., 1970, 51, 415-422, https://doi.org/10.1016/S0021-9673(01)96890-6 . [all data]

Germaine and Haken, 1969
Germaine, R.W.; Haken, J.K., Gas chromatography of homologous esters. Part 2. Unsaturated esters, J. Chromatogr., 1969, 43, 43-47, https://doi.org/10.1016/S0021-9673(00)99163-5 . [all data]


Notes

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