Camphene

Formula: C₁₀H₁₆
Molecular weight: 136.2340
IUPAC Standard InChI: InChI=1S/C10H16/c1-7-8-4-5-9(6-8)10(7,2)3/h8-9H,1,4-6H2,2-3H3
IUPAC Standard InChIKey: CRPUJAZIXJMDBK-UHFFFAOYSA-N
CAS Registry Number: 79-92-5
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
- Bicyclo[2.2.1]heptane, 2,2-dimethyl-3-methylene-, (1R)-
Other names: Bicyclo[2.2.1]heptane, 2,2-dimethyl-3-methylene-; 2,2-Dimethyl-3-methylenebicyclo[2.2.1]heptane; 2,2-Dimethyl-3-methylenenorbornane; 3,3-Dimethyl-2-methylenenorbornane; 3,3-Dimethyl-2-methylenenorcamphane; NA 9011; (-)-camphene
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Normal alkane RI, non-polar column, temperature ramp

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Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-1	RTX-1	RTX-1	Mega-5
Column length (m)	60.	30.	60.	60.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	50.
T_end (C)	250.	240.	230.	230.	220.
Heat rate (K/min)	3.	3.	2.	2.	3.
Initial hold (min)	1.				1.
Final hold (min)	20.		5.	5.	5.
I	950.	955.	950.	950.	950.
Reference	Sardashti, Valizadeh, et al., 2013	Alizadeh and Shaabani, 2012	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012	Dell'Agli, Sanna, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5	HP-5	RTX-1
Column length (m)	30.	25.	25.	25.	60.
Carrier gas	Helium	Hydrogen	Hydrogen	Hydrogen	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.22
Phase thickness (μm)	0.25	0.52	0.52	0.52	0.25
T_start (C)	40.	40.	40.	40.	60.
T_end (C)	250.	280.	280.	280.	230.
Heat rate (K/min)	3.	4.	4.	4.	2.
Initial hold (min)	1.
Final hold (min)	3.	10.	10.	10.	45.
I	954.	941.	942.	942.	940.
Reference	Jian-Yu, Zhu, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Yapi, Boti, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	DB-5	DB-5	DB-5 MS
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	50.	60.	50.	40.	60.
T_end (C)	250.	240.	240.	250.	270.
Heat rate (K/min)	7.	3.	20.	3.	3.
Initial hold (min)	1.		1.	5.
Final hold (min)	5.			20.
I	951.	954.	952.	950.	959.
Reference	Zouari, Ayadi, et al., 2012	Bertoli, Lepnardi, et al., 2011	Cais-Sokolinska, Majcher, et al., 2011	Cao, Li, et al., 2011	Cui, Yang, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP-Sil 5 CB	DB-1	HP-5 MS	DB-5	SE-30 MS
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	Hydrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	35.	60.	50.
T_end (C)	230.	210.	250.	240.	250.
Heat rate (K/min)	3.	5.	5.	3.	5.
Initial hold (min)			3.		5.
Final hold (min)			10.		10.
I	956.	959.	947.	953.	953.
Reference	Esseien, Aboaba, et al., 2011	Fathi, Sahari, et al., 2011	Kadri, Zarai, et al., 2011	Karimi, Farmani, et al., 2011	Menichini, Tundis, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP-Sil 5 CB	Methylsiloxane + 5 % Ph-groups	HP-5	HP-5 MS	ZB-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Nitrogen	Helium	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.26	0.25	0.25	0.25	0.25
T_start (C)	45.	60.	50.	30.	60.
T_end (C)	280.	230.	280.	250.	290.
Heat rate (K/min)	3.	7.	5.	5.	5.
Initial hold (min)		2.	1.	3.
Final hold (min)	22.	20.	1.	10.
I	947.	939.	953.	948.	951.
Reference	Mothana, Hasson, et al., 2011	Nadim, Malik, et al., 2011	Tekaya-Karoui, Boughalleb, et al., 2011	Zarai, Kadri, et al., 2011	Boix, Victorio, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5 MS	RTX-1	DB-5	DB-5 MS	SPB-1
Column length (m)	30.	60.	30.	60.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.20
T_start (C)	60.	60.	50.	40.	70.
T_end (C)	290.	230.	250.	250.	220.
Heat rate (K/min)	5.	2.	2.	5.	3.
Initial hold (min)				15.
Final hold (min)		30.		15.	15.
I	954.	950.	954.	954.	943.
Reference	Boix, Victorio, et al., 2010	Dib, Djabou, et al., 2010	Ho, Wang, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010	Neves, Rosa, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5 MS	HP-5	HP-5 MS	SLB-5 MS
Column length (m)	30.	30.	30.	30.	10.
Carrier gas	Helium	Helium	Hydrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.10
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.10
T_start (C)	60.	100.	70.	60.	50.
T_end (C)	220.	220.	290.	220.	250.
Heat rate (K/min)	5.	2.	5.	6.	10.
Initial hold (min)	10.			3.
Final hold (min)
I	953.	949.	955.	950.	946.
Reference	Ogunwande, Flamini, et al., 2010	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Dordevic, et al., 2010	Safaei-Ghomi and Batooli, 2010	Scandinaro, Tranchida, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5 MS	DB-5 MS	DB-5	DB-1-MS	DB-1
Column length (m)	10.	30.	30.	60.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.10	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.10	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	40.	30.	50.
T_end (C)	250.	240.	240.	200.	220.
Heat rate (K/min)	10.	3.	3.	2.	4.
Initial hold (min)			1.	4.	2.
Final hold (min)				35.	2.
I	949.	954.	928.	940.	939.
Reference	Scandinaro, Tranchida, et al., 2010	Silva, Pott, et al., 2010	de Souza, Lopes, et al., 2010	Takeoka, Hobbs, et al., 2010	Xu, Tang, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5	OV-101	SE-54
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	70.	60.
T_end (C)	250.	250.	240.	220.	260.
Heat rate (K/min)	10.	7.	3.	2.	2.
Initial hold (min)	1.	1.			5.
Final hold (min)	3.	5.			999.
I	953.	954.	954.	941.	950.
Reference	Yang, Zhang, et al., 2010	Zouari, Zouari, et al., 2010	Alim, Goze, et al., 2009	Benites, Moiteiro, et al., 2009	Dayisoylu and Alma, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5	DB-5	RTX-1	RTX-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	70.	60.	60.
T_end (C)	250.	250.	240.	230.	230.
Heat rate (K/min)	2.	5.	5.	2.	2.
Initial hold (min)	8.	2.
Final hold (min)	15.			30.	30.
I	955.	954.	951.	944.	950.
Reference	Farhat, Ginies, et al., 2009	Ho, Wang, et al., 2009	Lawal and Oyedelji, 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	DB-5	5 % Phenyl methyl siloxane	DB-5
Column length (m)	50.	30.	30.	60.	30.
Carrier gas	Helium	Helium	Nitrogen	Helium	Nitrogen
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	45.	40.	90.	40.
T_end (C)	220.	250.	250.	225.	230.
Heat rate (K/min)	2.	3.	3.	3.	2.
Initial hold (min)		3.	1.
Final hold (min)	20.	5.	10.	3.
I	944.	950.	954.	955.	954.
Reference	Ottavioli, Bighelli, et al., 2009	Porto, Decorti, et al., 2009	Rahimi-Nasrabadi, Gholivand, et al., 2009	Retta, Gattuso, et al., 2009	Scrivanti, Anton, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1 MS	DB-5	DB-5	DB-5 MS	HP-5MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	40.	60.	40.	40.	50.
T_end (C)	250.	220.	240.	250.	240.
Heat rate (K/min)	6.	5.	3.	4.	5.
Initial hold (min)	1.	3.	1.	2.
Final hold (min)	4.	5.		2.
I	940.	953.	928.	952.	954.
Reference	Seo, Kim, et al., 2009	Shafaghat and Sadeghi, 2009	de Souza, Lopes, et al., 2009	Su, Wang, et al., 2009	Wannes, Mhamdi, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium		N2	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	50.	60.	60.	50.
T_end (C)	280.	280.	280.	220.	230.
Heat rate (K/min)	4.	9.	3.	5.	4.
Initial hold (min)		3.		10.	4.
Final hold (min)		3.			10.
I	947.	952.	948.	955.	953.
Reference	Zhao, Zeng, et al., 2009	Aicha, Ines, et al., 2008	Baziou, Couladis, et al., 2008	Flamini, Tebano, et al., 2008	Forero, Quijano, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	VF-5MS	SLB-5 MS	ZB-1	DB-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	Helium	Helium	Helium	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	240.	50.	45.	60.
T_end (C)	300.	320.	250.	230.	250.
Heat rate (K/min)	3.	20.	3.	3.	5.
Initial hold (min)		1.	2.
Final hold (min)	30.		10.		10.
I	950.	929.	949.	942.	952.
Reference	Isidorov, Lech, et al., 2008	Kowalski, 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008	Mosayebi, Amin, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Elite-1	HP-5 MS	HP-5	RTX-5	HP-5
Column length (m)	30.	30.	30.	20.	25.
Carrier gas	Helium	Helium	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.18	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	246.	250.	280.	280.	240.
Heat rate (K/min)	3.	2.	5.	4.	4.
Initial hold (min)		8.	1.	1.	2.
Final hold (min)		15.	1.
I	944.	943.	962.	951.	955.
Reference	Raj, Baby, et al., 2008	Sahraoui, Vian, et al., 2008	Saidana, Mahjoub, et al., 2008	Skalicka-Wozniak, Los, et al., 2008	Verdian-rizi, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	HP-5	HP-5 MS	DB-5	DB-5MS
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	Helium	Helium	Helium	Nitrogen	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.32	0.25
T_start (C)	65.	60.	50.	60.	60.
T_end (C)	260.	250.	230.	220.	240.
Heat rate (K/min)	6.	5.	3.	5.	3.
Initial hold (min)		30.	10.	3.
Final hold (min)			10.	5.
I	981.	952.	953.	947.	952.
Reference	Wang, Yi, et al., 2008	Yassa and Akhani, 2008	Adams, Beauchamp, et al., 2007	Amiri, 2007	Andrade, Oliveira, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	CP Sil 5 CB	HP-5MS	SE-52	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	N2	He		He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.26
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	200.	300.	280.	220.	240.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)				1.
Final hold (min)	20.			5.
I	969.	945.	950.	943.	944.
Reference	Araque, Rojas, et al., 2007	Baran, von Reuss, et al., 2007	Basta, Pavlovic, et al., 2007	Bicchi, Cordero, et al., 2007	Bos, Woerdenbag, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	DB-5	DB-5	HP-5MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	N2	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.26	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	40.	60.	60.
T_end (C)	280.	240.	220.	290.	250.
Heat rate (K/min)	3.	5.	3.	3.	2.
Initial hold (min)		1.			8.
Final hold (min)		4.			15.
I	951.	953.	960.	944.	942.
Reference	Bozin B., Mlmica-Dukic N., et al., 2007	Cheraif, Ben Jannet, et al., 2007	Chyau, Tsai, et al., 2007	Elfami, Bos, et al., 2007	Ferhat, Meklati, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZP-5	DB-1	DB-5	Col-Elite 5MS	DBP-5
Column length (m)	60.	60.	30.	30.	25.
Carrier gas	He	Nitrogen	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.22
T_start (C)	40.	60.	60.	30.	40.
T_end (C)	260.	250.	210.	246.	250.
Heat rate (K/min)	6.	4.	30.	3.	3.
Initial hold (min)	7.	1.	3.		1.
Final hold (min)	1.	10.			10.
I	958.	950.	942.	951.	924.
Reference	Füssel, Dötterl, et al., 2007	Ghasempour, Shirinpour, et al., 2007	Ghasemi, Yamini, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Heravi and Sereshti, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	HP-5	DB-5MS	ZB-5	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He		Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	50.
T_end (C)	250.	250.	280.	220.	260.
Heat rate (K/min)	5.	5.	3.	4.	2.5
Initial hold (min)	5.	5.		5.	1.
Final hold (min)	10.	10.	30.	20.	20.
I	953.	951.	929.	948.	937.
Reference	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007	Marongiu B., Piras A., et al., 2007	Mohottalage, Tabacchi, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	Methyl Silicone	DB-1	SPB-1
Column length (m)	30.	25.	50.	50.	30.
Carrier gas	He	H2	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.2
Phase thickness (μm)	0.32	0.33		0.25	0.2
T_start (C)	50.	60.	50.	95.	70.
T_end (C)	250.	240.	240.	240.	220.
Heat rate (K/min)	5.	3.	3.	4.	3.
Initial hold (min)
Final hold (min)					15.
I	946.	953.	953.	938.	943.
Reference	Nori-Shargh, Raftari, et al., 2007	Oliveira, Leitão, et al., 2007	Ozcan and Chalchat, 2007	Pala-Paul, Brophy, et al., 2007	Pinto, Salgueiro, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	BPX-5	DB-1	DB-1	DB-1
Column length (m)	30.	50.	60.	60.	60.
Carrier gas	He	He	Nitrogen		He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	1.	0.25	0.25	0.25
T_start (C)	50.	50.	60.	60.	60.
T_end (C)	250.	300.	250.	250.	250.
Heat rate (K/min)	2.	4.	4.	5.	5.
Initial hold (min)		1.	1.
Final hold (min)		10.	10.
I	945.	972.	950.	945.	950.
Reference	Raal, Orav, et al., 2007	Rali, Wossa, et al., 2007	Reza, Ebrahim, et al., 2007	Salehi, Asghari, et al., 2007	Salehi, Fakhari, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DBP-5	DB-5	DB-5	Elite-5MS
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	Helium	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.22	0.25	0.25	0.5
T_start (C)	50.	40.	60.	40.	40.
T_end (C)	240.	250.	320.	250.	280.
Heat rate (K/min)	4.	3.	10.	2.	4.
Initial hold (min)		1.			5.
Final hold (min)		10.	4.	33.	10.
I	950.	924.	953.	951.	949.
Reference	Sefidkon, Abbasi, et al., 2007	Sereshti and Samadi, 2007	Smelcerovic, Spiteller, et al., 2007	Sylvestre, Pichette, et al., 2007	Tava, Pecetti, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5 MS	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.32
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	280.	280.	280.	250.	250.
Heat rate (K/min)	3.	3.	3.	3.	5.
Initial hold (min)				5.	30.
Final hold (min)				10.
I	953.	930.	954.	942.	952.
Reference	Tsokou, Georgopoulos, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Yassa and Akhani, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-5	ZB-5	AT-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	N2	N2	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	50.	40.	60.
T_end (C)	280.	280.	265.	300.	200.
Heat rate (K/min)	9.	9.	2.5	2.	4.
Initial hold (min)	3.	3.	1.
Final hold (min)	3.	3.	20.		20.
I	949.	952.	949.	950.	956.
Reference	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006	Bazargani, Almasirad, et al., 2006	Biondi, Sari, et al., 2006	Borges, Rojas, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-1	SPB-1	DB-1	DB-5
Column length (m)	30.	50.	30.	60.	30.
Carrier gas	He	He	Helium	Nitrogen	N2
Substrate
Column diameter (mm)	0.25	0.2	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.5	0.20		0.25
T_start (C)	60.	60.	70.	40.	70.
T_end (C)	280.	250.	220.	200.	230.
Heat rate (K/min)	3.	2.	3.	2.	2.
Initial hold (min)				1.	2.
Final hold (min)		120.	15.	9.	20.
I	951.	943.	943.	943.	955.
Reference	Bozin, Mimicá-Dukic, et al., 2006	Castel, Fernandez, et al., 2006	Cavaleiro, Pinto, et al., 2006	Chen, Sheu, et al., 2006	Choi, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-5MS	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He			Helium	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.26	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	246.	230.	280.	290.	250.
Heat rate (K/min)	3.	3.	4.	3.	2.
Initial hold (min)
Final hold (min)		15.
I	952.	953.	955.	944.	953.
Reference	Coronel, Cerda-Garcia-Rojas, et al., 2006	Damjanovic, Skala, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006	Farah, Afifi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-1	DB-5	DB-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	50.
T_end (C)	300.	250.	240.	240.	250.
Heat rate (K/min)	5.	2.	5.	5.	3.
Initial hold (min)	5.		2.	2.
Final hold (min)	5.	40.			10.
I	949.	944.	950.	950.	951.
Reference	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006	Havlik, Kokoska, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	HP-5MS	HP-5MS	Methyl Silicone
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	50.	90.
T_end (C)	260.	280.	280.	280.	220.
Heat rate (K/min)	3.	5.	5.	5.	7.
Initial hold (min)		4.	4.	4.	2.
Final hold (min)		10.	10.	10.
I	952.	953.	956.	953.	946.
Reference	Javidnia, Miri, et al., 2006	Kim, Abd El-Aty, et al., 2006	Kim, Abd El-Aty, et al., 2006	Kim, El-Aty, et al., 2006	Kitchlu, Bakshi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-1	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	N2	N2	N2
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	260.	300.	300.	300.	200.
Heat rate (K/min)	5.	4.	5.	4.	5.
Initial hold (min)	2.		4.
Final hold (min)	13.
I	954.	948.	943.	939.	948.
Reference	Kucuk, Gulec, et al., 2006	Kula, Izydorczyk, et al., 2006	Kurowska and Galazka, 2006	Lis and Milczarek, 2006	Martin, Joseph, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	5 % Phenyl methyl siloxane	HP-101	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	Nitrogen	N2	Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.52	0.25	0.2	0.25
T_start (C)	50.	50.	60.	70.	50.
T_end (C)	280.	280.	280.	200.	250.
Heat rate (K/min)	5.	5.	3.	3.	3.
Initial hold (min)				2.	5.
Final hold (min)	5.	5.	30.	15.
I	950.	950.	928.	953.	948.
Reference	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Marongiu, Piras, et al., 2006	Mastelic, Jerkovic, et al., 2006	Mirza, Navaei, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	CP-Sil 5 CB	NB-30
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He	Hydrogen	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.15	0.25
T_start (C)	60.	60.	50.	50.	50.
T_end (C)	220.	220.	250.	230.	250.
Heat rate (K/min)	4.	4.	4.	3.	2.
Initial hold (min)	5.	5.
Final hold (min)
I	956.	956.	952.	955.	943.
Reference	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Najafpour Navaei, Mirza, et al., 2006	Olawore, Usman, et al., 2006	Orav, Raal, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SE-52	DB-1	HP-5MS	DB-5
Column length (m)	25.	50.	50.	30.	30.
Carrier gas	N2	Helium	N2	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.15		0.25	0.25	0.25
T_start (C)	50.	50.	95.	40.	70.
T_end (C)	200.	240.	240.	260.	280.
Heat rate (K/min)	4.	3.	4.	4.	4.
Initial hold (min)	3.				4.
Final hold (min)
I	955.	953.	953.	952.	953.
Reference	Ouamba, Ouabonzi, et al., 2006	Ozcan, Chalchat, et al., 2006	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Petrovic, Ristic, et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Hydrogen	Hydrogen	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	70.	60.	60.	60.
T_end (C)	280.	280.	280.	200.	260.
Heat rate (K/min)	4.	4.	3.	2.	5.
Initial hold (min)	4.	4.
Final hold (min)				60.
I	953.	952.	930.	953.	951.
Reference	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pitarokili, Tzakou, et al., 2006	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	DB-1	FSOT-RSL-200	DB-5	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He		Hydrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	70.	40.	50.	40.
T_end (C)	300.	230.	280.	240.	240.
Heat rate (K/min)	2.	2.	6.	4.	4.
Initial hold (min)		2.	5.
Final hold (min)		20.	5.
I	950.	949.	953.	951.	952.
Reference	Sari M., Biondi D.M., et al., 2006	Sawamura, Onishi, et al., 2006	Schmidt, Jirovetz, et al., 2006	Sefidkon, Abbasi, et al., 2006	Sefidkon and Jamzad, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-1	CP Sil 5 CB	SPB-5
Column length (m)	60.	25.	60.	25.	60.
Carrier gas	He	N2	Helium		He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.32
Phase thickness (μm)		0.33	0.25		1.
T_start (C)	40.	30.	60.	50.	40.
T_end (C)	250.	280.	250.	230.	230.
Heat rate (K/min)	4.	3.	5.	3.	3.
Initial hold (min)					5.
Final hold (min)			10.		2.
I	953.	954.	948.	950.	961.
Reference	Sefidkon, Jamzad, et al., 2006	Shafi, Jose, et al., 2006	Sonboli, Mirjalili, et al., 2006	Tesso, Kubeczka, et al., 2006	Tornambe, Cornu, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	SPB-1	SPB-1	DB-5
Column length (m)	30.	50.	50.	30.	30.
Carrier gas	N2	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	60.	90.	50.	50.	40.
T_end (C)	240.	240.	220.	250.	250.
Heat rate (K/min)	4.	4.	4.	4.	4.
Initial hold (min)			1.	1.
Final hold (min)			10.	10.
I	952.	938.	940.	943.	947.
Reference	Trilles, Bombarda, et al., 2006	Velasco-Negueruela, Pérez-Alonso, et al., 2006	Wong, Lim, et al., 2006	Wong, Sivasothy, et al., 2006	Yadegarinia, Gachkar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5MS	DB-5	Methyl Silicone
Column length (m)	30.	30.	30.	50.	60.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.249	0.25	0.3	0.3
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	280.	290.	240.	240.	240.
Heat rate (K/min)	3.	3.	3.	2.	3.
Initial hold (min)
Final hold (min)
I	944.	945.	954.	950.	949.
Reference	Basta, Tzakou, et al., 2005	Bos, Stojanova, et al., 2005	Busman, Zoghbi, et al., 2005	Chagonda and Chalchat, 2005	Chalchat and Özcan, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	HP-5	DB-1	DB-1	HP-1
Column length (m)	60.	25.	30.	60.	50.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.2	0.25	0.25	0.2
Phase thickness (μm)	1.	0.33	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	230.	240.	250.	250.	250.
Heat rate (K/min)	3.	3.	5.	5.	2.
Initial hold (min)	5.		5.		60.
Final hold (min)		7.	15.
I	961.	945.	955.	950.	944.
Reference	Cornu, Kondjoyan, et al., 2005	Duarte, Figueira, et al., 2005	Facundo, Pinto, et al., 2005	Fakhari, Salehi, et al., 2005	Fernandez, Lizzani-Cuvelier, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	RSL-200	DB-1
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	50.	40.	40.	50.
T_end (C)	300.	250.	280.	280.	265.
Heat rate (K/min)	5.	3.	8.	6.	2.5
Initial hold (min)	5.	3.		2.	1.
Final hold (min)	5.	10.		10.	30.
I	949.	952.	946.	956.	941.
Reference	Figuérédo, Cabassu, et al., 2005	Ghasemi Y., Faridi P., et al., 2005	Jelén, Krawczyk, et al., 2005	Jirovetz, Buchbauer, et al., 2005	Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He		Helium
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)			0.25	0.25	0.25
T_start (C)	60.	60.	35.	35.	38.
T_end (C)	240.	240.	280.	280.	220.
Heat rate (K/min)	3.	3.	4.	4.	5.
Initial hold (min)			2.	2.	1.
Final hold (min)					2.
I	955.	956.	946.	946.	946.
Reference	Khayyat and Karimi, 2005	Khayyat and Karimi, 2005	Kowalski and Wolski, 2005	Kowalski, 2005	Krist, Stuebiger, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	DB-5	CP Sil 5 CB	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.15	0.25
T_start (C)	60.	60.	60.	50.	40.
T_end (C)	230.	280.	220.	230.	250.
Heat rate (K/min)	3.	3.	4.	3.	5.
Initial hold (min)		30.	5.		0.5
Final hold (min)					2.
I	943.	933.	954.	951.	953.
Reference	Limberger, Sobral, et al., 2005	Marongiu, Piras, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005	Ogunwande, Olawore, et al., 2005	Özel, Gögüs, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	CP Sil 5 CB	CP Sil 5 CB	HP-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25		0.25
T_start (C)	60.	40.	40.	60.	60.
T_end (C)	280.	220.	220.	240.	275.
Heat rate (K/min)	3.	4.	4.	5.	4.
Initial hold (min)		1.	1.
Final hold (min)
I	954.	954.	954.	950.	950.
Reference	Petrakis, Roussis, et al., 2005	Rohloff and Bones, 2005	Rohloff and Bones, 2005	Saeidnia, Gohari, et al., 2005	Sajjadi and Ghannadi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	PE-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	220.	240.	230.	230.	280.
Heat rate (K/min)	3.	4.	5.	3.	3.
Initial hold (min)	4.		2.
Final hold (min)			4.	20.
I	950.	952.	947.	954.	944.
Reference	Salehi, Sefidkon, et al., 2005	Sefidkon and Jamzad, 2005	Singh, Raina, et al., 2005	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5	HP-5MS	HP-5 MS	HP-5MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.50	0.25
T_start (C)	60.	40.	50.	60.	60.
T_end (C)	250.	210.	240.	260.	280.
Heat rate (K/min)	5.	2.	3.	3.	3.
Initial hold (min)		2.	3.
Final hold (min)	10.	33.		20.
I	952.	953.	932.	953.	930.
Reference	Sonboli A., Fakhari A.R., et al., 2005	Stevanovic, Garneau, et al., 2005	Tepe B., Sokmen M., et al., 2005	Topçu, Barla, et al., 2005	Tzakou, Bazos, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5MS	SPB-1	CP Sil 5 CB
Column length (m)	50.	50.	30.	50.	30.
Carrier gas	N2			He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	90.	60.	40.	50.	50.
T_end (C)	240.	240.	220.	220.	200.
Heat rate (K/min)	4.	3.	3.	4.	5.
Initial hold (min)			5.	3.
Final hold (min)			10.	30.
I	938.	937.	942.	946.	952.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2	Vichi, Riu-Aumatell, et al., 2005	Wong, Lee, et al., 2005	Agnaniet, Menut, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-1	SPB-5	DB-5	ZB-5
Column length (m)	50.	60.	60.	25.	60.
Carrier gas		N2	He	Nitrogen	He
Substrate
Column diameter (mm)	0.22	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	1.	0.25	0.25
T_start (C)	60.	70.	60.	60.	40.
T_end (C)	220.	230.	200.	240.	260.
Heat rate (K/min)	2.	2.	4.	3.	6.
Initial hold (min)		2.			4.6
Final hold (min)	20.	20.	30.		1.
I	944.	954.	953.	949.	963.
Reference	Blanc, Muselli, et al., 2004	Choi, 2004	Gauvin, Ravaomanarivo, et al., 2004	JAvidnia, Mojab, et al., 2004	Jürgens and Dötterl, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	RTX-1	SE-54	RTX-1	DB-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	N2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	40.
T_end (C)	280.	300.	260.	300.	210.
Heat rate (K/min)	4.	4.	2.	4.	2.
Initial hold (min)	4.		5.		2.
Final hold (min)					33.
I	949.	950.	949.	944.	952.
Reference	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004	Lis, Boczek, et al., 2004	Lopez Arze, Collin, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5MS	HP-5MS	NB-30	NB-30
Column length (m)	25.	30.	30.	50.	50.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	220.	280.	280.	250.	250.
Heat rate (K/min)	5.	3.	3.	2.	2.
Initial hold (min)
Final hold (min)		30.
I	946.	924.	952.	945.	945.
Reference	Mallavarapu, Kulkarni, et al., 2004	Marongiu, Porcedda, et al., 2004	Mimica-Dukic, Bozin, et al., 2004	Orav, Stulova, et al., 2004	Orav, Stulova, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	NB-30	NB-30	DB-5	Methyl Silicone
Column length (m)	50.	50.	50.	30.	60.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	50.	50.	35.	60.
T_end (C)	240.	250.	250.	220.	200.
Heat rate (K/min)	4.	2.	2.	2.5	4.
Initial hold (min)					1.
Final hold (min)				6.	20.
I	943.	945.	943.	954.	949.
Reference	Palá-Paúl, Velasco-Negueruela, et al., 2004	Raal, Arak, et al., 2004	Raal, Paaver, et al., 2004	Rohloff, Mordal, et al., 2004	Rojas, Usubillaga, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5MS	DB-1	DB-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	He	He		Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	70.	70.
T_end (C)	200.	280.	280.	230.	230.
Heat rate (K/min)	4.	4.	4.	2.	2.
Initial hold (min)	1.			2.	2.
Final hold (min)	20.			20.
I	949.	946.	951.	955.	955.
Reference	Royas, Usubillaga, et al., 2004	Sadeghpour, Asghari, et al., 2004	Sajjadi and Shahpiri, 2004	Sawamura, Son, et al., 2004	Sawamura, Sou, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-1	DB-5	HP-5
Column length (m)	30.	60.	30.	30.	25.
Carrier gas		He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.5
T_start (C)	50.	40.	40.	40.	30.
T_end (C)	250.	280.	260.	250.	280.
Heat rate (K/min)	3.	4.	2.	2.	3.
Initial hold (min)	5.	5.	5.	5.
Final hold (min)			20.	20.
I	952.	953.	945.	951.	954.
Reference	Sefidkon, Jamzad, et al., 2004	Sefidkon and Shaabani, 2004	Senatore, Napolitano, et al., 2004	Senatore, Rigano, et al., 2004	Shafi, Nambiar, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	CP Sil 5 CB	BPX-5	CP Sil 8 CB
Column length (m)	25.	30.	20.	25.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.52	0.25	0.25	1.	0.25
T_start (C)	40.	60.	100.	60.	50.
T_end (C)	240.	240.	270.	250.	200.
Heat rate (K/min)	4.	3.	8.	3.	10.
Initial hold (min)			2.	5.	3.
Final hold (min)				10.	2.
I	953.	950.	940.	957.	950.
Reference	Simic, Sokovic, et al., 2004	Tellez, Khan, et al., 2004	Thappa, Bakshi, et al., 2004	Vilaseca, Guy, et al., 2004	Wang and Guo-Y. -L., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 8 CB	DB-5	HP-5MS	DB-5	DB-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.32	0.249	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	70.
T_end (C)	200.	300.	275.	240.	230.
Heat rate (K/min)	5.	3.	4.	4.	2.
Initial hold (min)	5.				2.
Final hold (min)					20.
I	953.	946.	952.	953.	955.
Reference	Wang, Guo, et al., 2004	Woerdenbag, Windono, et al., 2004	Afsharypuor and Jahromy, 2003	Cabanillas, Lopez, et al., 2003	Choi, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RTX-5Sil	HP-1	DB-1	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	70.	50.	60.
T_end (C)	280.	200.	200.	200.	275.
Heat rate (K/min)	3.	4.	10.	5.	4.
Initial hold (min)
Final hold (min)		10.
I	949.	950.	944.	933.	951.
Reference	Couladis, Özcan, et al., 2003	Dudai, Larkov, et al., 2003	Fekam Boyom, Amvam Zollo, et al., 2003	Fekam Boyom, Ngouana, et al., 2003	Ghannadi, Aghazari, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RSL-200	RSL-200	CP Sil 5 CB	DB-5MS
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	H2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	35.	60.
T_end (C)	275.	280.	280.	280.	240.
Heat rate (K/min)	4.	6.	6.	5.	3.
Initial hold (min)		5.	5.	2.5
Final hold (min)		5.	5.
I	950.	939.	950.	940.	948.
Reference	Hajhashemi, Ghannadi, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2	Kanjilal, Kotoky, et al., 2003	Maia, Taveira, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	ZB-1	DB-1	HP-5	OV-101
Column length (m)	30.	30.	60.	30.	50.
Carrier gas	He	N2	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.2
Phase thickness (μm)	0.25	0.25	0.25		0.5
T_start (C)	60.	45.	50.	70.	50.
T_end (C)	280.	230.	270.	210.	250.
Heat rate (K/min)	3.	3.	4.	2.	2.
Initial hold (min)
Final hold (min)	30.			60.
I	948.	942.	952.	951.	940.
Reference	Marongiu, Porcedda, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003	Mirza, Nik, et al., 2003	Mookdasanit, Tamura, et al., 2003	Orav, Kailas, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	DB-1	DB-5
Column length (m)	50.	30.	30.	60.	30.
Carrier gas	N2	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	60.	60.	50.	75.
T_end (C)	240.	280.	280.	250.	220.
Heat rate (K/min)	4.	4.	3.	4.	3.
Initial hold (min)		10.			4.
Final hold (min)		40.
I	957.	953.	934.	953.	954.
Reference	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003	Priestap, van Baren, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5MS	HP-5	DB-5
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	220.	220.	275.	280.	240.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)
Final hold (min)
I	943.	943.	951.	951.	950.
Reference	Rasooli and Mirmostafa, 2003	Rasooli and Mirmostafa, 2003	Sadraei, Ghannadi, et al., 2003	Sajjadi and Mehregan, 2003	da Silva, Luz, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	DB-1	Cross-Linked Methylsilicone	HP-5
Column length (m)	60.	60.	50.	25.	25.
Carrier gas		N2	N2	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.53
T_start (C)	40.	70.	90.	70.	40.
T_end (C)	250.	230.	240.	250.	280.
Heat rate (K/min)	5.	2.	4.	4.	4.
Initial hold (min)	15.	2.
Final hold (min)		20.
I	949.	958.	924.	938.	950.
Reference	Stashenko, Jaramillo, et al., 2003	Tu, Onishi, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003, 2	Velickovic, Randjelovic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5	DB-5
Column length (m)	25.	25.	25.	30.	30.
Carrier gas	H2	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.53	0.53	0.53	0.32	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	280.	280.	280.	250.	240.
Heat rate (K/min)	4.	4.	4.	5.	3.
Initial hold (min)				30.
Final hold (min)
I	954.	942.	954.	959.	952.
Reference	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Yassa, Akhani, et al., 2003	Zoghbi, Andrade, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	OV-101	DB-5	HP-1
Column length (m)	25.	30.	25.	30.	30.
Carrier gas	N2	He		He	He
Substrate
Column diameter (mm)	0.25	0.249	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	60.	50.	60.	70.
T_end (C)	250.	300.	200.	280.	220.
Heat rate (K/min)	4.	3.	5.	3.	3.
Initial hold (min)
Final hold (min)	10.	5.		30.	15.
I	952.	946.	944.	947.	942.
Reference	Zrira, Elamrani, et al., 2003	Bos, Koulman, et al., 2002	Boyom, Keumedjio, et al., 2002	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	5 % Phenyl methyl siloxane	DB-1	DB-5MS	DB-5MS	BP-1
Column length (m)	30.	60.	30.	30.	25.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.50
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	75.	50.	60.	50.	60.
T_end (C)	200.	200.	280.	280.	220.
Heat rate (K/min)	3.	3.	3.	15.	5.
Initial hold (min)	4.	6.		2.
Final hold (min)	8.			10.	10.
I	954.	963.	961.	946.	946.
Reference	Cicció and Gómez-Laurito, 2002	Cimanga, Apers, et al., 2002	Congiu, Falconieri, et al., 2002	Damon, Hernández, et al., 2002	Das, Ram, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5	SE-30	HP-5
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	N2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	60.	70.	50.
T_end (C)	250.	245.	275.	240.	200.
Heat rate (K/min)	4.	3.	4.	4.	3.
Initial hold (min)		20.
Final hold (min)
I	953.	931.	946.	957.	954.
Reference	Farah, Fechtal, et al., 2002	Gancel, Ollé, et al., 2002	Ghannadi, Sajjadi, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Isidorov and Jdanova, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	SPB-5	DB-5	DB-5	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	35.	35.
T_end (C)	280.	240.	240.	280.	280.
Heat rate (K/min)	6.	5.	3.	3.	4.
Initial hold (min)	5.	3.		2.	2.
Final hold (min)	5.	10.		15.	15.
I	955.	961.	952.	946.	946.
Reference	Jirovetz, Buchbauer, et al., 2002	Kim and Lee, 2002	Kobaisy, Tellez, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-1	DB-1	SPB-5
Column length (m)	25.	25.	30.	50.	30.
Carrier gas	He	He	He	N2	Helium
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)			0.25	0.25	0.25
T_start (C)	50.	50.	60.	80.	60.
T_end (C)	200.	200.	250.	225.	250.
Heat rate (K/min)	5.	5.	4.	4.	4.
Initial hold (min)			10.		2.
Final hold (min)					20.
I	944.	945.	944.	941.	953.
Reference	Kuiate, Bessière, et al., 2002	Menut, Bessière, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Pino, Marbot, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	DB-1	DB-1	RTX-5	DB-1
Column length (m)	50.	60.	60.	20.	50.
Carrier gas	N2	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.18	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.4	0.25
T_start (C)	90.	40.	40.	20.	60.
T_end (C)	220.	280.	280.	290.	240.
Heat rate (K/min)	3.	4.	4.	40.	3.
Initial hold (min)		5.	5.	3.5
Final hold (min)				0.5
I	942.	954.	953.	949.	937.
Reference	Priestap, van Baren, et al., 2002	Sefidkon, Jalili, et al., 2002	Sefidkon, 2002	Sies A., Hirsch R., et al., 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	DB-5MS	DB-5	SPB-5
Column length (m)	30.	60.	30.	30.	60.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	60.	40.
T_end (C)	280.	250.	270.	240.	220.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)		5.			5.
Final hold (min)					15.
I	953.	952.	948.	955.	951.
Reference	Velickovic, Randjelovic, et al., 2002	Yamini, Sefidkon, et al., 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Cornu, Carnat, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5	Optima-5	RTX-1
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	He	He	N2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	40.	40.	60.	50.	60.
T_end (C)	280.	280.	220.	250.	300.
Heat rate (K/min)	4.	4.	5.	3.	4.
Initial hold (min)	5.	5.	10.	3.
Final hold (min)
I	936.	940.	955.	943.	945.
Reference	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Gallori, Flamini, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001	Kalemba, Marschall, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	SPB-5	CBP-1	DB-1	DB-1
Column length (m)	30.	60.	25.	60.	30.
Carrier gas	N2	Helium	Nitrogen	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	50.	50.	50.	80.
T_end (C)	180.	240.	210.	270.	225.
Heat rate (K/min)	2.	3.	3.	4.	4.
Initial hold (min)	2.	3.	2.
Final hold (min)	1.	10.
I	942.	959.	941.	952.	938.
Reference	Kamath, Asha, et al., 2001	Kim and Lee, 2001	Ly, Yamauchi, et al., 2001	Mirza, Ahmadi, et al., 2001	Palá-Paúl, Pérez-Alonso, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-1	CP Sil 5 CB	CP-Sil 5 CB
Column length (m)	60.	30.	30.	25.	25.
Carrier gas	He	H2	He	He	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)		0.25		0.39	0.39
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	250.	285.	240.	220.	220.
Heat rate (K/min)	3.	3.	3.	5.	5.
Initial hold (min)	5.
Final hold (min)
I	953.	946.	946.0	949.	949.
Reference	Rousis, Papadogianni, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001	Santos, Moreira, et al., 2001	Sayyah, Kamalinejad, et al., 2001	Sayyah, Kamalinejad, et al., 2001, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5	OV-101	OV-101	SPB-1
Column length (m)	30.	30.	50.	50.	30.
Carrier gas	Helium	He	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25			0.2
T_start (C)	50.	60.	80.	80.	80.
T_end (C)	250.	240.	200.	200.	300.
Heat rate (K/min)	5.	3.	2.	2.	5.
Initial hold (min)	2.				3.
Final hold (min)	5.
I	955.	954.	953.	953.	954.
Reference	Shang, Hu, et al., 2001	Tellez M., Estell R., et al., 2001	Yang, 2001	Yang, 2001, 2	Fraternale, Giamperi, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	SPB-5	DB-1	DB-5	BP-1
Column length (m)	60.	60.	25.	30.	25.
Carrier gas	H2	He	Nitrogen	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.50	0.22	0.33
Phase thickness (μm)	0.25	0.25	0.25	0.25	1.0
T_start (C)	40.	70.	60.	70.	60.
T_end (C)	250.	240.	220.	230.	275.
Heat rate (K/min)	6.	5.	5.	4.	4.
Initial hold (min)		8.		2.
Final hold (min)		20.		20.
I	954.	958.	947.	951.	952.
Reference	Jirovetz, Puschmann, et al., 2000	Kim, Kim, et al., 2000	Mallavarapu, Rao, et al., 2000	Mitiku, Sawamura, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	OV-101	DB-5	SE-30	Methyl Silicone
Column length (m)	30.	50.	30.	25.	60.
Carrier gas	He	Nitrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25		0.25		0.25
T_start (C)	60.	40.	60.	60.	40.
T_end (C)	275.	200.	240.	230.	220.
Heat rate (K/min)	4.	2.	3.	3.	5.
Initial hold (min)		10.			10.
Final hold (min)
I	951.	952.	954.	941.	943.70
Reference	Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2	Tamura, Boonbumrung, et al., 2000	Tellez, Dayan, et al., 2000	Ali N.A.M. and Jantan, 1999	Baraldi, Rapparini, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	SPB-1	OV-101	SE-30	RTX-1
Column length (m)	25.	50.	52.	30.	30.
Carrier gas	Hydrogen		Helium	N2	N2
Substrate
Column diameter (mm)	0.32	0.2	0.26	0.25	0.25
Phase thickness (μm)	0.30	0.33	0.13	0.25	0.25
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	200.	260.	220.	220.	300.
Heat rate (K/min)	3.	4.	3.	4.	4.
Initial hold (min)	1.		0.	10.
Final hold (min)	10.		0.
I	933.	943.	943.	945.	948.
Reference	Bicchi, Binello, et al., 1999	Choo, Wong, et al., 1999	Dzumayev, Tkachenko, et al., 1999	Jassbi, Ahmad, et al., 1999	Kalemba, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	SE-30	DB-1	OV-1
Column length (m)	25.	30.	25.	30.	25.
Carrier gas	He		He	He	H2
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.25	0.25
Phase thickness (μm)	0.25	1.		0.25	0.25
T_start (C)	50.	40.	60.	50.	40.
T_end (C)	290.	200.	230.	200.	220.
Heat rate (K/min)	4.	3.	3.	4.	3.
Initial hold (min)		5.	10.		5.
Final hold (min)					5.
I	946.	948.	941.	948.	941.
Reference	Koulman, 1999	Meynier, Novelli, et al., 1999	Mohd and Jantan, 1999	Nori-Shargh, Norouzi-Arasi, et al., 1999	Oberhofer, Nikiforov, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	OV-101	SE-30	Ultra-2
Column length (m)	25.	50.	50.	30.	25.
Carrier gas	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)		0.25	0.25	0.20
T_start (C)	50.	70.	70.	60.	40.
T_end (C)	230.	240.	220.	200.	300.
Heat rate (K/min)	3.	4.	2.	3.	5.
Initial hold (min)			5.	4.	4.
Final hold (min)
I	946.	938.	936.	943.	949.
Reference	Oyedeji, Olawore, et al., 1999	Palá-Paúl, Pérez-Alonso, et al., 1999	Pateira, Nogueira, et al., 1999	Prikhod'ko, Klyuev, et al., 1999	Quiroz, Fuentes-Contreras, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	CP Sil 5 CB	DB-1	DB-5	DB-1
Column length (m)	25.	25.	60.	30.	60.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.5	0.25	0.25	0.25	0.32
Phase thickness (μm)		0.39	0.25	0.25
T_start (C)	60.	60.	40.	40.	60.
T_end (C)	220.	220.	280.	220.	230.
Heat rate (K/min)	5.	5.	4.	4.	3.
Initial hold (min)		5.	5.	5.
Final hold (min)	10.	20.			5.
I	947.	948.	945.	947.	950.
Reference	Rao, Bhattacharya, et al., 1999	Rustaiyan, Masoudi, et al., 1999	Sefidkon, Dabiri, et al., 1999	Sefidkon and Khajavi, 1999	Shafiee, Javidnia, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SPB-5	CP Sil 5 CB	OV-101	DB-5MS
Column length (m)	30.	60.	25.	25.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.32		0.20	0.25
Phase thickness (μm)	0.25	1.	0.39		0.25
T_start (C)	60.	40.	60.	80.	60.
T_end (C)	240.	200.	220.	240.	240.
Heat rate (K/min)	3.	3.	5.	6.	3.
Initial hold (min)		5.
Final hold (min)		2.
I	954.	959.	951.	946.	949.
Reference	Tellez, Canel, et al., 1999	Viallon C., Verdier-Metz I., et al., 1999	Weyerstahl, Marschall, et al., 1999	Zenkevich, Kosman, et al., 1999	Zoghbi, Andrade, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	SE-30	DB-5	HP-5
Column length (m)	50.	30.	25.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.2	0.25	0.2
Phase thickness (μm)	0.25	0.25		0.25	0.33
T_start (C)	60.	60.	60.	60.	70.
T_end (C)	240.	240.	180.	240.	290.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)			10.		8.
Final hold (min)	20.				20.
I	951.	945.	947.	949.	954.
Reference	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998	Jantan, Ahmad, et al., 1998	Maia, Zohhbi, et al., 1998	Poiana, Sicari, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	OV-101	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	60.	25.	25.	25.	25.
Carrier gas	He		N2	N2	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	50.	50.	50.	60.
T_end (C)	280.	200.	290.	290.	300.
Heat rate (K/min)	4.	5.	4.	4.	6.
Initial hold (min)	5.
Final hold (min)
I	970.	944.	937.	937.	937.
Reference	Stashenko, Cervantes, et al., 1998	Zollo, Biyiti, et al., 1998	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-Sulfur	SPB-Sulfur	DB-1	DB-5	DB-5
Column length (m)	30.	30.		30.	30.
Carrier gas	He	He		Helium	He
Substrate
Column diameter (mm)	0.32	0.32		0.25	0.25
Phase thickness (μm)	4.	4.		0.25
T_start (C)	45.	45.	80.	60.	60.
T_end (C)	240.	240.	220.	240.	240.
Heat rate (K/min)	5.	5.	6.	3.	4.
Initial hold (min)	13.	13.
Final hold (min)	5.	5.
I	964.	964.	938.	954.	953.
Reference	Mariaca, Berger, et al., 1997	Mariaca, Berger, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Zunino, Novillo-Newton, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	OV-101	OV-101	HP-1	HP-5
Column length (m)	23.	50.	50.	25.
Carrier gas	He	N2	He	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.32
Phase thickness (μm)	0.17	0.17		0.25
T_start (C)	60.	50.	50.	60.	35.
T_end (C)	250.	220.	250.	220.	200.
Heat rate (K/min)	5.	5.	2.	4.	6.
Initial hold (min)	3.			2.	2.
Final hold (min)	30.			20.
I	940.	950.	941.	940.	966.
Reference	Ayedoun, Adeoti, et al., 1996	Chacko, Jayalekshmy, et al., 1996	Orav, Kailas, et al., 1996	Thanh, Dung, et al., 1996	Larsen and Frisvad, 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	DB-1	DB-1	HP-5
Column length (m)	50.	60.	60.	60.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25
T_start (C)	70.	50.	70.	70.	35.
T_end (C)	180.	250.	270.	270.	200.
Heat rate (K/min)	1.	3.5	2.5	2.5	6.
Initial hold (min)		5.	5.	5.	2.
Final hold (min)
I	943.	942.	962.	962.	966.
Reference	Orav, Kuningas, et al., 1995	Stashenko, Torres, et al., 1995	Tirado, Stashenko, et al., 1995	Tirado, Stashenko, et al., 1995	Larsen and Frisvad, 1994
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	HP-5	HP-5	Methyl Silicone	Methyl Silicone
Column length (m)	50.			50.	50.
Carrier gas	N2			N2	N2
Substrate
Column diameter (mm)	0.27			0.25	0.25
Phase thickness (μm)	0.2			0.17	0.17
T_start (C)	80.	40.	40.	80.	80.
T_end (C)	240.	210.	210.	200.	200.
Heat rate (K/min)	3.	2.	2.	2.	3.
Initial hold (min)
Final hold (min)
I	948.	951.	952.	954.	954.
Reference	Ramanoelina, Viano, et al., 1994	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	Methyl Silicone	DB-1	SPB-5	SE-54
Column length (m)	25.	25.	60.	30.	30.
Carrier gas			He		Hydrogen
Substrate
Column diameter (mm)	0.25	0.50	0.32		0.25
Phase thickness (μm)			1.2	1.0	0.25
T_start (C)	60.	60.	30.	50.	60.
T_end (C)	280.	220.	240.	250.	250.
Heat rate (K/min)	5.	5.	3.	8.	2.
Initial hold (min)			10.		5.
Final hold (min)					2.
I	949.	951.	948.	948.	947.
Reference	Kaul, Singh, et al., 1993	Mallavarapu, Ramesh, et al., 1993	Ciccioli, Cecinato, et al., 1992	King and Knight, 1992	Kollmannsberger, Nitz, et al., 1992
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	RSL-150	BP-1	OV-101	OV-101
Column length (m)	30.	30.	25.	50.	50.
Carrier gas	N2			N2	N2
Substrate
Column diameter (mm)		0.32	0.33	0.25	0.25
Phase thickness (μm)		0.20
T_start (C)	80.	30.	45.	80.	80.
T_end (C)	220.	200.	180.	200.	200.
Heat rate (K/min)	4.	3.	3.	2.	2.
Initial hold (min)			3.
Final hold (min)
I	943.	942.	946.	952.	954.
Reference	Velasco-Negueruela, Pérez Alonso, et al., 1991	Ronse and De Pooter, 1990	Wyllie, Brophy, et al., 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	SE-30	OV-101	OV-101	OV-1
Column length (m)	50.	40.	50.	50.	60.
Carrier gas	H2	He	N2	N2	Helium
Substrate
Column diameter (mm)	0.30	0.50	0.25	0.25	0.50
Phase thickness (μm)		0.75			1.2
T_start (C)	40.	30.	80.	80.	40.
T_end (C)	250.	220.	200.	200.	220.
Heat rate (K/min)	10.	3.	2.	2.	2.
Initial hold (min)	1.
Final hold (min)
I	943.	939.	947.	954.	940.
Reference	Brophy, Davies, et al., 1989	de Pooter, de Buyck, et al., 1989	Sugisawa, Yang, et al., 1989	Sugisawa, Yang, et al., 1989	Wahab, Aboutabl, et al., 1987
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-1	OV-101	SE-30	SE-30+Igepal
Column length (m)	10.		50.	50.	100.
Carrier gas	H2	He	He	He
Substrate
Column diameter (mm)	0.25		0.31	0.5	0.25
Phase thickness (μm)	0.25
T_start (C)	50.	40.	0.	40.	70.
T_end (C)	250.	220.	225.	170.	170.
Heat rate (K/min)	5.	2.	3.	3.	1.
Initial hold (min)			1.	3.
Final hold (min)
I	945.	940.	934.	943.	948.
Reference	Perry, Baxter, et al., 1986	De Pooter, De Buyck, et al., 1986	del Rosario, de Lumen, et al., 1984	Heydanek and McGorrin, 1981	Shibamoto and Jennings, 1977
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary
Active phase	SE-30+Igepal	SF-96
Column length (m)	100.	111.
Carrier gas		Nitrogen
Substrate
Column diameter (mm)	0.25	0.76
Phase thickness (μm)
T_start (C)	70.
T_end (C)	170.	130.
Heat rate (K/min)	1.	3.
Initial hold (min)		8.
Final hold (min)		40.
I	952.	941.
Reference	Shibamoto and Jennings, 1977	Donetzhuber, Johansson, et al., 1976
Comment	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

Alizadeh and Shaabani, 2012
Alizadeh, A.; Shaabani, M., Essential oil composition, phenolic content, antioxidant and antimicrobial activity in Salvia officinalis L. cultivated in Iran, Adv. Environ. Biol., 2012, 6, 1, 221-226. [all data]

Bendiabdellah, El Amine Dib, et al., 2012
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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