2-Methoxy-4-vinylphenol


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSOptima-5HP-5 MSHP-5 MSOV-1
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHelium HeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.50.
Tend (C) 230.246.300.260.250.
Heat rate (K/min) 3.3.15.4.5.
Initial hold (min)  1.2. 3.
Final hold (min)   10.5.2.
I 1322.1313.1331.1306.1282.
ReferencePripdeevech and Saansoomchai, 2013Al-Qudah, Muhaidat, et al., 2012Xu, Han, et al., 2012Miyazawa, Marumoto, et al., 2011Hu, Liang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5HP-5 MSZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHydrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.70.70.40.
Tend (C) 290.290.290.290.280.
Heat rate (K/min) 5.5.5.5.6.
Initial hold (min)     1.
Final hold (min)  10. 10.9.
I 1318.1318.1319.1311.1324.
ReferenceLazarevic, Radulovic, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2Harrison and Priest, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-1HP-5 MSHP-1HP-1
Column length (m) 30.25.30.50.50.
Carrier gas Helium HeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.250.200.20
Phase thickness (μm) 0.250.170.250.330.33
Tstart (C) 70.50.60.60.60.
Tend (C) 290.260.300.250.250.
Heat rate (K/min) 5.1.15.2.2.
Initial hold (min)  5.2.  
Final hold (min) 10.5.10.20.20.
I 1318.1291.1331.1282.1287.
ReferenceRadulovic, Blagojevic, et al., 2009Wetwiayaklung, Thavanapong, et al., 2009Xu, Han, et al., 2009Breme, Langle, et al., 2008Breme, Langle, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5MSHP-5MSDB-5RTX-5Elite-5MS
Column length (m) 10.30.30.10.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.180.250.250.180.32
Phase thickness (μm) 0.180.250.250.20.5
Tstart (C) 40.50.60.40.40.
Tend (C) 295.280.240.275.280.
Heat rate (K/min) 10.5.2.50.4.
Initial hold (min) 1.54. 0.55.
Final hold (min)  10. 0.510.
I 1325.1317.1304.1327.1309.
ReferenceRisticevic, Carasek, et al., 2008Cho, Abd El-Aty, et al., 2007Miyazawa and Tamura, 2007Setkova, Risticevic, et al., 2007Tava, Pecetti, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBHP-1DB-5HP-5MS
Column length (m) 30.25.50.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.32 0.20.320.25
Phase thickness (μm) 0.25 0.5 0.25
Tstart (C) 40.80.60.60.50.
Tend (C) 250.270.250.250.280.
Heat rate (K/min) 4.10.2.4.5.
Initial hold (min) 2.  5.4.
Final hold (min) 5. 120. 10.
I 1317.1311.1278.1320.1318.
ReferenceXu, Fan, et al., 2007Ayoub, Al-Azizi, et al., 2006Castel, Fernandez, et al., 2006Fadel, Mageed, et al., 2006Kim, Abd El-Aty, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5SPB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHeliumHeliumH2
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.40.60.50.
Tend (C) 280.260.240.250.280.
Heat rate (K/min) 5.5.4.4.4.
Initial hold (min) 4.2. 2.2.
Final hold (min) 10.13.5.20.10.
I 1318.1314.1305.1312.1315.
ReferenceKim, El-Aty, et al., 2006Kucuk, Gulec, et al., 2006Miyazawa and Kawata, 2006Pino, Marquez, et al., 2006Pino, Sauri-Duch, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1HP-1DB-1DB-5
Column length (m) 13.550.50.25.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.20.20.250.25
Phase thickness (μm)  0.50.50.250.25
Tstart (C) 35.60.60.50.40.
Tend (C) 225.250.250.250.240.
Heat rate (K/min) 6.2.2.3.4.
Initial hold (min) 3.  3.2.
Final hold (min)  40.60.  
I 1316.1300.1286.1299.1313.
Referencede Souza, Vásquez, et al., 2006Valette, Fernandez, et al., 2006Bendimerad and Bendiab, 2005Cégiéla-Carlioz, Bessière, et al., 2005El-Sayed, Heppelthwaite, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5ZB-5DB-5HP-1
Column length (m) 30.30.60.30.50.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 60.40.40.60.60.
Tend (C) 250.260.260.280.220.
Heat rate (K/min) 4.2.6.4.2.
Initial hold (min) 2.5.4.610. 
Final hold (min) 20.20.1.40.40.
I 1323.1314.1326.1308.1277.
ReferencePino, Marbot, et al., 2005Senatore, Apostolides Arnold, et al., 2005Jürgens and Dötterl, 2004Pino, Marbot, et al., 2003Valette, Fernandez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5DB-5DB-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHe 
Substrate      
Column diameter (mm) 0.250.320.250.530.32
Phase thickness (μm) 0.250.250.251.50.5
Tstart (C) 60.40.60.40.35.
Tend (C) 250.230.240.225.275.
Heat rate (K/min) 4.6.3.6.6.
Initial hold (min) 2.2. 5. 
Final hold (min) 20.5. 30. 
I 1306.1320.1310.1312.1318.
ReferencePino, Marbot, et al., 2002Sanz, Czerny, et al., 2002Tellez, Khan, et al., 2002Cadwallader and Heo, 2001Rouseff, Jella, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5BP-5OV-101
Column length (m) 30.30.30.50.10.
Carrier gas HeH2H2HeHelium
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (μm) 0.250.50.51.0.52
Tstart (C) 40.60.60.40.35.
Tend (C) 230.245.245.190.225.
Heat rate (K/min) 6.3.3.2.6.
Initial hold (min) 2.3.3.5.3.
Final hold (min) 5.20.20.  
I 1324.1317.1317.1328.1279.
ReferenceCzerny and Grosch, 2000Kotseridis and Baumes, 2000Kotseridis and Baumes, 2000Lopez, Ferreira, et al., 1999Deibler, Acree, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima 1DB-1DB-1DB-1DB-1
Column length (m) 25.30.60.60.60.
Carrier gas HeliumHe HeHe
Substrate      
Column diameter (mm) 0.200.250.250.250.32
Phase thickness (μm) 0.250.25   
Tstart (C) 50.50.30.30.30.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 3.5.4.4.4.
Initial hold (min)   25.25.25.
Final hold (min)   20.20.20.
I 1297.1277.1280.1280.1280.
ReferenceFons, Rapior, et al., 1998Kjällstrand, Ramnäs, et al., 1998Buttery, Ling, et al., 1997Buttery and Ling, 1995Buttery, Stern, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedCapillaryCapillary
Active phase DB-1DB-1SE-54DB-1DB-5
Column length (m) 30.30.3.60.30.
Carrier gas HeHe  H2
Substrate   Chromosorb G AW DMCS (100-120 mesh)  
Column diameter (mm) 0.250.25  0.3
Phase thickness (μm) 0.250.25   
Tstart (C) 50.50.50.30.80.
Tend (C) 240.240.230.200.250.
Heat rate (K/min) 5.5.6.4.16.
Initial hold (min) 3.3.2.25. 
Final hold (min)   10.30. 
I 1286.1289.1315.1280.1277.
ReferenceShiota, 1993Shiota, 1993Schieberle, 1991Buttery, Takeoka, et al., 1990Spadone, Takeoka, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-1DB-1DB-5
Column length (m) 50.60.60.60.30.
Carrier gas H2   Hydrogen
Substrate      
Column diameter (mm) 0.30.320.320.320.35
Phase thickness (μm)  0.250.250.251.0
Tstart (C) 80.50.50.50.45.
Tend (C) 250.250.250.250.220.
Heat rate (K/min) 16.4.4.4.2.
Initial hold (min)      
Final hold (min)      
I 1328.1280.1280.1280.1326.
ReferenceSpadone, Takeoka, et al., 1990Flath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989Georgilopoulos and Gallois, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB5-30W
Column length (m) 30.
Carrier gas He
Substrate  
Column diameter (mm) 0.25
Phase thickness (μm) 0.25
Tstart (C) 60.
Tend (C) 300.
Heat rate (K/min) 5.
Initial hold (min)  
Final hold (min)  
I 1336.
ReferenceSchwab and Schreier, 1988
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Pino, Marbot, et al., 2005
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Senatore, Apostolides Arnold, et al., 2005
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Jürgens and Dötterl, 2004
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Pino, Marbot, et al., 2003
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Notes

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