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1,6,10-Dodecatriene, 7,11-dimethyl-3-methylene-


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5MSHP-1DB-1
Column length (m) 30.30.30.50.60.
Carrier gas HeliumHeliumHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 45.50.50.60.70.
Tend (C) 250.280.280.250.230.
Heat rate (K/min) 3.4.5.2.2.
Initial hold (min) 3. 4. 2.
Final hold (min) 5. 10.40.20.
I 1459.1459.1460.1444.1448.
ReferencePorto, Decorti, et al., 2009Zhao, Zeng, et al., 2009Cho, Abd El-Aty, et al., 2007Filippi, Lanfranchi, et al., 2006Sawamura, Onishi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5 MSCP Sil 5 CBOV-101
Column length (m) 25.30.30.20.50.
Carrier gas H2HeHeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.2
Phase thickness (mum) 0.520.250.250.250.5
Tstart (C) 50.60.60.100.50.
Tend (C) 280.275.240.270.250.
Heat rate (K/min) 2.54.3.8.2.
Initial hold (min) 5.  2. 
Final hold (min)      
I 1450.1464.1457.1422.1450.
ReferenceWang, Kong, et al., 2006Asadipour, Mehrabani, et al., 2005Urdampilleta, Amat, et al., 2005Thappa, Bakshi, et al., 2004Orav, Kailas, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5PTE-5CBP-1OV-101OV-101
Column length (m) 60.60.25.50.50.
Carrier gas  H2NitrogenHeN2
Substrate      
Column diameter (mm) 0.250.320.250.20.25
Phase thickness (mum) 0.250.300.25  
Tstart (C) 40.60.50.50.80.
Tend (C) 250.285.210.250.200.
Heat rate (K/min) 5.4.33.2.2.
Initial hold (min) 15. 2.  
Final hold (min)      
I 1460.1458.1446.1445.1449.
ReferenceStashenko, Jaramillo, et al., 2003Gudzic, Djokovic, et al., 2002Ly, Yamauchi, et al., 2001Orav and Kann, 2001Yang, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SPB-1OV-101DB-5MSSPB-5
Column length (m) 50.50.50.30.50.
Carrier gas N2 N2HeHe
Substrate      
Column diameter (mm) 0.250.20.20.250.32
Phase thickness (mum)  0.33 0.250.25
Tstart (C) 80.60.80.60.60.
Tend (C) 200.260.200.240.240.
Heat rate (K/min) 2.4.1.3.3.
Initial hold (min)      
Final hold (min)   20. 20.
I 1449.1447.1444.1458.1458.
ReferenceYang, 2001, 2Choo, Wong, et al., 1999Menon, Chacko, et al., 1999Zoghbi, Andrade, et al., 1999Doneanu and Anitescu, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1HP-5OV-1CBP-1HP-5
Column length (m) 50.25.30.25. 
Carrier gas HeHe He 
Substrate      
Column diameter (mm) 0.320.20.320.22 
Phase thickness (mum) 0.250.330.25  
Tstart (C) 50.70.40.60.35.
Tend (C) 250.290.270.240.200.
Heat rate (K/min) 10.3.2.5.6.
Initial hold (min) 5.8.4. 2.
Final hold (min) 20.20.   
I 1450.1484.1455.1458.1437.
ReferenceKökdil, Kurucu, et al., 1998Poiana, Sicari, et al., 1998Kökdil, Tanker, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Larsen and Frisvad, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-101RSL-150OV-101OV-101
Column length (m)  50.30.50.50.
Carrier gas  H2 N2N2
Substrate      
Column diameter (mm)  0.320.320.250.25
Phase thickness (mum)  0.30.20  
Tstart (C) 35.65.30.80.80.
Tend (C) 200.300.200.200.200.
Heat rate (K/min) 6.2.3.2.2.
Initial hold (min) 2.5.   
Final hold (min)      
I 1466.1472.1447.1448.1449.
ReferenceLarsen and Frisvad, 1995Demarne and van der Walt, 1993Ronse and De Pooter, 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-1OV-101OV-1
Column length (m) 50.50.50.50.40.
Carrier gas N2N2He He
Substrate      
Column diameter (mm) 0.250.250.200.300.5
Phase thickness (mum)   0.20 0.75
Tstart (C) 80.80.30.40.30.
Tend (C) 200.200.220.230.220.
Heat rate (K/min) 2.2.2.3.53.
Initial hold (min)    5. 
Final hold (min)      
I 1448.1449.1446.1448.1446.
ReferenceSugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989de Pooter, Nicolai, et al., 1988Nykanen, 1986de Pooter, de Buyck, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-101OV-3
Column length (m) 30.150.
Carrier gas He 
Substrate   
Column diameter (mm) 0.50.66
Phase thickness (mum) 0.8 
Tstart (C) 40.20.
Tend (C) 220.170.
Heat rate (K/min) 2.1.
Initial hold (min)   
Final hold (min)   
I 1447.1450.
ReferenceDe Pooter and Schamp, 1986Buttery, Xu, et al., 1985
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Porto, Decorti, et al., 2009
Porto, C.Da.; Decorti, D.; Kikic, I., Flavour compounds of Lavandula angustifolia L. to use in food manufacturing: comparison of three different extraction methods, Food Chem., 2009, 112, 4, 1072-1078, https://doi.org/10.1016/j.foodchem.2008.07.015 . [all data]

Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Cho, Abd El-Aty, et al., 2007
Cho, S.-K.; Abd El-Aty, A.M.; Choi, J.-H.; Kim, M.R.; Shim, J.H., Optimized conditions for the extraction of secondary volatile metabolites in Angelica roots by accelerated solvent extraction, J. Pharm. Biomed. Anal., 2007, 44, 5, 1154-1158, https://doi.org/10.1016/j.jpba.2007.03.011 . [all data]

Filippi, Lanfranchi, et al., 2006
Filippi, J.-J.; Lanfranchi, D.-A.; Prado, S.; Baldovini, N.; Meierhenrich, U.J., Composition, Enantiomeric Distribution, and Antibacterial Activity of the Essential Oil of Achillea ligustica All. from Corsica, J. Agric. Food Chem., 2006, 54, 17, 6308-6313, https://doi.org/10.1021/jf060752y . [all data]

Sawamura, Onishi, et al., 2006
Sawamura, M.; Onishi, Y.; Ikemoto, J.; Tu, N.T.M.; Phi, N.T.L., Characteristic odour components of bergamot (Citrus bergamia Risso) essential oil, Flavour Fragr. J., 2006, 21, 4, 609-615, https://doi.org/10.1002/ffj.1604 . [all data]

Wang, Kong, et al., 2006
Wang, P.; Kong, C.H.; Zhang, C.X., Chemical Composition and Antimicrobial Activity of the Essential Oil from Ambrosia trifida L., Molecules, 2006, 11, 7, 549-555, https://doi.org/10.3390/11070549 . [all data]

Asadipour, Mehrabani, et al., 2005
Asadipour, A.; Mehrabani, M.; Najafi, M.L., Volatile oil composition of Centaurea aucheri (DC.) wagenitz, DARU, 2005, 13, 3, 160-164. [all data]

Urdampilleta, Amat, et al., 2005
Urdampilleta, J.D.; Amat, A.G.; Bidau, C.J.; Koslobsky, N.K., Biosystematic and chemosystematic studies in five South Americal species of Conyza (Asteraceae), Bol. Soc. Argent. Bot., 2005, 40, 1-2, 101-107. [all data]

Thappa, Bakshi, et al., 2004
Thappa, R.K.; Bakshi, S.K.; Dhar, L.; Agarwal, S.G.; Kitchlu, S.; Kaul, M.K.; Suri, K.A., Significance of changed climatic factors on essential oil composition of Echinacea purpurea under subtropical conditions, Flavour Fragr. J., 2004, 19, 5, 452-454, https://doi.org/10.1002/ffj.1352 . [all data]

Orav, Kailas, et al., 2003
Orav, A.; Kailas, T.; Jegorova, A., Composition of the essential oil of dill, celery, and parsley from Estonia, Proc. Est. Acad. Sci. Chem., 2003, 52, 4, 147-154. [all data]

Stashenko, Jaramillo, et al., 2003
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Comparación de la composición química y de la actividad antioxidante in vitro de los metabolitos secundarios volátiles de plantas de la familia verbenaceae, Rev. Acad. Colomb. Cienc. Exactas Fis. Nat., 2003, 27, 105, 579-597. [all data]

Gudzic, Djokovic, et al., 2002
Gudzic, B.; Djokovic, D.; Vajs, V.; Palic, R.; Stojanovic, G., Composition and antimicrobial activity of the essential oil of Hypericum maculatum Crantz, Flavour Fragr. J., 2002, 17, 5, 392-394, https://doi.org/10.1002/ffj.1112 . [all data]

Ly, Yamauchi, et al., 2001
Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

Orav and Kann, 2001
Orav, A.; Kann, J., Determination of peppermint and orange aroma compounds in food and beverages, Proc. Est. Acad. Sci. Chem., 2001, 50, 4, 217-225. [all data]

Yang, 2001
Yang, R., Analysis of the volatile components in peel oil of Yuzu by gas chromatography/mass spectrometry, Chin. J. Anal. Chem., 2001, 29, 3, 313-316. [all data]

Yang, 2001, 2
Yang, R., Volatile compounds in peel oil of Citrus sudachi, Food Sci. (Beijing), 2001, 22, 3, 71-73. [all data]

Choo, Wong, et al., 1999
Choo, L.-C.; Wong, S.-M.; Liew, K.-Y., Essential oil of nutmeg pericarp, J. Sci. Food Agric., 1999, 79, 13, 1954-1957, https://doi.org/10.1002/(SICI)1097-0010(199910)79:13<1954::AID-JSFA460>3.0.CO;2-I . [all data]

Menon, Chacko, et al., 1999
Menon, A.N.; Chacko, S.; Narayanan, C.S., Free and glycosidically bound volatiles of cardamom (Eletteria cardamomum Maton var. miniscula Burkill), Flavour Fragr. J., 1999, 14, 1, 65-68, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<65::AID-FFJ789>3.0.CO;2-A . [all data]

Zoghbi, Andrade, et al., 1999
Zoghbi, M.G.B.; Andrade, E.H.A.; Maia, J.G.S., Volatile constituents from leaves and flowers of Alpinia speciosa K. Schum. and A. purpurata (Viell.) Schum., Flavour Fragr. J., 1999, 14, 6, 411-414, https://doi.org/10.1002/(SICI)1099-1026(199911/12)14:6<411::AID-FFJ854>3.0.CO;2-U . [all data]

Doneanu and Anitescu, 1998
Doneanu, C.; Anitescu, G., Supercritical carbon dioxide extraction of Angelica archangelica L. root oil, J. Supercrit. Fluids, 1998, 12, 1, 59-67, https://doi.org/10.1016/S0896-8446(97)00040-5 . [all data]

Kökdil, Kurucu, et al., 1998
Kökdil, G.; Kurucu, S.; Yildiz, A., Essential oil composition of Nepeta nuda L. ssp. nuda, Flavour Fragr. J., 1998, 13, 4, 233-234, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<233::AID-FFJ730>3.0.CO;2-7 . [all data]

Poiana, Sicari, et al., 1998
Poiana, M.; Sicari, V.; Mincione, B., Supercritical carbon dioxide (SC-CO2) extraction of grapefruit flavedo, Flavour Fragr. J., 1998, 13, 2, 125-130, https://doi.org/10.1002/(SICI)1099-1026(199803/04)13:2<125::AID-FFJ708>3.0.CO;2-# . [all data]

Kökdil, Tanker, et al., 1997
Kökdil, G.; Tanker, M.; Kurucu, S.; Topcu, G., Essential oil analysis of Nepeta cilicia Boiss., Flavour Fragr. J., 1997, 12, 2, 99-101, https://doi.org/10.1002/(SICI)1099-1026(199703)12:2<99::AID-FFJ619>3.0.CO;2-# . [all data]

Zygadlo, Ariza-Espinar, et al., 1997
Zygadlo, J.A.; Ariza-Espinar, L.; Velasco-Negueruela, A.; Perez-Alonso, M.J., Volatile constituents of Stevia achalensis hieronymus, Flavour Fragr. J., 1997, 12, 4, 297-299, https://doi.org/10.1002/(SICI)1099-1026(199707)12:4<297::AID-FFJ625>3.0.CO;2-2 . [all data]

Larsen and Frisvad, 1995
Larsen, T.O.; Frisvad, J.C., Characterization of volatile metabolites from 47 Penicillium taxa, Mycol. Res., 1995, 99, 10, 1153-1166, https://doi.org/10.1016/S0953-7562(09)80271-2 . [all data]

Demarne and van der Walt, 1993
Demarne, F.-E.; van der Walt, J.J.A., Composition of the Essential Oil of Pelargonium citronellum (Geraniaceae), J. Essent. Oil Res., 1993, 5, 3, 233-238, https://doi.org/10.1080/10412905.1993.9698214 . [all data]

Ronse and De Pooter, 1990
Ronse, A.C.; De Pooter, H.L., Essential Oil Production by Belgian Artemisia alba (Turra) before and after Micropropagation, J. Essent. Oil Res., 1990, 2, 5, 237-242, https://doi.org/10.1080/10412905.1990.9697873 . [all data]

Yang and Sugisawa, 1990
Yang, R.; Sugisawa, H., Citrus Suachi Hort. ex Shirai. Volatile components in Sudachi (Citrus Sudachi Hort. ex Shirai) juice, Nippon Shokuhin Kogyo Gakkaishi, 1990, 37, 12, 946-952, https://doi.org/10.3136/nskkk1962.37.12_946 . [all data]

Sugisawa, Yang, et al., 1989
Sugisawa, H.; Yang, R.H.; Kawabata, C.; Tamura, H., Volatile constituents in the peel oil of sudachi (Citrus sudachi), Agric. Biol. Chem., 1989, 53, 6, 1721-1723, https://doi.org/10.1271/bbb1961.53.1721 . [all data]

de Pooter, Nicolai, et al., 1988
de Pooter, H.L.; Nicolai, B.; De Laet, J.; De Buyck, L.F.; Schamp, N.M.; Goetghebeur, P., The Essential Oils of Five Nepeta Species. A Preliminary Evaluation of their Use in Chemotaxonomy by Cluster Analysis, Flavour Fragr. J., 1988, 3, 4, 155-159, https://doi.org/10.1002/ffj.2730030404 . [all data]

Nykanen, 1986
Nykanen, I., High Resolution Gas Chromatographic - Mass Spectrometric determination of the Flavour Composition of Wild Majoram (Origanum vulgare L.) Cultivated in Finland, Z. Lebensm Unters Forsch, 1986, 183, 4, 267-272, https://doi.org/10.1007/BF01087742 . [all data]

de Pooter, de Buyck, et al., 1986
de Pooter, H.L.; de Buyck, L.F.; Schamp, N.M.; Aboutabl, E.; De Bruyn, A.; Husain, S.Z., The Volatile Fraction of Senecio glaucus subsp. coronopifolius, Flavour Fragr. J., 1986, 1, 4-5, 159-163, https://doi.org/10.1002/ffj.2730010406 . [all data]

De Pooter and Schamp, 1986
De Pooter, H.L.; Schamp, N.M., Comparison of the Volatile Composition of Some Calamintha/Satureja Species, Prog. Essnt. Oil. Res., 1986, 139-150. [all data]

Buttery, Xu, et al., 1985
Buttery, R.G.; Xu, C.; Ling, L.C., Volatile components of wheat leaves (and stems): Possible insect attractants, J. Agric. Food Chem., 1985, 33, 1, 115-117, https://doi.org/10.1021/jf00061a033 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References