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1,6,10-Dodecatriene, 7,11-dimethyl-3-methylene-


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5DB-5HP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Program 50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)not specifiednot specified50 0C 95 min) 3 0C/min -> 100 0C 4 0C/min -> 160 0C 5 0C/min -> 220 0C (15 min)40C(3min) => 8C/min => 160C => 15C/min => 300C (10min)
I 1451.1445.1461.1456.1457.
ReferenceDelort and Jaquier, 2009Porto, Decorti, et al., 2009Porto, Decorti, et al., 2009Yang, Yang, et al., 2009Liu, Song, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1HP-5MSSE-52SPB-5VF-5MS
Column length (m) 30.30.25.30.30.
Carrier gas HeliumHeH2HeliumHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.420.100.25
Program 40 0C (2 min) 6 0C/min -> 130 0C 10 0C/min -> 300 0C40C(3min) => 6C/min => 160C => 10C/min => 300C (10min)60C(8min) => 3C/min => 180C => 20C/min => 250C (10min)40 0C (1 min) 10 0C/min -> 120 0C 0.5 0C/min -> 150 0C 20 0C/min -> 280 0C (5 min)40C(1min) => 15C/min => 100C => 4C/min => 250C (1min)
I 1444.1460.1455.1458.1434.
ReferenceSuschke, Sporer, et al., 2007Yu, Huang, et al., 2007Lorenzo, Loayza, et al., 2006Navickiene, Morandim, et al., 2006Xie, Sun, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5CP Sil 8 CBCP Sil 8 CBCP-Sil 8CB-MS
Column length (m) 50.30.50.50.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.250.320.320.32
Phase thickness (mum) 0.250.1 0.25 
Program 60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)35C => 4C/min => 180C => 10C/min => 250C60C(2min) => 5C/min => 160C (1min) => 10C/min => 250C (2min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)60C(1min) => 3C/min => 70C => 15C/min => 170C(8min) => 5C/min => 250C
I 1458.1435.1460.1458.1443.
ReferenceNivinskienë, Butkienë, et al., 2005Albuquerque, Silveira, et al., 2004Judpentienë and Mockutë, 2004Judpentienë and Mockutë, 2004, 2Mockute, Bernotiene, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30CBP-1OV-101SE-30
Column length (m) 60.60.25.50.30.
Carrier gas HeHeNitrogenN2Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)   0.25 0.20
Program 50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0Cnot specifiednot specifiednot specifiednot specified
I 1476.1476.1448.1449.1448.
ReferenceLi, Wu, et al., 2002Li, Wu, et al., 2002Ly, Yamauchi, et al., 2001Yang, 2001Prikhod'ko, Klyuev, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-5DB-5OV-101OV-1
Column length (m) 50.30.30. 35.
Carrier gas He    
Substrate      
Column diameter (mm) 0.320.250.25 0.50
Phase thickness (mum) 0.250.250.25 1.5
Program 1)50C(1min) => 4C/min => 180C => 2C/min => 250C(10min) 2)50C(1min) => 6C/min => 200C => 12C/min => 250C(5min)35C(1min) => 5C/min => 230C => 20C/min => 280C35C(1min) => 5C/min => 230C => 20C/min => 280Cnot specifiednot specified
I 1450.1462.1462.1449.1446.
ReferenceKökdil, 1998Jelen H.H., Mirocha C.J., et al., 1995Jelen H.H., Mirocha C.J., et al., 1995De Pooter, Vermeesch, et al., 1989De Pooter and Schamp, 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Delort and Jaquier, 2009
Delort, E.; Jaquier, A., Novel terpenyl esters from Australian finger lime (Citrus australasica) peel extract, Flav. Fragr. J., 2009, 24, 3, 123-132, https://doi.org/10.1002/ffj.1922 . [all data]

Porto, Decorti, et al., 2009
Porto, C.Da.; Decorti, D.; Kikic, I., Flavour compounds of Lavandula angustifolia L. to use in food manufacturing: comparison of three different extraction methods, Food Chem., 2009, 112, 4, 1072-1078, https://doi.org/10.1016/j.foodchem.2008.07.015 . [all data]

Yang, Yang, et al., 2009
Yang, Z.; Yang, W.; Peng, Q.; He, Q.; Feng, Y.; Luo, S.; Yu, Z., Volatile phytochemical composition of rhisome of ginger after extraction by headspace solid-phase microextraction, petrol ether extraction and steam distillation extraction, Bangladesh J. Pharmacol., 2009, 4, 2, 136-143, https://doi.org/10.3329/bjp.v4i2.3232 . [all data]

Liu, Song, et al., 2007
Liu, L.; Song, G.; Hu, Y., GC?MS Analysis of the Essential Oils of Piper nigrum L. and Piper longum L., Chromatographia, 2007, 66, 9-10, 785-790, https://doi.org/10.1365/s10337-007-0408-2 . [all data]

Suschke, Sporer, et al., 2007
Suschke, U.; Sporer, F.; Schneele, J.; Geiss, H.K.; Reichling, J., Antibacterial and Cytotoxic activity of Nepeta cataria L., Nepeta cataria var. citriodora (Beck.) Balb. and Melissa officinalis L. essential oils, Natural Product Communications, 2007, 2, 12, 1277-1286. [all data]

Yu, Huang, et al., 2007
Yu, Y.; Huang, T.; Yang, B.; Liu, X.; Duan, G., Development of gas chromatography-mass spectrometry with microwave distillation and simultaneous solid-phase microextraction for rapid determination of volatile constituents in ginger, J. Pharm. Biomed. Anal., 2007, 43, 1, 24-31, https://doi.org/10.1016/j.jpba.2006.06.037 . [all data]

Lorenzo, Loayza, et al., 2006
Lorenzo, D.; Loayza, I.; Dellacassa, E., Composition and chiral characterization of the essential oil of Buddleja tucumanensis from Bolivia, Flavour Fragr. J., 2006, 21, 1, 95-98, https://doi.org/10.1002/ffj.1526 . [all data]

Navickiene, Morandim, et al., 2006
Navickiene, H.M.D.; Morandim, A.A.; Alécio, A.C.; Regasini, L.O.; Bergamo, D.C.B.; Telascrea, M.; Cavalheiro, A.J.; Lopes, M.N.; Bolzani, V.S.; Furlan, M.; Marques, M.O.M.; Young, M.C.M.; Kato, M.J., Composition and antifungal activity of essential oils from Piper aduncum, Piper arboreum and Piper tuberculatum, Quim. Nova, 2006, 29, 3, 467-470, https://doi.org/10.1590/S0100-40422006000300012 . [all data]

Xie, Sun, et al., 2006
Xie, J.; Sun, B.; Yu, M., Constituents of top fragrance from fresh flowers of Robinia Pseudoacacia L. occurring in China, Flavour Fragr. J., 2006, 21, 5, 798-800, https://doi.org/10.1002/ffj.1720 . [all data]

Nivinskienë, Butkienë, et al., 2005
Nivinskienë, O.; Butkienë, R.; Mockutë, D., Chemical composition of seed (fruit) essential oils of Angelica archangelica L. growing wild in Lithuania, Chemija, 2005, 16, 3-4, 51-54. [all data]

Albuquerque, Silveira, et al., 2004
Albuquerque, M.R.J.R.; Silveira, E.R.; Uchôa, D.E.A.; Lemos, T.L.G.; Souza, E.B.; Santiago, G.M.P.; Pessoa, O.D.L., Chemical composition and larvicidal activity of the essential oils from Eupatorium betonicaeforme (D.C.) Baker (Asteraceae), J. Agric. Food Chem., 2004, 52, 22, 6708-6711, https://doi.org/10.1021/jf0352881 . [all data]

Judpentienë and Mockutë, 2004
Judpentienë, A.; Mockutë, D., Chemical composition of essential oils produced by pink flower inflorescences of wild Achillea millefolium L., Chemija, 2004, 15, 28-32. [all data]

Judpentienë and Mockutë, 2004, 2
Judpentienë, A.; Mockutë, D., Chemical composition of essential oils of Artemisia absinthium L. (wormwood) growing wild in Vilnius, Chemija, 2004, 15, 4, 64-68. [all data]

Mockute, Bernotiene, et al., 2003
Mockute, D.; Bernotiene, G.; Judzentiene, A., Volatile compounds of the aerial parts of wild St. John's wort (Hypericum perforatum L.) plants, Chemija, 2003, 14, 3, 108-111. [all data]

Li, Wu, et al., 2002
Li, C.; Wu, H.; Yang, L.; ren, Y., Study of the composition of ginger oil from Laifeng, Flavour Fragr. Cosmetics, 2002, 5, 15-17. [all data]

Ly, Yamauchi, et al., 2001
Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

Yang, 2001
Yang, R., Analysis of the volatile components in peel oil of Yuzu by gas chromatography/mass spectrometry, Chin. J. Anal. Chem., 2001, 29, 3, 313-316. [all data]

Prikhod'ko, Klyuev, et al., 1999
Prikhod'ko, A.B.; Klyuev, N.A.; Volkovich, S.V.; Emets, T.I.; Petrenko, V.V.; Dolya, E.V., Component composition od the essential oil of Thymus dimorphus, Chem. Nat. Comp., 1999, 35, 1, 46-51, https://doi.org/10.1007/BF02238208 . [all data]

Kökdil, 1998
Kökdil, G., Composition of the essential oil of Clinopodium vulgare L. ssp. arundanum (Boiss.) Nyman collected from two different localities in Turkey, Flavour Fragr. J., 1998, 13, 3, 170-172, https://doi.org/10.1002/(SICI)1099-1026(199805/06)13:3<170::AID-FFJ721>3.0.CO;2-H . [all data]

Jelen H.H., Mirocha C.J., et al., 1995
Jelen H.H.; Mirocha C.J.; Wasowicz E.; Kaminski E., Production of volatile sesquiterpenes by Fusarium sambucinum strans with different abilities to synthesize trichlothecenes, Appl. Environ. Microbiol., 1995, 61, 11, 3815-3820. [all data]

De Pooter, Vermeesch, et al., 1989
De Pooter, H.L.; Vermeesch, J.; Schamp, N.M., The Essential Oils of Tanacetum vulgare L. and Tanacetum parthenium (L.) Schultz-Bip, J. Essent. Oil Res., 1989, 1, 1, 9-13, https://doi.org/10.1080/10412905.1989.9699438 . [all data]

De Pooter and Schamp, 1987
De Pooter, H.L.; Schamp, N.M., The Essential Oil of Mentha X villosa nm. alopecuroides, Flavour Fragr. J., 1987, 2, 4, 163-165, https://doi.org/10.1002/ffj.2730020405 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References