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Secobarbital

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase DB-5BP-1BP-1SPB-1SE-30
Column length (m) 15.25.25.25. 
Carrier gas HeN2N2He 
Substrate      
Column diameter (mm) 0.250.220.530.20 
Phase thickness (mum) 0.20.251.  
Temperature (C) 220.200.200.250.200.
I 1810.1772.1777.1786.1770.
ReferencePhillips, Logan, et al., 1990Japp, Gill, et al., 1987Japp, Gill, et al., 1987Lora-Tamayo, Rams, et al., 1986Stead, Gill, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase OV-1OV-101OV-101OV-101OV-101
Column length (m)  2.2.2.2.
Carrier gas  N2N2N2N2
Substrate  Chromosorb G AW DMCS (80-100 mesh)Chromosorb G AW DMCS (80-100 mesh)Chromosorb G AW DMCS (80-100 mesh)Chromosorb G AW DMCS (80-100 mesh)
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 200.200.200.200.200.
I 1790.1790.1790.1795.1815.
ReferenceBerninger and Möller, 1977Möller, 1976Möller, 1976Möller, 1976Möller, 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Phillips, Logan, et al., 1990
Phillips, A.M.; Logan, B.K.; Stafford, D.T., Further applications for capillary gas chromatography in routine quantitative toxicological analyses, J. Hi. Res. Chromatogr., 1990, 13, 11, 754-758, https://doi.org/10.1002/jhrc.1240131106 . [all data]

Japp, Gill, et al., 1987
Japp, M.; Gill, R.; Osselton, M.D., Comparison of drug retention indices determined on packed, wide bore capillary and narrow bore capillary columns, J. Forensic Sci., 1987, 32, 6, 1574-1586. [all data]

Lora-Tamayo, Rams, et al., 1986
Lora-Tamayo, C.; Rams, M.A.; Chacon, J.M.R., Gas Chromatographic Data for 187 Nitrogen- or Phosphorus-Containing Drugs and Metabolites of Toxicological Interest Analysed on Methyl Silicone Capillary Columns, J. Chromatogr., 1986, 374, 73-85, https://doi.org/10.1016/S0378-4347(00)83254-5 . [all data]

Stead, Gill, et al., 1982
Stead, A.H.; Gill, R.; Evans, A.T.; Moffat, A.C., Predictions of gas chromatographic retention characteristics of barbiturates from molecular structure, J. Chromatogr., 1982, 234, 2, 277-283, https://doi.org/10.1016/S0021-9673(00)81866-X . [all data]

Berninger and Möller, 1977
Berninger, H.; Möller, M.R., Retentionsindices zur gaschromatographischen Identifizierung von Arzneimitteln, Arch. Toxicol., 1977, 37, 4, 295-305, https://doi.org/10.1007/BF00330821 . [all data]

Möller, 1976
Möller, M.R., Comparability of retention indices of polar substances at elevated temperatures, Chromatographia, 1976, 9, 7, 311-314, https://doi.org/10.1007/BF02268832 . [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References